Development of a sensitive and selective liquid chromatography-mass spectrometry method for high throughput analysis of paralytic shellfish toxins using graphitised carbon solid phase extraction

Journal of Chromatography A

Volumn 1387, Issue , 2015, Pages 1-12

  Boundy, Michael J ^a   Selwood, Andrew I ^a   Harwood, D Tim ^a   McNabb, Paul S ^a   Turner, Andrew D ^b  

^a CAWTHRON INSTITUTE   (New Zealand)

^b CENTRE FOR ENVIRONMENT   (United Kingdom)

Author keywords

Food safety; Graphitised carbon SPE; HILIC MS MS; Marine biotoxins; Paralytic shellfish toxins; Shellfish

Indexed keywords

CARBON; DESALINATION; FOOD SAFETY; HYDROPHILICITY; LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; PHASE SEPARATION; SHELLFISH; TOXIC MATERIALS; TURNAROUND TIME;

GRAPHITISED CARBON SPE; HIGH-THROUGHPUT ANALYSIS; HILIC-MS/MS; HYDROPHILIC INTERACTION LIQUID CHROMATOGRAPHIES; MARINE BIOTOXINS; PARALYTIC SHELLFISH TOXINS; SELECTIVE LIQUID CHROMATOGRAPHY; SINGLE LABORATORY VALIDATIONS;

EXTRACTION;

ACETIC ACID; ACETONITRILE; CALCIUM; FORMIC ACID; MAGNESIUM; PARALYTIC SHELLFISH TOXIN; POTASSIUM; SHELLFISH TOXIN; SODIUM; UNCLASSIFIED DRUG; CARBON; MARINE TOXIN; SHELLFISH POISONING;

ANALYTICAL PARAMETERS; ARTICLE; CALIBRATION; CHEMICAL PHENOMENA; CONTROLLED STUDY; CRASSOSTREA GIGAS; ELUTION; FLUORESCENCE ANALYSIS; GRAPHITIZED CARBON SOLID PHASE EXTRACTION; HYDROPHILIC INTERACTION LIQUID CHROMATOGRAPHY ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY; INTERMETHOD COMPARISON; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY FLUORESCENCE DETECTION METHOD; MATRIX INTERFERENCE; MONITORING; MULTIPLE REACTION MONITORING; MYTILUS EDULIS; NONHUMAN; PERNA CANALICULUS; PRECIPITATION; PRIORITY JOURNAL; PROCESS OPTIMIZATION; REPRODUCIBILITY; RETENTION TIME; SENSITIVITY AND SELECTIVITY; SOLID PHASE EXTRACTION; SOLVENT EFFECT; STRUCTURE ANALYSIS; TANDEM MASS SPECTROMETRY; TEMPERATURE DEPENDENCE; TOXIN ANALYSIS; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; ANALYSIS; ANIMAL; BIVALVE; CHEMICAL ANALYSIS; CHEMISTRY; DEVICES; FOOD HANDLING; PREVENTION AND CONTROL; PROCEDURES; SHELLFISH;

BIVALVIA;

ANIMALS; BIVALVIA; CARBON; CHEMISTRY TECHNIQUES, ANALYTICAL; CHROMATOGRAPHY, LIQUID; FOOD TECHNOLOGY; LIMIT OF DETECTION; MARINE TOXINS; SHELLFISH; SHELLFISH POISONING; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

EID: 84924577158     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2015.01.086     Document Type: Article

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