Supercritical carbon dioxide extraction of lithium-ion battery electrolytes

Journal of Supercritical Fluids

Volumn 94, Issue , 2014, Pages 216-222

  Grützke, Martin ^a   Kraft, Vadim ^a   Weber, Waldemar ^a   Wendt, Christian ^a   Friesen, Alex ^a   Klamor, Sebastian ^a   Winter, Martin ^a   Nowak, Sascha ^a  

^a UNIVERSITY OF MÜNSTER   (Germany)

Author keywords

Battery separators; Electrolyte aging; Lithium ion battery electrolyte; Solid electrolyte interphase (SEI); Supercritical fluid extraction (SFE)

Indexed keywords

CARBON DIOXIDE; CARBONATION; CARBOXYLATION; EFFLUENT TREATMENT; GAS CHROMATOGRAPHY; ION CHROMATOGRAPHY; IONIZATION OF GASES; IONS; LITHIUM COMPOUNDS; MASS SPECTROMETRY; SCANNING ELECTRON MICROSCOPY; SEPARATORS; SOLID ELECTROLYTES; SOLID-STATE BATTERIES; SUPERCRITICAL FLUID EXTRACTION; SUPERCRITICAL FLUIDS;

BATTERY SEPARATORS; ELECTROLYTE DEGRADATIONS; LITHIUM IONS; PROOF-OF-PRINCIPLE EXPERIMENTS; SOLID ELECTROLYTE INTERPHASE; STRUCTURE DETERMINATION; SUPERCRITICAL CARBON DIOXIDE EXTRACTION; SUPERCRITICAL FLUID EXTRACTION (SFE); LITHIUM-ION BATTERY; SUPERCRITICAL CARBON DIOXIDES;

LITHIUM-ION BATTERIES; EXTRACTION;

EID: 84907366785     PISSN: 08968446     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.supflu.2014.07.014     Document Type: Article

References (35)

1. M. Winter, and J.O. Besenhard Wiederaufladbare Batterien Chemie unserer Zeit 33 1999 320 332
2. R. Wagner, N. Preschitschek, S. Passerini, J. Leker, and M. Winter Current research trends and prospects among the various materials and designs used in lithium-based batteries Journal of Applied Electrochemistry 43 2013 481 496
3. K.C. Möller, T. Hodal, W.K. Appel, M. Winter, and J.O. Besenhard Fluorinated organic solvents in electrolytes for lithium ion cells Journal of Power Sources 97-98 2001 595 597 (Pubitemid 32631335)
4. K. Tasaki, A. Goldberg, and M. Winter On the difference in cycling behaviors of lithium-ion battery cell between the ethylene carbonate- and propylene carbonate-based electrolytes Electrochimica Acta 56 2011 10424 10435
5. H.J. Santner, C. Korepp, M. Winter, J.O. Besenhard, and K.C. Möller In-situ FTIR investigations on the reduction of vinylene electrolyte additives suitable for use in lithium-ion batteries Analytical and Bioanalytical Chemistry 379 2004 266 271 (Pubitemid 40882952)
6. C. Korepp, H.J. Santner, T. Fujii, M. Ue, J.O. Besenhard, K.C. Möller, and M. Winter 2-Cyanofuran - a novel vinylene electrolyte additive for PC-based electrolytes in lithium-ion batteries Journal of Power Sources 158 2006 578 582 (Pubitemid 43870409)
7. K. Xu Nonaqueous liquid electrolytes for lithium-based rechargeable batteries Chemical Reviews 104 2004 4303 4418
8. M. Winter The solid electrolyte interphase - the most important and the least understood solid electrolyte in rechargeable Li batteries Zeitschrift für Physikalische Chemie 223 2009 1395
9. 6 containing electrolytes Journal of the Electrochemical Society 160 2013 A535 A541
10. 6-based electrolytes for lithium-ion batteries Journal of the Electrochemical Society 152 2005 A2327 A2334
11. L. Gireaud, S. Grugeon, S. Pilard, P. Guenot, J.-M. Tarascon, and S. Laruelle Mass spectrometry investigations on electrolyte degradation products for the development of nanocomposite electrodes in lithium ion batteries Analytical Chemistry 78 2006 3688 3698 (Pubitemid 43853049)
12. G. Gachot, S. Grugeon, M. Armand, S. Pilard, P. Guenot, J.-M. Tarascon, and S. Laruelle Deciphering the multi-step degradation mechanisms of carbonate-based electrolyte in Li batteries Journal of Power Sources 178 2008 409 421
13. G. Gachot, P. Ribière, D. Mathiron, S. Grugeon, M. Armand, J.-B. Leriche, S. Pilard, and S. Laruelle Gas chromatography/mass spectrometry as a suitable tool for the Li-ion battery electrolyte degradation mechanisms study Analytical Chemistry 83 2011 478 485
14. L. Terborg, S. Nowak, S. Passerini, M. Winter, U. Karst, P.R. Haddad, and P.N. Nesterenko Ion chromatographic determination of hydrolysis products of hexafluorophosphate salts in aqueous solution Analytica Chimica Acta 714 2012 121 126
15. L. Terborg, S. Weber, F. Blaske, S. Passerini, M. Winter, U. Karst, and S. Nowak Investigation of thermal aging and hydrolysis mechanisms in commercial lithium ion battery electrolyte Journal of Power Sources 242 2013 832 837
16. B. Vortmann, S. Nowak, and C. Engelhard Rapid characterization of lithium ion battery electrolytes and thermal aging products by low-temperature plasma ambient ionization high-resolution mass spectrometry Analytical Chemistry 85 2013 3433 3438
17. L. Terborg, S. Weber, S. Passerini, M. Winter, U. Karst, and S. Nowak Development of gas chromatographic methods for the analyses of organic carbonate-based electrolytes Journal of Power Sources 245 2014 836 840
18. V. Kraft, M. Grützke, W. Weber, M. Winter, and S. Nowak IC-ESI-MS method development and investigation of lithium hexafluorophosphate-based organic electrolytes and their thermal decomposition products Journal of Chromatography A 1354 2014 92 100
19. K.-H. Chiu, H.-K. Yak, C.M. Wai, and Q. Lang Dry ice-originated supercritical and liquid carbon dioxide extraction of organic pollutants from environmental samples Talanta 65 2005 149 154
20. D.R. Lide CRC Handbook of Chemistry and Physics 85 ed. 2004 CRC Press
21. P.W. Atkins, and J.D. Paula Kurzlehrbuch Physikalische Chemie 2005 Wiley-VCH
22. M. Roth Helium head pressure carbon dioxide in supercritical fluid extraction and chromatography: thermodynamic analysis of the effects of helium Analytical Chemistry 70 1998 2104 2109
23. S. Castillo, F. Ansart, C. Laberty-Robert, and J. Portal Advances in the recovering of spent lithium battery compounds Journal of Power Sources 112 2002 247 254
24. T. Georgi-Maschler, B. Friedrich, R. Weyhe, H. Heegn, and M. Rutz Development of a recycling process for Li-ion batteries Journal of Power Sources 207 2012 173 182
25. M.J. Lain Recycling of lithium ion cells and batteries Journal of Power Sources 97-98 2001 736 738 (Pubitemid 32631363)
26. S.E. Sloop, System and method for removing an electrolyte from an energy storage and/or conversion device using a supercritical fluid, Patent No. US 7,198,865 B2 (2007).
27. T.A. Immel, M. Grützke, A.-K. Späte, U. Groth, P. Öhlschlager, and T. Huhn Synthesis and X-ray structure analysis of a heptacoordinate titanium(IV)-bis-chelate with enhanced in vivo antitumor efficacy Chemical Communications 48 2012 5790 5792
28. U. Heider, R. Oesten, and M. Jungnitz Challenge in manufacturing electrolyte solutions for lithium and lithium ion batteries quality control and minimizing contamination level Journal of Power Sources 81-82 1999 119 122 (Pubitemid 32077793)
29. 6 and stability of PF5 in Li-ion battery electrolytes Journal of the Electrochemical Society 150 2003 A1628 A1636
30. J. Vetter, P. Novák, M.R. Wagner, C. Veit, K.C. Möller, J.O. Besenhard, M. Winter, M. Wohlfahrt-Mehrens, C. Vogler, and A. Hammouche Ageing mechanisms in lithium-ion batteries Journal of Power Sources 147 2005 269 281
31. H. Yoshida, T. Fukunaga, T. Hazama, M. Terasaki, M. Mizutani, and M. Yamachi Degradation mechanism of alkyl carbonate solvents used in lithium-ion cells during initial charging Journal of Power Sources 68 1997 311 315 (Pubitemid 127396151)
32. X. Zhang, P.N. Ross, R. Kostecki, F. Kong, S. Sloop, J.B. Kerr, K. Striebel, E.J. Cairns, and F. McLarnon Diagnostic characterization of high power lithium-ion batteries for use in hybrid electric vehicles Journal of the Electrochemical Society 148 2001 A463 A470
33. T. Sasaki, T. Abe, Y. Iriyama, M. Inaba, and Z. Ogumi Formation mechanism of alkyl dicarbonates in Li-ion cells Journal of Power Sources 150 2005 208 215
34. T. Sasaki, T. Abe, Y. Iriyama, M. Inaba, and Z. Ogumi Effect of an alkyl dicarbonate on Li-ion cell performance Journal of the Electrochemical Society 152 2005 A2046 A2050
35. G. Gachot, S. Grugeon, G.G. Eshetu, D. Mathiron, P. Ribière, M. Armand, and S. Laruelle Thermal behaviour of the lithiated-graphite/electrolyte interface through GC/MS analysis Electrochimica Acta 83 2012 402 409