Low temperature hydrothermal synthesis and characterization of iron oxide powders of diverse morphologies from spent pickle liquor

Powder Technology

Volumn 276, Issue , 2015, Pages 214-221

  Sinha, Manish K ^a,b   Sahu, Sushanta K ^a   Meshram, Pratima ^a   Prasad, L B ^b   Pandey, Banshi D ^a  

^a NATIONAL METALLURGICAL LABORATORY   (India)

^b BANARAS HINDU UNIVERSITY   (India)

Author keywords

Goethite; Hematite; Hydrothermal synthesis; Magnetic properties; Nano particles; Pickle liquor

Indexed keywords

HEMATITE; IRON OXIDES; MAGNETIC PROPERTIES; MORPHOLOGY; NANOMAGNETICS; NANOPARTICLES; PARTICLE SIZE; RARE EARTH COMPOUNDS; SYNTHESIS (CHEMICAL); TEMPERATURE; TRANSMISSION ELECTRON MICROSCOPY; X RAY POWDER DIFFRACTION;

CHARACTERIZATION STUDIES; GOETHITE; IRON OXIDE NANOPARTICLE; MORPHOLOGY AND STRUCTURES; NANO-CRYSTALLINE STRUCTURES; PICKLE LIQUORS; STRUCTURE AND MORPHOLOGY; SYNTHESIS AND CHARACTERIZATIONS;

HYDROTHERMAL SYNTHESIS;

FERRIC HYDROXIDE; FERRIC OXIDE; ULTRASMALL SUPERPARAMAGNETIC IRON OXIDE;

ARTICLE; CONTROLLED STUDY; CRYSTAL STRUCTURE; FERROMAGNETISM; HYDROTHERMAL SYNTHESIS; HYSTERESIS; LOW TEMPERATURE PROCEDURES; MAGNETISM; MAGNETOMETRY; METAL EXTRACTION; PARTICLE SIZE; PH; POWDER; RAMAN SPECTROMETRY; REACTION TIME; ROOM TEMPERATURE; STRUCTURE ANALYSIS; SYNTHESIS; TRANSMISSION ELECTRON MICROSCOPY; VIBRATIONAL SAMPLE MAGNETOMETRY; X RAY POWDER DIFFRACTION;

EID: 84924405651     PISSN: 00325910     EISSN: 1873328X     Source Type: Journal    
DOI: 10.1016/j.powtec.2015.02.006     Document Type: Article

References (27)

1. 3 elaborated by sol-gel. Electrochim. Acta 2013, 111:869-875.
2. 3 nano-powders by using simple but novel chemical methods. Powder Technol. 2009, 192:245-249.
3. 3 nano-platelets prepared by mechanochemical/thermal processing. Powder Technol. 2011, 210:198-202.
4. 3 superstructures. Powder Technol. 2013, 235:475-478.
5. Cui X., Liu T., Zhang Z., Wang L., Zuo S., Zhu W. Hematite nanorods with tunable porous structure: facile hydrothermal-calcination route synthesis, optical and photocatalytic properties. Powder Technol. 2014, 266:113-119.
6. Guo P., Wei Z., Wang B., Ding Y., Li H., Hang G., Zhao X.S. Controlled synthesis, magnetic and sensing properties of hematite nanorods and microcapsules. Colloids Surf. A Physicochem. Eng. Asp. 2011, 380:234-240.
7. Supattarasakda K., Petcharoen K., Permpool T., Sirivat A., Lerdwijitjarud W. Control of hematite nanoparticle size and shape by the chemical precipitation method. Powder Technol. 2013, 249:353-359.
8. Cornell R.M., Giovanoli R. Effect of solution conditions on the proportion and morphology of goethite formed from ferrihydrite. Clay Miner. 1985, 33:424-432.
9. Tadic M., Čitakovic N., Panjan M., Stojanovic Z., Markovic D., Spasojevic V. Synthesis, morphology, microstructure and magnetic properties of hematite submicron particles. J. Alloys Compd. 2011, 509:7639-7644.
10. 3 microparticles using glycine: surface characterization, reaction mechanism and electrochemical activity. J. Alloys Compd. 2011, 509:9821-9825.
11. 3) superstructure with high coercivity. J. Alloys Compd. 2012, 543:118-124.
12. 3: hydrothermal synthesis, formation mechanism, and magnetic properties. J. Alloys Compd. 2013, 10.1016/j.jallcom.2013.05.215.
13. Riveros P.A., Dutrizac J.E. The precipitation of hematite from ferric chloride media. Hydrometallurgy 1996, 46:85-104.
14. Lu B., Li P., Liu H., Zhao L., Wei Y. Synthesis of hexagonal pyramidal columnar hematite particles by a two-step solution route and their characterization. Powder Technol. 2012, 216:132-136.
15. 3 with various morphologies. J. Alloys Compd. 2013, 555:74-81.
16. 3 uniform nanocrystallines. J. Alloys Compd. 2007, 433:216-220.
17. Konishi Y., Nomura T., Mizoe K. A new synthesis route from spent sulfuric acid pickling solution to ferrite nanoparticles. Hydrometallurgy 2004, 74:57-65.
18. Ciminelli V.S.T., Dias A., Braga H.C. Simultaneous production of impurity-free water and magnetite from steel pickling liquors by microwave-hydrothermal processing. Hydrometallurgy 2006, 84:37-42.
19. Agrawal A., Sahu K.K. Value addition to sulfate waste Pickle liquor of steel industry using hydrometallurgical processes. Metall. and Mater. Trans. 2009, 40B:877-885.
20. Csicsovszki G., Kekesi T., Torok T. Selective recovery of Zn and Fe from spent pickling solutions by the combination of anion exchange and membrane electrowinning techniques. Hydrometallurgy 2005, 77:19-28.
21. Sinha M.K., Sahu S.K., Meshram Pratima, Pandey B.D. Solvent extraction and separation of zinc and iron from spent pickle liquor. Hydrometallurgy 2014, 147-148:103-111.
22. Hanesch M. Raman spectroscopy of iron oxides and (oxy) hydroxides at low laser power and possible applications in environmental magnetic studies. Geophys. J. Int. 2009, 177:941-948.
23. Legodi M.A., De Waal D. The preparation of magnetite, goethite, hematite and maghemite of pigment quality from mill scale iron waste. Dyes Pigments 2007, 74:161-168.
24. 2 precipitates: influence of Fe(II) concentration and stirring speed. J. Phys. Chem. Solids 2008, 69:2124-2130.
25. Wang J., Ren F., Yi R., Yan A., Qui G., Liu X. Solvothermal synthesis and magnetic properties of size-controlled nickel ferrite nanoparticles. J. Alloys Compd. 2009, 479:791-796.
26. 3 hexagonal platelets. Particuology 2010, 8:386-389.
27. Zhang Y.C., Tang J.Y., Hu X.Y. Controllable synthesis and magnetic properties of pure hematite and maghemite nanocrystals from a molecular precursor. J. Alloys Compd. 2008, 462:24-28.