Synthesis of tungsten oxide nanoparticles using a hydrothermal method at ambient pressure

Journal of Materials Research

Volumn 29, Issue 13, 2014, Pages 1424-1430

  Ahmadi, Majid ^a   Younesi, Reza ^b   Guinel, Maxime J F ^a  

^a UNIVERSITY OF PUERTO RICO   (Puerto Rico)

^b TECHNICAL UNIVERSITY OF DENMARK   (Denmark)

Author keywords

electron energy loss spectroscopy; electron microscopy; nanoparticles; tungsten oxide; tungstite; XPS; XRD

Indexed keywords

ELECTRON ENERGY LOSS SPECTROSCOPY; ELECTRON MICROSCOPY; ELECTRON SCATTERING; NANOPARTICLES; NANORODS; OXIDES; PHASE TRANSITIONS; TRANSMISSION ELECTRON MICROSCOPY; TUNGSTEN COMPOUNDS; X RAY DIFFRACTION; X RAY PHOTOELECTRON SPECTROSCOPY; DISSOCIATION; ELECTRON ENERGY LEVELS; ELECTRONS; HYDROTHERMAL SYNTHESIS; NANOSTRUCTURES; OXALIC ACID; SYNTHESIS (CHEMICAL); TUNGSTEN;

LARGE SCALE PRODUCTIONS; NANOPARTICLES MORPHOLOGY; ORTHORHOMBIC STRUCTURES; POWDER X RAY DIFFRACTION; SODIUM TUNGSTATE SOLUTIONS; TUNGSTEN OXIDE; TUNGSTITE; XRD;

SYNTHESIS (CHEMICAL); ELECTRON ENERGY LOSS SPECTROSCOPY;

EID: 84905082750     PISSN: 08842914     EISSN: 20445326     Source Type: Journal    
DOI: 10.1557/jmr.2014.155     Document Type: Article

References (46)

1. N. Soultanidis, W. Zhou, C.J. Kiely, and M.S. Wong: Solvothermal synthesis of ultrasmall tungsten oxide nanoparticles. Langmuir 28, 17771 (2012
2. 3 films: Synthesis, characterization, and applications. J. Am. Chem. Soc. 123, 10639 (2001
3. 3. Langmuir 26, 19148 (2010
4. V. Wood, M.J. Panzer, J.E. Halpert, J.M. Caruge, M.G. Bawendi, and V. Bulovic: Selection of metal oxide charge transport layers for colloidal quantum dot LEDs. ACS Nano 3, 3581 (2009
5. 3 based thinfilm for visible-light induced oxidation and superhydrophilicity. J. Phys. Chem. C 116, 15421 (2012
6. 3 film electrodes. J. Phys. Chem. C 117, 7005 (2013
7. X. Chen, J. Ye, S. Ouyang, T. Kako, Z. Li, and Z. Zou: Enhanced incident photon-to-electron conversion efficiency of tungsten trioxide photoanodes based on 3D-photonic crystal design. ACS Nano 5, 4310 (2011
8. M.G. Walter, E.L. Warren, J.R. McKone, S.W. Boettcher, Q. Mi, E.A. Santori, and N.S. Lewis: Solar water splitting cells. Chem. Rev. 110, 6446 (2010
9. K. Maeda, M. Higashi, D. Lu, R. Abe, and K. Domen: Efficient nonsacrificial water splitting through two-step photoexcitation by visible light using a modified oxynitride as a hydrogen evolution photocatalyst. J. Am. Chem. Soc. 132, 5858 (2010
10. M. Higashi, R. Abe, A. Ishikawa, T. Takata, B. Ohtani, and K. Domen: Z-scheme overall water splitting on modified-TaON photocatalysts under visible light (k,500 nm). Chem. Lett. 37, 138 (2008
11. M.R.Waller, T.K. Townsend, J. Zhao, E.M. Sabio, R.L. Chamousis, N.D. Browning, and F.E. Osterloh: Single-crystal tungsten oxide nanosheets: Photochemical water oxidation in the quantum confinement regime. Chem. Mater. 24, 698 (2012
12. 3/Si tandem photoelectrodes. J. Phys. Chem. C 117, 6949 (2013
13. 3/BiVO4 heterojunction films for efficient photoelectrochemical water splitting. Nano Lett. 11, 1928 (2011
14. 3 as a carbon-free electrocatalyst with enhanced electrochemical activity for methanol oxidation. J. Phys. Chem. B 112, 12024 (2008
15. 3/W photoanode and Cu2O/Cu photocathode for simultaneous wastewater treatment and electricity generation. Environ. Sci. Technol. 46, 11451 (2012
16. 3.H2O: Visible-light photocatalyst for bacteria destruction. Inorg. Chem. 48, 10697 (2009
17. 2 into hydrocarbon fuels under visible light. ACS Appl. Mater. Interfaces 4, 3372 (2012
18. J. Yin, H. Cao, J. Zhang, M. Qu, and Z. Zhou: Synthesis and applications of c-tungsten oxide hierarchical nanostructures. Cryst. Growth Des. 13, 759 (2013
19. 2 gasochromic films doped with Pd catalyst. ACS Appl. Mater. Interfaces 3, 4573 (2011
20. 3 nanorods with their enhanced properties for photocatalysis and gas sensing. J. Phys. Chem. C 114, 2049 (2010
21. 3 for sensing of acetone in the human breath. Chem. Mater. 22, 3152 (2010
22. G. Gu, B. Zheng, W.Q. Han, S. Roth, and J. Liu: Tungsten oxide nanowires on tungsten substrates. Nano Lett. 2, 849 (2002
23. 2.72. J. Mater. Chem. 13, 445 (2003
24. J. Polleux, A. Gurlo, N. Barsan, U. Weimar, M. Antonietti, and M. Niederberger: Template-free synthesis and assembly of singlecrystalline tungsten oxide nanowires and their gas-sensing properties. Angew. Chem., Int. Ed. 45, 261 (2005
25. J. Polleux, N. Pinna, M. Antonietti, and M. Niederberger: Growth and assembly of crystalline tungsten oxide nanostructures assisted by bioligation. J. Am. Chem. Soc. 127, 15595 (2005
26. C. Klinke, J.B. Hannon, L. Gignac, K. Reuter, and P. Avouris: Tungsten oxide nanowire growth by chemically induced strain. J. Phys. Chem. B 109, 17787 (2005
27. 2. Chem. Commun. 3, 269-270 (1999
28. 3 nanorods/nanowires into hierarchical nanostructures. J. Phys. Chem. B 110, 23829 (2006
29. 3 nanotrees for super-hydrophilic thin films. Adv. Mater. 21, 1373 (2009
30. S. Supothina, P. Seeharaj, S. Yoriya, and M. Sriyudthsak: Synthesis of tungsten oxide nanoparticles by acid precipitation method. Ceram. Int. 33, 931 (2007
31. M. Sun, N. Xu, Y.W. Cao, J.N. Yao, and E.G. Wang: Nanocrystalline tungsten oxide thin film: Preparation, microstructure, and photochromic behavior. J. Mater. Res. 15, 927 (2000
32. 3) nanoleaves, nanoparticles and nanoflakes. Microsc. Microanal. 19(S2), 1580 (2013
33. 3.H2O) nanoleaves and nanoribbons. Acta Mater. 69, 203 (2014
34. 3.H2O. Can. Minerol. 22, 681 (1984
35. 3. Acta Cryst. 21, 158 (1966
36. A.F. Holleman, E. Wiberg, and N. Wiberg: Inorganic Chemistry (Academic Press, Berlin, New York, Walter De Gruyter, San Diego, 2001); p. 1389.
37. C. Balazsi and J. Pfeifer: Structure and morphology changes caused by wash treatment of tungstic acid precipitates. Solid State Ionics 124, 73 (1999
38. 2 production and Fe (III) ion reduction under visible light. J. Phys. Chem. Lett. 1, 1196 (2010
39. 3). J. Mater. Sci. 49(17), 5899 (2014
40. 3 powder. J. Phys. Chem. C 111, 1213 (2007
41. C.C. Ahn and O.L. Krivanek: EELS Atlas: A Reference Guide of Electron Energy Loss Spectra Covering All Stable Elements (ASU HREM Facility & GatanInc, Warrendale, PA, 1983
42. 3, x 5 0 to 0.33. J. Solid State Chem. 178, 1008 (2005
43. C.C. Ahn and P. Rez: Inner shell edge profiles in electron energy loss spectroscopy. Ultramicroscopy 17, 105 (1985
44. F. Jollet, T. Petit, S. Gota, N. Thromat, M. Soyer Gautier, and A. Pasturel: The electronic structure of uranium dioxide: An oxygen K-edge x-ray absorption study. J. Phys.: Condens. Matter 9, 9393 (1997
45. A. Harvey, B. Guo, I. Kennedy, S. Risbud, and V. Leppert: A systematic study of the oxygen K edge in the cubic and less commonmonoclinic phases of the rare earth oxides (Ho, Er, Tm, Yb) by electon energy loss spectroscopy. J. Phys.: Condens. Matter 18, 2181 (2006
46. D.W. McComb: Bonding and electronic structure in zirconia pseudopolymorphs investigated by electron energy-loss spectroscopy. Phys. Rev. B 54, 7094 (1996).