In situ surface-enhanced raman spectroscopy of the electrochemical reduction of carbon dioxide on silver with 3,5-diamino-1,2,4-triazole

Journal of Physical Chemistry C

Volumn 118, Issue 31, 2014, Pages 17567-17576

  Schmitt, Kevin G ^a   Gewirth, Andrew A ^a  

^a UNIVERSITY OF ILLINOIS AT URBANA CHAMPAIGN   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ADSORPTION; CARBON MONOXIDE; ELECTROLYTIC REDUCTION; HYDROCARBONS; NITROGEN COMPOUNDS; RAMAN SPECTROSCOPY; SILVER; STRETCHING;

ELECTROCHEMICAL REDUCTIONS; HYDROCARBON SPECIES; POTENTIAL-DEPENDENT; SILVER ELECTRODE; STRETCHING VIBRATIONS; SURFACE ENHANCED RAMAN SPECTROSCOPY; SURFACE SITES; VIBRATIONAL SHIFT;

CARBON DIOXIDE;

EID: 84905843000     PISSN: 19327447     EISSN: 19327455     Source Type: Journal    
DOI: 10.1021/jp503598y     Document Type: Article

References (69)

1. 2 Fixation Chem. Rev. 2013, 113, 6621-6658
2. 2 to Liquid Fuels Chem. Soc. Rev. 2009, 38, 89-99
3. Costentin, C.; Robert, M.; Savéant, J. M. Catalysis of the Electrochemical Reduction of Carbon Dioxide Chem. Soc. Rev. 2013, 42, 2423-2436
4. 2 Utilization via Direct Heterogeneous Electrochemical Reduction J. Phys. Chem. Lett. 2010, 1, 3451-3458
5. 2 Reduction on Metal Electrodes. In Modern Aspects of Electrochemistry, Vayenas, C.; White, R.; Gamboa-Aldeco, M., Eds. Springer: New York, 2008; Vol. 42, pp 89-189.
6. 2 Reduction to CO J. Phys. Chem. Lett. 2013, 4, 388-392
7. 2 at Metal Electrodes in Aqueous Media Electrochim. Acta 1994, 39, 1833-1839
8. Surdhar, P. S.; Mezyk, S. P.; Armstrong, D. A. Reduction Potential of the Carboxyl Radical Anion in Aqueous Solutions J. Phys. Chem. 1989, 93, 3360-3363
9. - and the Alcohol Radicals J. Phys. Chem. 1989, 93, 409-414
10. Spichiger-Ulmann, M.; Augustynski, J. Electrochemical Reduction of Bicarbonate Ions at a Bright Palladium Cathode J. Chem. Soc., Faraday Trans. 1 1985, 81, 713-716
11. Podlovchenko, B. I.; Kolyadko, E. A.; Lu, S. G. Electroreduction of Carbon Dioxide on Palladium Electrodes at Potentials Higher than the Reversible Hydrogen Potential J. Electroanal. Chem. 1994, 373, 185-187
12. Kortlever, R.; Tan, K. H.; Kwon, Y.; Koper, M. T. M. Electrochemical Carbon Dioxide and Bicarbonate Reduction on Copper in Weakly Alkaline Media J. Solid State Electrochem. 2013, 17, 1843-1849
13. Stalder, C. J.; Chao, S.; Wrighton, M. S. Electrochemical Reduction of Aqueous Bicarbonate to Formate with High Current Efficiency Near the Thermodynamic Potential at Chemically Derivatized Electrodes J. Am. Chem. Soc. 1984, 106, 3673-3675
14. 2 on Silver as Probed by Surface-Enhanced Raman Scattering J. Raman Spectrosc. 1995, 26, 335-340
15. 2 at an Ag Electrode in KOH-Methanol at Low Temperature Electrochim. Acta 1998, 44, 573-578
16. Oda, I.; Ogasawara, H.; Ito, M. Carbon Monoxide Adsorption on Copper and Silver Electrodes During Carbon Dioxide Electroreduction Studied by Infrared Reflection Absorption Spectroscopy and Surface-Enhanced Raman Spectroscopy Langmuir 1996, 12, 1094-1097
17. 2 at Three-Phase (Gas|Liquid|Solid) and Two-Phase (Liquid|Solid) Interfaces on Ag Electrodes J. Electroanal. Chem. 2002, 533, 113-118
18. McQuillan, A. J.; Hendra, P. J.; Fleischmann, M. Raman Spectroscopic Investigation of Silver Electrodes J. Electroanal. Chem. 1975, 65, 933-944
19. Azuma, M.; Hashimoto, K.; Hiramoto, M.; Watanabe, M.; Sakata, T. Carbon Dioxide Reduction at Low Temperature on Various Metal Electrodes J. Electroanal. Chem. 1989, 260, 441-445
20. 2 to CO J. Electrochem. Soc. 2013, 160, F69-F74
21. Hori, Y.; Ito, H.; Okano, K.; Nagasu, K.; Sato, S. Silver-Coated Ion Exchange Membrane Electrode Applied to Electrochemical Reduction of Carbon Dioxide Electrochim. Acta 2003, 48, 2651-2657
22. Mahoney, M. R.; Howard, M. W.; Cooney, R. P. Raman Spectra of Carbon Monoxide Adsorbed on Silver Electrodes J. Electroanal. Chem. 1984, 161, 163-167
23. Orozco, G.; Pérez, M. C.; Rincón, A.; Gutiérrez, C. Adsorption and Electrooxidation of Carbon Monoxide on Silver Langmuir 1998, 14, 6297-6306
24. Ikezawa, Y.; Saito, H.; Matsubayashi, H.; Toda, G. Comparative Study of CO Adsorbed on Pt, Pd, Au and Ag Electrodes in Neutral Solution by IR Reflection Absorption Spectroscopy J. Electroanal. Chem. 1988, 252, 395-402
25. Furukawa, H.; Takahashi, M.; Ito, M. SERS and FT-IR Studies of CO Adsorbed on Underpotential Deposited Ag/Pt Electrodes J. Electroanal. Chem. 1990, 280, 415-423
26. Gajdoš, M..; Eichler, A.; Hafner, J. CO Adsorption on Close-Packed Transition and Noble Metal Surfaces: Trends from Ab Initio Calculations J. Phys.: Condens. Matter 2004, 16, 1141-1164
27. Su, H. Y.; Yang, M. M.; Bao, X. H.; Li, W. X. The Effect of Water on the CO Oxidation on Ag(111) and Au(111) Surfaces: A First-Principle Study J. Phys. Chem. C 2008, 112, 17303-17310
28. 2 to CO at Low Overpotentials Science 2011, 334, 643-644
29. 2 Mediated with Methylviologen at Roughened Silver Electrodes J. Electroanal. Chem. 2002, 518, 6-12
30. 2 to CO J. Am. Chem. Soc. 2012, 134, 19520-19523
31. Mahoney, M. R.; Howard, M. W.; Cooney, R. P. Carbon Dioxide Conversion to Hydrocarbons at Silver Electrode Surfaces Chem. Phys. Lett. 1980, 71, 59-63
32. Taylor, C. E.; Garvey, S. D.; Pemberton, J. E. Carbon Contamination at Silver Surfaces: Surface Preparation Procedures Evaluated by Raman Spectroscopy and X-ray Photoelectron Spectroscopy Anal. Chem. 1996, 68, 2401-2408
33. Tsang, J. C.; Demuth, J. E.; Sanda, P. N.; Kirtley, J. R. Enhanced Raman Scattering from Carbon Layers on Silver Chem. Phys. Lett. 1980, 76, 54-57
34. Ambrosio, R. C.; Gewirth, A. A. Characterization of Water Structure on Silver Electrode Surfaces by SERS with Two-Dimensional Correlation Spectroscopy Anal. Chem. 2010, 82, 1305-1310
35. Schultz, Z. D.; Feng, Z. V.; Biggin, M. E.; Gewirth, A. A. Vibrational Spectroscopic and Mass Spectrometric Studies of the Interaction of Bis(3-Sulfopropyl)-Disulfide with Cu Surfaces J. Electrochem. Soc. 2006, 153, C97-C107
36. 2 on Single Crystal Electrodes of Silver Ag(111), Ag(100) and Ag(110) J. Electroanal. Chem. 1997, 440, 283-286
37. Jovic, B. M.; Jovic, V. D.; Stafford, G. R. Cyclic Voltammetry on Ag(111) and Ag(100) Faces in Sodium Hydroxide Solutions Electrochem. Commun. 1999, 1, 247-251
38. Savinova, E. R.; Wasle, S.; Doblhofer, K. Structure and Activity Relations in the Hydrogen Peroxide Reduction at Silver Electrodes in Alkaline NaF/NaOH Electrolytes Electrochim. Acta 1998, 44, 1341-1348
39. Savinova, E. R.; Kraft, P.; Pettinger, B.; Doblhofer, K. In Situ Raman Spectroscopy Studies of the Interface Between Silver(111) Electrodes and Alkaline NaF Electrolytes J. Electroanal. Chem. 1997, 430, 47-56
40. Horswell, S. L.; Pinheiro, A. L.; Savinova, E. R.; Danckwerts, M.; Pettinger, B.; Zei, M. S.; Ertl, G. A Comparative Study of Hydroxide Adsorption on the (111), (110), and (100) Faces of Silver with Cyclic Voltammetry, Ex Situ Electron Diffraction, and In Situ Second Harmonic Generation Langmuir 2004, 20, 10970-10981
41. Iwasaki, N.; Sasaki, Y.; Nishina, Y. Ag Electrode Reaction in NaOH Solution Studied by In-Situ Raman Spectroscopy Surf. Sci. 1988, 198, 524-540
42. 2O System J. Solution Chem. 1972, 1, 329-339
43. Kai, S.; Chaozhi, W.; Guangzhi, X. Surface Enhanced Raman Spectra of Carbonate, Hydrocarbonate, and Substituted Acetic Acids on Silver Hydrosols Spectrochim. Acta, Part A 1989, 45, 1029-1032
44. 3 Solution Studied by SERS Surf. Sci. 1988, 198, 541-554
45. Wood, T. H.; Klein, M. V. Raman Scattering from Carbon Monoxide Adsorbed on Evaporated Silver Films J. Vac. Sci. Technol. 1979, 16, 459-461
46. Müslehiddinoǧlu, J.; Vannice, M. A. CO Adsorption on Supported and Promoted Ag Epoxidation Catalysts J. Catal. 2003, 213, 305-320
47. DilLella, D. P.; Gohin, A.; Lipson, R. H.; McBreen, P.; Moskovits, M. Enhanced Raman Spectroscopy of CO Adsorbed on Vapor-Deposited Silver J. Chem. Phys. 1980, 73, 4282-4295
48. Qu, Z. P.; Zhou, S. T.; Wu, W. C.; Li, C.; Bao, X. H. CO Adsorption and Correlation Between CO Surface Coverage and Activity/Selectivity of Preferential CO Oxidation Over Supported Ag Catalyst: An In Situ FTIR Study Catal. Lett. 2005, 101, 21-26
49. Dumas, P.; Tobin, R. G.; Richards, P. L. Study of Adsorption States and Interactions of CO on Evaporated Noble Metal Surfaces by Infrared Absorption Spectroscopy: I. Silver Surf. Sci. 1986, 171, 555-578
50. Blyholder, G. Molecular Orbital View of Chemisorbed Carbon Monoxide J. Phys. Chem. 1964, 68, 2772-2777
51. Fenner, W. R.; Hyatt, H. A.; Kellam, J. M.; Porto, S. P. S. Raman Cross Section of Some Simple Gases J. Opt. Soc. Am. 1973, 63, 73-77
52. Mason, S. E.; Grinberg, I.; Rappe, A. M. First-Principles Extrapolation Method for Accurate CO Adsorption Energies on Metal Surfaces Phys. Rev. B: Condens. Matter Mater. Phys. 2004, 69, 161401
53. Lambert, D. K. Vibrational Stark Effect of Adsorbates at Electrochemical Interfaces Electrochim. Acta 1996, 41, 623-630
54. Zhang, P.; Cai, J.; Chen, Y.-X.; Tang, Z.-Q.; Chen, D.; Yang, J.; Wu, D.-Y.; Ren, B.; Tian, Z.-Q. Potential-Dependent Chemisorption of Carbon Monoxide at a Gold Core-Platinum Shell Nanoparticle Electrode: A Combined Study by Electrochemical in Situ Surface-Enhanced Raman Spectroscopy and Density Functional Theory J. Phys. Chem. C 2010, 114, 403-411
55. Abild-Pedersen, F.; Andersson, M. P. CO Adsorption Energies on Metals with Correction for High Coordination Adsorption Sites-a Density Functional Study Surf. Sci. 2007, 601, 1747-1753
56. Ishi, S.; Ohno, Y.; Viswanathan, B. An Overview on the Electronic and Vibrational Properties of Adsorbed CO Surf. Sci. 1985, 161, 349-372
57. Guennoun, L.; El jastimi, J.; Guédira, F.; Marakchi, K.; Kabbaj, O. K.; El Hajji, A.; Zaydoun, S. Molecular Geometry and Vibrational Studies of 3,5-Diamino-1,2,4-Triazole Using Quantum Chemical Calculations and FT-IR and FT-Raman Spectroscopies Spectrochim. Acta, Part A 2011, 78, 347-353
58. Kumar, V. K.; Keresztury, G.; Sundius, T.; Xavier, R. J. Hydrogen Bonding and Molecular Vibrations of 3,5-Diamino-1,2,4-Triazole Spectrochim. Acta, Part A 2005, 61, 261-267
59. Gabryszewski, M.; Wieczorek, B. Silver(I) Complexes with 1,2,4-Triazole, 1-Ethyl-1,2,4-Triazole, 3-Amino-1,2,4-Triazole, 4-Amino-1,2,4-Triazole and 3,5-Diamino-1,2,4-Triazole Polish J. Chem. 1998, 72, 2352-2355
60. 2 Groups. In The Handbook of Infrared and Raman Characteristic Frequencies of Organic Molecules; Academic Press: San Diego, 1991; Chapter 10, pp 155-178.
61. Pergolese, B.; Muniz-Miranda, M.; Bigotto, A. Study of the Adsorption of 1,2,3-Triazole on Silver and Gold Colloidal Nanoparticles by Means of Surface Enhanced Raman Scattering J. Phys. Chem. B 2004, 108, 5698-5702
62. Wrzosek, B.; Cukras, J.; Bukowska, J. Adsorption of 1,2,4-Triazole on a Silver Electrode: Surface-Enhanced Raman Spectroscopy and Density Functional Theory Studies J. Raman Spectrosc. 2012, 43, 1010-1017
63. Sarkar, J.; Chowdhury, J.; Talapatra, G. B. Adsorption of 4-Methyl-4 H -1,2,4-Triazole-3-Thiol Molecules on Silver Nanocolloids: FT-IR, Raman, and Surface-Enhanced Raman Scattering Study Aided by Density Functional Theory J. Phys. Chem. C 2007, 111, 10049-10061
64. Lin-Vien, D.; Colthup, N. B.; Fateley, W. G.; Grasselli, J. G. Alkanes. In The Handbook of Infrared and Raman Characteristic Frequencies of Organic Molecules; Academic Press: San Diego, 1991; Chapter 2, pp 9-28.
65. Sun, S. C.; Birke, R. L.; Lombardi, J. R. Surface-Enhanced Raman Spectroscopy of Surfactants on Silver Electrodes J. Phys. Chem. 1990, 94, 2005-2010
66. Foucault, R.; Birke, R. L.; Lombardi, J. R. SERS of Surfactants in Monolayer and Multibilayer Forms on an Electrified Ag Surface Langmuir 2003, 19, 8818-8827
67. Brown, R. G. Raman Spectra of Polyethylenes J. Chem. Phys. 1963, 38, 221-225
68. Cooney, R. P.; Mahoney, M. R.; Howard, M. W. Intense Raman Spectra of Surface Carbon and Hydrocarbons on Silver Electrodes Chem. Phys. Lett. 1980, 76, 448-452
69. Kuhl, K. P.; Cave, E. R.; Abram, D. N.; Jaramillo, T. F. New Insights into the Electrochemical Reduction of Carbon Dioxide on Metallic Copper Surfaces Energy Environ. Sci. 2012, 5, 7050-7059