Atmospheric pressure gas chromatography-time-of-flight-mass spectrometry (APGC-ToF-MS) for the determination of regulated and emerging contaminants in aqueous samples after stir bar sorptive extraction (SBSE)

Analytica Chimica Acta

Volumn 851, Issue C, 2014, Pages 1-13

  Pintado Herrera, Marina G ^a   González Mazo, Eduardo ^a   Lara Martín, Pablo A ^a  

^a UNIVERSITY OF CÁDIZ   (Spain)

Author keywords

Atmospheric pressure gas chromatography; Emerging contaminants; Regulated contaminants; Stir bar sorptive extraction; Water

Indexed keywords

AROMATIC HYDROCARBONS; ATMOSPHERIC IONIZATION; ATMOSPHERIC PRESSURE; CHROMATOGRAPHY; CONTAMINATION; DRUG PRODUCTS; EFFLUENTS; FILTRATION; FLAME RETARDANTS; GAS CHROMATOGRAPHY; GROUNDWATER; IMPACT IONIZATION; INDUCTIVELY COUPLED PLASMA; IONIC STRENGTH; IONIZATION; IONIZATION OF GASES; MASS SPECTROMETRY; ODORS; ORGANIC POLLUTANTS; POLYCHLORINATED BIPHENYLS; POLYCYCLIC AROMATIC HYDROCARBONS; SEWAGE; SPECTROMETRY; WATER; WATER POLLUTION;

ELECTRON IMPACT-IONIZATION; EMERGING CONTAMINANT; ORGANOPHOSPHORUS FLAME RETARDANTS; POLYCHLORINATED BIPHENYL (PCBS); POLYCYCLIC AROMATIC HYDROCARBONS (PAHS); SIMULTANEOUS DETERMINATIONS; STIR BAR SORPTIVE EXTRACTION; TIME OF FLIGHT MASS SPECTROMETRY;

EXTRACTION;

BIOCIDE; CHEMOREPELLENT; ENDOCRINE DISRUPTOR; FLAME RETARDANT; FRAGRANCE; GROUND WATER; ORGANIC COMPOUND; ORGANOPHOSPHORUS COMPOUND; PESTICIDE; POLYCHLORINATED BIPHENYL DERIVATIVE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE; RADIOPROTECTIVE AGENT; RIVER WATER; SEA WATER; WATER; WATER POLLUTANT;

ACCURACY; AQUATIC ENVIRONMENT; AQUEOUS SOLUTION; ARTICLE; ATMOSPHERIC PRESSURE GAS CHROMATOGRAPHY TIME OF FLIGHT MASS SPECTROMETRY; CHEMICAL ANALYSIS; DESORPTION; GAS CHROMATOGRAPHY; IONIC STRENGTH; IONIZATION; LIMIT OF DETECTION; LIQUID DESORPTION; MEASUREMENT; PH; PRIORITY JOURNAL; PROCESS OPTIMIZATION; RESIDUE ANALYSIS; SEPARATION TECHNIQUE; SEWAGE EFFLUENT; STIR BAR SORPTIVE EXTRACTION; TIME; TIME OF FLIGHT MASS SPECTROMETRY; ULTRAVIOLET RADIATION; VALIDATION PROCESS; WATER SAMPLING; ANALYSIS; ATMOSPHERIC PRESSURE; CHEMISTRY; FRACTIONATION; ISOLATION AND PURIFICATION; MASS FRAGMENTOGRAPHY; OSMOLARITY; PROCEDURES; SOCIAL CONTROL; WATER POLLUTANT;

ATMOSPHERIC PRESSURE; CHEMICAL FRACTIONATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HYDROGEN-ION CONCENTRATION; OSMOLAR CONCENTRATION; SOCIAL CONTROL, FORMAL; WATER; WATER POLLUTANTS, CHEMICAL;

EID: 84927579080     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2014.05.030     Document Type: Article

References (39)

1. Gomez M.J., Herrera S., Sole D., Garcia-Calvo E., Fernandez-Alba A.R. Automatic searching and evaluation of priority and emerging contaminants in wastewater and river water by stir bar sorptive extraction followed by comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry. Anal. Chem. 2011, 83:2638-2647.
2. Johnsen A., Karlson U. Diffuse PAH contamination of surface soils: environmental occurrence, bioavailability, and microbial degradation. Appl. Microbiol. Biotechnol. 2007, 76:533-543.
3. Stockholm convention on persistent organic pollutants. , 2001. http://www.wipo.int/wipolex/en/other_treaties/text.jsp%3Ffile_id=194841.
4. Pintado-Herrera M.G., Gonzalez-Mazo E., Lara-Martin P.A. Determining the distribution of triclosan and methyl triclosan in estuarine settings. Chemosphere 2013, 95:478-485.
5. Jaspers V.L.B., Sonne C., Soler-Rodriguez F., Boertmann D., Dietz R., Eens M., Rasmussen L.M., Covaci A. Persistent organic pollutants and methoxylated polybrominated diphenyl ethers in different tissues of white-tailed eagles (Haliaeetus albicilla) from West Greenland. Environ. Pollut. 2013, 175:137-146.
6. O'Toole S., Metcalfe C. Synthetic musks in fish from urbanized areas of the lower Great Lakes, Canada. J. Great Lakes Res. 2006, 32:361-369.
7. Gago-Ferrero P., Diaz-Cruz M., Barcelo D. An overview of UV-absorbing compounds (organic UV filters) in aquatic biota. Anal. Bioanal. Chem. 2012, 404:2597-2610.
8. European water policy directive 2008/105/EC. , 2008. http://eur-lex.europa.eu/LexUriServ/LexUriServ.do%3Furi=CELEX:32008L0105:EN:NOT.
9. Azzouz A., Souhail B., Ballesteros E. Continuous solid-phase extraction and gas chromatography-mass spectrometry determination of pharmaceuticals and hormones in water samples. J. Chromatogr. A 2010, 1217:2956-2963.
10. Krüger O., Christoph G., Kalbe U., Berger W. Comparison of stir bar sorptive extraction (SBSE) and liquid-liquid extraction (LLE) for the analysis of polycyclic aromatic hydrocarbons (PAH) in complex aqueous matrices. Talanta 2011, 85:1428-1434.
11. Liu H., Liu L., Xiong Y., Yang X., Luan T. Simultaneous determination of UV filters and polycyclic musks in aqueous samples by solid-phase microextraction and gas chromatography-mass spectrometry. J. Chromatogr. A 2010, 1217:6747-6753.
12. Barco-Bonilla N., Romero-González R., Plaza-Bolaños P., Fernández-Moreno J.L., Garrido Frenich A., Martínez Vidal J.L. Comprehensive analysis of polycyclic aromatic hydrocarbons in wastewater using stir bar sorptive extraction and gas chromatography coupled to tandem mass spectrometry. Anal. Chim. Acta 2011, 693:62-71.
13. Kawaguchi M., Ito R., Honda H., Endo N., Okanouchi N., Saito K., Seto Y., Nakazawa H. Simultaneous analysis of benzophenone sunscreen compounds in water sample by stir bar sorptive extraction with in situ derivatization and thermal desorption-gas chromatography-mass spectrometry. J. Chromatogr. A 2008, 1200:260-263.
14. Prieto A., Basauri O., Rodil R., Usobiaga A., Fernández L.A., Etxebarria N., Zuloaga O. Stir-bar sorptive extraction: a view on method optimisation, novel applications, limitations and potential solutions. J. Chromatogr. A 2010, 1217:2642-2666.
15. Pérez-Carrera E., León V.M., Parra Gómez A., González-Mazo E. Simultaneous determination of pesticides, polycyclic aromatic hydrocarbons and polychlorinated biphenyls in seawater and interstitial marine water samples, using stir bar sorptive extraction-thermal desorption-gas chromatography-mass spectrometry. J. Chromatogr. A 2007, 1170:82-90.
16. Pintado-Herrera M.G., Gonzalez-Mazo E., Lara-Martin P.A. Environmentally friendly analysis of emerging contaminants by pressurized hot water extraction-stir bar sorptive extraction-derivatization and gas chromatography-mass spectrometry. Analytical and Bioanalytical Chemistry 2013, 405:401-411.
17. Quintana J.B., Rodil R., Muniategui-Lorenzo S., López-Mahía P., Prada-Rodríguez D. Multiresidue analysis of acidic and polar organic contaminants in water samples by stir-bar sorptive extraction-liquid desorption-gas chromatography-mass spectrometry. J. Chromatogr. A 2007, 1174:27-39.
18. Machado S., GonÇalves C., Cunha E., Guimaraes A., Alpendurada M.F. New developments in the analysis of fragrances and earthy-musty compounds in water by solid-phase microextraction (metal alloy fibre) coupled with gas chromatography (tandem) mass spectrometry. Talanta 2011, 84:1133-1140.
19. Canellas E., Vera P., Domeño C., Alfaro P., Nerín C. Atmospheric pressure gas chromatography coupled to quadrupole-time of flight mass spectrometry as a powerful tool for identification of non intentionally added substances in acrylic adhesives used in food packaging materials. J. Chromatogr. A 2012, 1235:141-148.
20. Portolés T., Cherta L., Beltran J., Hernández F. Improved gas chromatography-tandem mass spectrometry determination of pesticide residues making use of atmospheric pressure chemical ionization. J. Chromatogr. A 2012, 1260:183-192.
21. Stevens D., Shi Q., Hsu C.S. Novel analytical technique for petroleum biomarker analysis. Energ. Fuel. 2013, 27:167-171.
22. Magi E., Di Carro M., Scapolla C., Nguyen K.T.N. Stir Bar Sorptive Extraction and LC-MS/MS for trace analysis of UV filters in different water matrices. Chromatographia 2012, 1-10.
23. Kataoka H. Derivatization reactions for the determination of amines by gas chromatography and their applications in environmental analysis. J. Chromatogr. A 1996, 733:19-34.
24. Buchholz K.D., Pawllszyn J. Optimization of solid -phase microextraction conditions for determination of phenols. Anal. Chem. 1994, 66:160-167.
25. K.K. Stenerson, The derivatization and analysis of amino acids by GC-MS. Reporter US. 25.3. , 2011. http://www.sigmaaldrich.com/content/dam/sigma-aldrich/articles/reporter-us/pdf/the-derivatization.pdf.
26. Kawaguchi M., Ishii Y., Sakui N., Okanouchi N., Ito R., Inoue K., Saito K., Nakazawa H. Stir bar sorptive extraction with in situ derivatization and thermal desorption-gas chromatography-mass spectrometry in the multi-shot mode for determination of estrogens in river water samples. J. Chromatogr. A 2004, 1049:1-8.
27. Kumirska J., Plenis A., Lukaszewicz P., Caban M., Migowska N., Bialk-Bielinska A., Czerwicka M., Stepnowski P. Chemometric optimization of derivatization reactions prior to gas chromatography-mass spectrometry analysis. J. Chromatogr. A 2013, 1296:164-178.
28. Negreira N., Rodriguez I., Rubi E., Cela R. Dispersive liquid-liquid microextraction followed by gas chromatography-mass spectrometry for the rapid and sensitive determination of UV filters in environmental water samples. Anal. Bioanal. Chem. 2010, 398:995-1004.
29. Ramírez N., Marcé R.M., Borrull F. Development of a stir bar sorptive extraction and thermal desorption-gas chromatography-mass spectrometry method for determining synthetic musks in water samples. J. Chromatogr. A 2011, 1218:156-161.
30. Sanchez-Ortega A., Unceta N., Gómez-Caballero A., Sampedro M.C., Akesolo U., Goicolea M.A., Barrio R.J. Sensitive determination of triazines in underground waters using stir bar sorptive extraction directly coupled to automated thermal desorption and gas chromatography-mass spectrometry. Anal. Chim. Acta 2009, 641:110-116.
31. Arbulu M., Sampedro M.C., Unceta N., Gómez-Caballero A., Goicolea M.A., Barrio R.J. A retention time locked gas chromatography-mass spectrometry method based on stir-bar sorptive extraction and thermal desorption for automated determination of synthetic musk fragrances in natural and wastewaters. J. Chromatogr. A 2011, 1218:3048-3055.
32. Camino-Sánchez F.J., Zafra-Gómez A., Pérez-Trujillo J.P., Conde-González J.E., Marques J.C., Vílchez J.L. Validation of a GC-MS/MS method for simultaneous determination of 86 persistent organic pollutants in marine sediments by pressurized liquid extraction followed by stir bar sorptive extraction. Chemosphere 2011, 84:869-881.
33. Ochiai N., Sasamoto K., Kanda H., Pfannkoch E. Sequential stir bar sorptive extraction for uniform enrichment of trace amounts of organic pollutants in water samples. J. Chromatogr. A 2008, 1200:72-79.
34. Sampedro M.C., Goicolea M.A., Unceta N., Sanchez-Ortega A., Barrio R.J. Sequential stir bar extraction, thermal desorption and retention time locked GC-MS for determination of pesticides in water. J. Sep. Sci. 2009, 32:3449-3456.
35. Cacho J.I., Campillo N., Viñas P., Hernández-Córdoba M. Determination of alkylphenols and phthalate esters in vegetables and migration studies from their packages by means of stir bar sorptive extraction coupled to gas chromatography-mass spectrometry. J. Chromatogr. A 2012, 1241:21-27.
36. Domeño C., Canellas E., Alfaro P., Rodriguez-Lafuente A., Nerin C. Atmospheric pressure gas chromatography with quadrupole time of flight mass spectrometry for simultaneous detection and quantification of polycyclic aromatic hydrocarbons and nitro-polycyclic aromatic hydrocarbons in mosses. J. Chromatogr. A 2012, 1252:146-154.
37. Esteve-Turrillas F.A., Pastor A., de la Guardia M. Comparison of different mass spectrometric detection techniques in the gas chromatographic analysis of pyrethroid insecticide residues in soil after microwave-assisted extraction. Anal. Bioanal. Chem. 2006, 384:801-809.
38. Rodil R., Moeder M. Development of a method for the determination of UV filters in water samples using stir bar sorptive extraction and thermal desorption-gas chromatography-mass spectrometry. J. Chromatogr. A 2008, 1179:81-88.
39. de Sousa F.A., Costa A.I.G., de Queiroz M., Teofilo R.F., Neves A.A., de Pinho G.P. Evaluation of matrix effect on the GC response of eleven pesticides by PCA. Food Chem. 2012, 135:179-185.