Synthesis, activity and hydrophobicity of Fe-ZSM-5 at silicalite-1 for NH3-SCR

Chemical Engineering Journal

Volumn 262, Issue , 2015, Pages 1199-1207

  Du, Tianyu ^a   Qu, Hongxia ^a   Liu, Qiong ^a   Zhong, Qin ^a   Ma, Weihua ^a  

^a NANJING UNIVERSITY OF SCIENCE AND TECHNOLOGY   (China)

Author keywords

Core shell; Fe ZSM 5; Hydrophobicity; NH3 SCR; Silicalite 1

Indexed keywords

ADSORPTION; HYDROPHOBICITY; SILICATE MINERALS; ZEOLITES;

ADSORPTION OF NO; ADSORPTION PERFORMANCE; CORE-SHELL; FE-ZSM5; FORMATION MECHANISM; HYDROTHERMAL CRYSTALLIZATION; SILICALITE-1; SILICALITE-1 SHELL;

SHELLS (STRUCTURES);

EID: 84909989558     PISSN: 13858947     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cej.2014.09.119     Document Type: Article

References (57)

1. x on Fe-ZSM-5, Cu-chabazite and combined Fe- and Cu-zeolite monolithic catalysts. Chem. Eng. Sci. 2013, 87:51-66.
2. Kim M.S., Lee D.W., Chung S.H., Hong Y.K., Lee S.H., Oh S.H., Cho I.H., Lee K.Y. Oxidation of ammonia to nitrogen over Pt/Fe/ZSM5 catalyst: influence of catalyst support on the low temperature activity. J. Hazard. Mater. 2012, 237-238:153-160.
3. 3. Appl. Catal. B 2010, 95:348-357.
4. Panahi P.N., Salari D., Niaei A., Mousavi S.M. NO reduction over nanostructure M-Cu/ZSM-5 (M: Cr, Mn, Co and Fe) bimetallic catalysts and optimization of catalyst preparation by RSM. J. Ind. Eng. Chem. 2013, 19:1793-1799.
5. Kumara M.S., Schwidder M., Grünert W., Bentrup U., Brückner A. Selective reduction of NO with Fe-ZSM-5 catalysts of low Fe content: Part II. Assessing the function of different Fe sites by spectroscopic in situ studies. J. Catal. 2006, 239:173-186.
6. x catalysts: new insights by a combined EPR and UV/VIS spectroscopic approach. J. Catal. 2004, 227:384-397.
7. 3-SCR performance. J. Catal. 2008, 260:205-216.
8. Brandenberger S., Kröcher O., Tissle A., Althoff R. Estimation of the fractions of different nuclear iron species in uniformly metal-exchanged Fe-ZSM-5 samples based on a Poisson distribution. Appl. Catal. A 2010, 373:168-175.
9. 3 over Fe-ZSM-5. Appl. Catal. B 2007, 74:34-39.
10. Long R.Q., Yang R.T. Characterization of Fe-ZSM-5 catalyst for selective catalytic reduction of nitric oxide by ammonia. J. Catal. 2000, 194:80-90.
11. Fejes P., Kiricsi I., Lázár K., Marsi I., Rockenbauer A., Korecz L., Nagy J.B., Aiello R., Testa F. Attempts to produce uniform Fe(III) siting in various Fe-content ZSM-5 zeolites determination of framework/extra-framework ratio of Fe(III) in zeolites by EPR and Mössbauer spectroscopy. Appl. Catal. A 2003, 242:247-266.
12. Brandenberger S., Kröcher O., Wokaun A., Tissler A., Althoff R. The role of Brønsted acidity in the selective catalytic reduction of NO with ammonia over Fe-ZSM-5. J. Catal. 2009, 268:297-306.
13. x with ammonia. Environ. Sci. Technol. 2010, 44:1799-1805.
14. Sedighi M., Keyvanloo K., Towfighi J. Kinetic study of steam catalytic cracking of naphtha on a Fe/ZSM-5 catalyst. Fuel 2013, 109:432-438.
15. Chen A., Ma X., Sun H. Decolorization of KN-R catalyzed by Fe-containing Y and ZSM-5 zeolites. J. Hazard. Mater. 2008, 156:568-575.
16. 3 on iron zeolite monolithic catalysts: steady-state and transient kinetics. Appl. Catal. B 2011, 104:110-126.
17. 3 over Fe/ZSM-5. Appl. Catal. A 2009, 366:84-92.
18. 2 mixtures. J. Catal. 2008, 259:96-103.
19. Sashkina K.A., Labko V.S., Rudina N.A., Parmon V.N., Parkhomchuk E.V. Hierarchical zeolite FeZSM-5 as a heterogeneous Fenton-type catalyst. J. Catal. 2013, 299:44-52.
20. Gu J., Jin Y.H., Zhou Y., Zhang M.J., Wu Y.J., Wang J. Unseeded organotemplate-free hydrothermal synthesis of heteroatomic MFI zeolite poly-nanocrystallites. J. Mater. Chem. A 2013, 1:2453-2460.
21. 2O activation on iron containing ZSM-5 type zeolites with different elemental composition. Appl. Catal. B 2012, 119-20:329-339.
22. 2O decomposition on iron zeolites by transient response experiments. Catal. Today 2005, 110:199-210.
23. 2O decomposition over Fe/ZSM-5: effect of high-temperature calcination and steaming. Catal. Lett. 2002, 81:205-212.
24. 2O: is every deposited oxygen active?. J. Catal. 2003, 219:273-285.
25. 2O Decomposition. J. Catal. 2000, 196:212-223.
26. 2 core-shell composites. Mater. Chem. Phys. 2012, 133:1144-1151.
27. Okamoto M., Osafune Y. MFI-type zeolite with a core-shell structure with minimal defects synthesized by crystal overgrowth of aluminum-free MFI-type zeolite on aluminum-containing zeolite and its catalytic performance. Microporous Mesoporous Mater. 2011, 143:413-418.
28. Miyamoto M., Kamei T., Nishiyama N., Egashira Y., Ueyama K. Single crystals of ZSM-5/silicalite composites. Adv. Mater. 2005, 17:1985-1988.
29. Weber R.W., Fletcher J.C.Q., Möller K.P., O'Connor C.T. The characterization and elimination of the external acidity of ZSM-5. Microporous Mater. 1996, 7:15-25.
30. Bouizi Y., Rouleau L., Valtchev V.P. Factors controlling the formation of core-shell zeolite-zeolite composites. Chem. Mater. 2006, 18:4959-4966.
31. You Z.Q., Liu G.Z., Wang L., Zhang X.W. Binderless nano-HZSM-5 zeolite coatings prepared through combining washcoating and dry-gel conversion (DGC) methods. Microporous Mesoporous Mater. 2013, 170:235-242.
32. Mores D., Stavitski E., Verkleij S.P., Lombard A., Cabiac A., Rouleau L., Patarin J., Simon-Masseron A., Weckhuysen B.M. Core-shell H-ZSM-5/silicalite-1 composites: Brønsted acidity and catalyst deactivation at the individual particle level. Phys. Chem. Chem. Phys. 2011, 13:15985-15994.
33. Li Q., Wang Z., Hedlund J., Creaser D., Zhang H., Zou X., Bons A. Synthesis and characterization of colloidal zoned MFI crystals. Microporous Mesoporous Mater. 2005, 78:1-10.
34. Ren N., Subotić B., Bronić J., Tang Y., Sikirić M.D., Mišić T., Svetličic V., Bosnar S., Jelic T.A. Unusual pathway of crystallization of zeolite ZSM-5 in a heterogeneous system: phenomenology and starting considerations. Chem. Mater. 2012, 24:17626-17637.
35. Nikolić M.P., Giannakopoulos K.P., Bokorov M., Srdić V.V. Effect of surface functionalization on synthesis of mesoporous silica core/shell particles. Microporous Mesoporous Mater. 2012, 155:8-13.
36. x surface stoichiometry by XPS: a comparison of various methods. Surf. Interface Anal. 1994, 22:89-92.
37. x) thin films. Appl. Surf. Sci. 1993, 222:70-71.
38. McIntyre N.S., Zetaruk D.G. X-ray photoelectron spectroscopic studies of iron oxides. Anal. Chem. 1977, 49:1521-1529.
39. Ciliberto E., Fragala I., Rizza R., Spoto G., Allen G.C. Synthesis of aluminum oxide thin films: use of aluminum tris-dipivaloylmethanate as a new low pressure metal organic chemical vapor deposition precursor. Appl. Phys. Lett. 1995, 67:1624-1626.
40. Mattogno G., Righini G., Montesperelli G., Traversa E. XPS analysis of the interface of ceramic thin films for humidity sensors. Appl. Surf. Sci. 1993, 70:363-366.
41. Andersson S.L.T., Howe R.F. An X-ray photoelectron study of metal clusters in zeolites. J. Phys. Chem. 1989, 93:4913-4920.
42. Tan B.J., Klabunde K.J., Sherwood P.M. A X-ray photoelectron spectroscopy studies of solvated metal atom dispersed catalysts. Monometallic iron and bimetallic iron-cobalt particles on alumina. Chem. Mater. 1990, 2:186-191.
43. 3. J. Catal. 2003, 213:251-271.
44. Qi G.S., Yang R.T. Ultra-active Fe/ZSM-5 catalyst for selective catalytic reduction of nitric oxide with ammonia. Appl. Catal. B 2005, 60:13-22.
45. x. Catal. Today 2006, 114:23-30.
46. Long R.Q., Yang R.T. Temperature-programmed desorption/surface reaction (TPD/TPSR) study of Fe-exchanged zsm-5 for selective catalytic reduction of nitric oxide by ammonia. J. Catal. 2001, 198:20-28.
47. 2 over CoH-ZSM-5. Fuel 2007, 86:1577-1586.
48. x over Fe/ZSM-5 catalysts: adsorption complexes and their reactivity toward hydrocarbons. J. Catal. 1998, 180:171-183.
49. 2 adsorption over Fe/ZSM-5: in situ FT-IR observation and relationships with Fe sites. J. Catal. 2010, 273:29-38.
50. Zecchina A., Bordiga S., Spoto G., Scarano D., Petrini G., Leofanti G., Padovan M., Otero C. Arean, low-temperature Fourier-transform infrared investigation of the interaction of CO with nanosized ZSM5 and silicalite. J. Chem. Soc., Faraday Trans. 1992, 88:2959-2969.
51. 2(a) catalysts. Appl. Surf. Sci. 1996, 99:151-160.
52. y surface species by IR spectroscopy. Catal. Rev. 2000, 42:71-144.
53. 27Al MAS NMR, and EXAFS spectroscopy. J. Catal. 2000, 192:236-247.
54. x adsorption and co-adsorption on Cu/silicalite-1. Phys. Chem. Chem. Phys. 2001, 3:5337-5341.
55. Battiston A.A., Bitter J.H., Koningsberger D.C. XAFS characterization of the binuclear iron complex in overexchanged Fe/ZSM5-structure and reactivity. Catal. Lett. 2000, 66:75-79.
56. Meng Y.T., Genuino H.C., Kuo C.H., Huang H., Chen S.Y., Zhang L.C., Rossi A., Suib S.L. One-step hydrothermal synthesis of manganese-containing MFI-type zeolite, Mn-ZSM-5, characterization, and catalytic oxidation of hydrocarbons. J. Am. Chem. Soc. 2013, 135:8594-8605.
57. Lai P.P., Rees L.V.C. Thermogravimetric studies of ion exchanged forms of zeolites X and Y. J. Chem. Soc., Faraday Trans. 1976, 1(72):1840-1847.