Preparation and processing of micro- and nano-scale materials by supercritical fluid technology

Supercritical Fluid Extraction of Nutraceuticals and Bioactive Compounds

Volumn , Issue , 2007, Pages 367-389

  Weidner, Eckhard ^a   Petermann, Marcus ^a  

^a RUHR UNIVERSITY BOCHUM   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84897676346     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1201/9781420006513     Document Type: Chapter

References (98)

1. Reverchon, E., Micro- and nano-particles produced by supercritical fluids assisted techniques: Present status and perspectives, Chem. Eng. Trans., 2, 1, 2002.
2. Jung, J. and Perrut, M., Particle design using supercritical fluids: Literature and patent survey, J. Supercrit. Fluids, 20, 179, 2001.
3. Knez, Z. and Weidner, E., Precipitation of solids with dense gases, in High Pressure Process Technology: Fundamentals and Application, Bertucco, A. and Vetter, G., Eds., Elsevier, 2002.
4. Weidner, E., Powderous composites by high pressure spray processes, in Proceedings of the Sixth International Symposium on Supercritical Fluids, Versailles, France, 2003, 3, 1483.
5. Gamse, T., Schwinghammer, S. and Marr, R., Erzeugung feinster partikel durch einsatz von überkritischen fluiden, Chem. Ing. Techn., 77, 669, 2005.
6. Türk, M. et al., Stabilization of pharmaceutical substances by the rapid expansion of supercritical solutions (RESS), in Proceedings of the Sixth International Symposium on Supercritical Fluids, Versailles, France, 2003, 3, 1747.
7. Reverchon, E., Supercritical-assisted atomization to produce micro- and/or nanoparticles of controlled size and distribution, Ind. Eng. Chem. Res., 41, 2405, 2002.
8. Reverchon, E. and Della Porta, G., Micronization of antibiotics by supercritical assisted atomization, J. Supercrit. Fluids, 26, 243, 2003.
9. Shariati, A. and Peters, C.J., Measurements and modeling of the phase behavior of ternary systems of interest for the GAS process: I. The system carbon dioxide+1- propanol+salicylic acid, J. Supercrit. Fluids, 23, 195, 2002.
10. Yeo, S., Kim, M. and Lee, J., Recrystallisation of sulfathiazole and chlorpropamide using the supercritical antisolvent process, J. Supercrit. Fluids, 25, 143, 2003.
11. Ventosa, N., Sala, S. and Veciana, J., DELOS process: A crystallisation technique using compressed fluids: 1. Comparison to the GAS crystallization methode, J. Supercrit. Fluids, 26, 33, 2003.
12. Sun, X. et al., The characteristics of coherent structures in the rapid expansion flow of the supercritical carbon dioxide, J. Supercrit. Fluids, 24, 231, 2002.
13. Hanna, M. and York, P., Patent WO 95/01221, 1994.
14. Weidner, E. et al., Manufacture of particles from high viscous melts using supercritical fluids, reviewed. Proc. “High Pressure in Venice”, ISBN 88-900775-1-4, 2, 735, 2002.
15. Peter, S. et al., Interfacial tension in binary systems containing a dense gas, in Supercritical Fluids: Fundamentals for Application, Kiran, E. and Levelt-Sengers, J.M.H., Eds., Boston, Kluwer Academic Publishers, 731, 1994. Proceedings of the NATO Advanced Study Institute on Supercritical Fluid-Fundamentals for Application, Kemer, Antalya, Turkey, July 18-31, 1993; NATO Dordrecht, Kluwer NATO ASI Series: Series E, 273.
16. Jakob, H., Peter, S. and Weidner, E., Die Viskositaet koexistierender Phasen bei der ueberkritischen Fluidextraktion, Chem. Ing. Techn., 59, 37, 1987.
17. Jaeger, P., Eggers, R. and Baumgartl, H., Interfacial properties of high viscous liquids in a supercritical carbon dioxide atmosphere, J. Supercrit. Fluids, 24, 203, 2002.
18. Gulari, E. et al., Rheology of molten polystyrene with dissolved supercritical and nearcritical gases, J. Polym. Sci., 37, 2771, 1999.
19. De Simone, J.M. et al., Viscosity effects on the thermal decomposition of bis(perfluoro-2N-propoxypropionyl) peroxide in dense carbon dioxide and fluorinated solvents, J. Am. Chem. Soc., 123, 30, 7199, 2001.
20. Petermann, M., Herstellung von Pulverlacken durch Verspruehung gashaltiger Schmelzen, Ph.D. Thesis, Erlangen, 1999.
21. Kayrak, D., Akman, U. and Hortacsu, Ö., Micronization of Ibuprofen by RESS, J. Supercrit. Fluids, 26, 17, 2003.
22. Kappler, P. et al., Size and morphology of particles generated by spraying polymer- melts with carbon dioxide, in Proceedings of the Sixth International Symposiumon Supercritical Fluids, Versailles, France, 2003, 1891.
23. Sievers, R.E. et al., Micronization of water-soluble or alcohol-soluble pharmaceuticals and model compounds with a low-temperature bubble dryer, J. Supercrit. Fluids, 26, 9, 2003.
24. Grüner, S., Otto, F. and Weinreich, B., CPF-technology: A new cryogenic spraying process for pulverization of liquid, in Proceedings of the Sixth International Symposium on Supercritical Fluids, Versailles, France, 2003, 1935.
25. Reverchon, E. et al., Pilot scale micronization of amoxicillin by supercritical antisolvent precipitation, J. Supercrit. Fluids, 26, 1, 2003.
26. Best, W. et al., German Patent 2 943 267, BASF AG, 1979.
27. Subramaniam, B. et al., Patent WO 97/31691.
28. Krause, H., Niehaus, M. and Teipel, U., German Patent DE 19711393, 1998.
29. Türk, M., Erzeugung von organischen Nanopartikeln mit ueberkritischen Fluiden, Habilitationsschrift, University Karlsruhe, 2001.
30. Türk, M. et al., Micronization of pharmaceutical substances by rapid expansion of supercritical solutions (RESS): Experiments and modelling, Part. Syst. Charact., 19, 327, 2002.
31. Reverchon, E. and Donsi, G., Salycylic acid solubilization in supercritical CO2 and its micronisation by RESS, J. Supercrit. Fluids, 6, 241, 1993.
32. Türk, M. et al., Micronisation of pharmaceutical substances by rapid expansion of supercritical solutions (RESS): A promising method to improve the bioavailability of poorly soluble pharmaceutical agents, J. Supercrit. Fluids, 22, 75, 2002.
33. Helfgen, B., Türk, M. and Schaber, K., Hydrodynamic and aerosol modelling of the rapid expansion of supercritical solutions (RESS), J. Supercrit. Fluids, 26, 225, 2003.
34. Diefenbacher, A. and Türk, M., Phase equilibria of organic solid solutes and supercritical fluids with respect to the RESS process, J. Supercrit. Fluids, 22, 175, 2002.
35. Orlovic, A. and Skala, D., Materials processing, using supercritical fluids, Hem. Ind., 59, 213, 2005.
36. Sun, Y.P. et al., Polymeric nanoparticles from rapid expansion of supercritical fluid solution, Chem. Eur. J., 11, 1366, 2005.
37. Moribe, K., Micronisation of phenylbutazone by rapid expansion of supercritical CO2 solution, Chem. Pharm. Bull., 53, 1025, 2005.
38. Türk, M. et al., Micronization of pharmaceutical substances by the rapid expansion of supercritical solutions (RESS): A promising method to improve bioavailability of poorly soluble pharmaceutical agents, J. Supercrit. Fluids, 22, 75, 2002.
39. Sane, A. and Thies, M.C., The formation of fluorinated tetraphenylporphyrin nanoparticles via rapid expansion process: RESS vs RESOLV, J. Phys. Chem. B, 109, 19688, 2005.
40. Türk, M., Herstellung organischer nanopartikeln und deren stabilisierung in wässrigen lösungen (RESSAS), Chem. Ing. Tech., 75, 792, 2003.
41. Türk, M. and Wahl, M., Utilization of supercritical fluid technology for the preparation of innovative carriers loaded with nanoparticular drugs, 2004 International Congress for Particle Technology (PARTEC). Ed. S.E. Pratsinis, Nueremberg, 2004.
42. Türk, M., Untersuchungen zum Coating von submikronen Partikeln mit dem CORESSVerfahren, Chem. Ing. Techn., 76, 3, 2004.
43. Thakur, R. and Gupta, R.B., Formation of phenytoin nanoparticles using rapid expansion of supercritical solution with solid cosolvent (RESS-SC) process, Int. J. Pharm., 308, 190, 2006.
44. Tümmel, R., Weiß, C. and Bertling, J., Smart materials: New ways to microstructured particles of environmental concern, Adv. Environ. Mat., II, 175, 2001.
45. Weber, A. and Kümmel, R., Nanoparticles by precipitation in supercritical fluids - possibilities and limitations, in Proceedings of the Seventh Meeting on Supercritical Fluids, Antibes, France, 2001, 49.
46. Weber, A. et al., A production plant for gas antisolvent crystallization, in Proceedings of the Fifth Meeting on Supercritical Fluids, Nice, France, 1998, 281.
47. Weber, A., Tschernjaew, J. and Kümmel, R., Coprecipitation with compressed antisolvents for the manufacture of microcomposites, in Proceedings of the Fifth Meeting on Supercritical Fluids, 1999, 243.
48. Krause, H., Niehaus, M. and Teipel, U., German Patent 19711393, 1998.
49. Yeo, S. et al., Supercritical anti-solvent process for a series of substituted para-linked aromatic polyamides: phase equilibria and morphology, Macromolecules, 26, 6207, 1993.
50. Berends, E.M. et al., Crystallization of phenanthrene from toluene with carbon dioxide by the GAS process, AIChE J., 42, 431, 1996.
51. Perez de Diego, Y. et al., Opening new operating windows for polymer and protein micronisation using the PCA process, J. Supercrit. Fluids, 36, 216, 2006.
52. Thiering, R., Dehghani, F. and Foster, N.R., Current issues relating to anti-solvent micronisation techniques and their extension to industrial scales, J. Supercrit. Fluids, 21, 159, 2001.
53. Weiß, C. et al., Modeling mass transfer and crystallization in disperse systems, Chem. Eng. Technol., 23, 485, 2000.
54. Weidner, E., Powder generation by high pressure spray processes, in Proceedings of the International Meeting on High Pressure Chemmical Engineering, Karlsruhe, Wissenschaftliche Berichte FZKA 6271, 1999, 217.
55. Knez, Z., Micronisation of pharmaceuticals using supercritical fluids, in Proceedings of the Seventh Meeting on Supercritical Fluids, Antibes, France, 1, 21, 2000.
56. Weidner, E., Petermann, M. and Blatter, K., Die herstellung von pulverlacken durch versprühen gashaltiger schmelzen, Chem. Ing. Techn., 72, 743, 2000.
57. Münüklü, P., Particle Formation of Ductile Materials using the PGSS Technology with Supercritical Carbon Dioxide, Ph.D. Thesis, University Delft, Netherlands, 2005.
58. Weidner, E., Petermann, M. and Knez, Z., Multifunctional composites by high pressure spray processes, in Current Opinion in Solid State and Material Science, Netherlands, Elsevier, 385, 2004.
59. Weidner, E., Powderous composites by high pressure spray processes, in Proceedings of the Sixth International Symposium on Supercritical Fluids, Versailles, France, 1483, 2003.
60. Rantakylä, M., Particle Production by Supercritical Antisolvent Processing Techniques, PhD Thesis, Helsinki University of Technology, Helsinki, 2004.
61. Weber, A. et al., A production plant for gas antisolvent crystallization, in Proceedings of the Fifth Meeting on Supercritical Fluids, Nice, France, 1998, 3, 281.
62. Tuerk, M., Erzeugung von organischen Nanopartikeln mit überkritischen Fluiden, Habilitationsschrift, Karlsruhe, 2001.
63. Grüner, S., Entwicklung eines Hochdrucksprühverfahrens zur Herstellung hochkonzentrierter, flüssigkeitsbeladener Pulver, Ph.D. Thesis, University Erlangen, Germany, 1999.
64. Grüner, S. et al., CPF-Process for powder generation from liquids, in Proceedings of the Fifth Conference on Supercritical Fluids and Their Applications, Garda, Italy, 1999, 471.
65. Grüner, S. and Otto, F., Adalbert Raps Forschungszentrum, Unpublished Data, Weihenstephan, 2005.
66. Brandin, G. et al., Tailor-made composites by high pressure spray processes, in Proceedings of the Fifth World Congress on Particle Technology, Orlando, FL, 2006.
67. Weidner, E. et al., Fluid-filled micro particles using PGSS technology, in Proceedings of the Third International Meeting on High Pressure Chemical Engineering, Erlangen, Germany, 2006.
68. Brandin, G., Herstellung pulverförmiger Komposite mittels Hochdrucksprühverfahren, Ph.D. Thesis, Ruhr-University, Bochum, 2005.
69. Brandin, G. et al., Fluid-filled micro particles by the use of the PGSS technology, Advanced Powder Technology, accepted for publication, 2006.
70. Weidner, E. et al., Production of powdery phase change materials using the PGSS process, J. Supercrit. Fluids, not yet published, 2006.
71. Weidner, E. et al., Manufacture of particles from high viscous melts using supercritical fluids, rev. Proc. “High Pressure in Venice”, ISBN 88-900775-1-4, 2, 735, 2002.
72. Petermann, M. et al., Micronization of polymer solutions by PGSS-drying, in Proceedings of the Eighth Conference on Supercritical Fluids and Their Applications, Ischia, Italy, 2006.
73. Weidner, E., Final report: Product engineering with neutraceuticals with superior quality, PRONUTRA, EU-Project, GRD1-1999-10212, 2003.
74. Meterc, D. et al., Extraction of natural substances and drying with PGSS process, Slovenian Chemical Days 2006, Maribor, 2006.
75. Meterc, D., Ph.D Thesis, Ruhr-University Bochum, in preparation.
76. Reverchon, E., Della Porta, G. and Falivene, M.G., Process parameters controlling the supercritical anti-solvent micronization of some antibiotics, in Proceedings of the Sixth Meeting on Supercritical Fluids, Chemistry and Materials, Nottingham, UK, 1999.
77. Chroenchaitrakool, M. et al., Micronization by RESS to enhance the dissolution rates of poorly water soluble pharmaceuticals, in Proceedings of the Fifth International Symposium on Supercritical Fluids, Atlanta, GA, 2000.
78. Foster, N.R. et al., Application of dense gas techniques for the production of fine particles, AAPS PharmSci, 5, 2, 105-111, 2003.
79. Manning, M.C. et al., U.S. Patent 5 770 559, 1998.
80. Martin, H.-J. et al., Nanoscale particles for pharmaceutical purpose by rapid expansion of supercritical solutions (RESS). Part II: Characterization of the product and use, in Proceedings of the Seventh Meeting on Supercritical Fluids, Antibes, France, 2000, 1, 53.
81. Frank, S.G. and Ye, C., Small particle formation and dissolution rate enhancement of relatively insoluble drugs using rapid expansion of supercritical solutions (RESS) processing, in Proceedings of the Fifth International Symposium on Supercritical Fluids (CD-ROM), 2000.
82. Foster, N.R. et al., Processing pharmaceuticals using dense gas technology, Proceedings of the Fifth International Symposium on Supercritical Fluids (CD-ROM), 2000.
83. Warwick, B. et al., Micronization of copper-indomethacin using gas anti-solvent processes, Ind. Eng. Chem. Res., 41, 8, 1993-2004, 2002.
84. Thiering, R., Dehghani, F. and Foster, N.R., Micronization of model proteins using compressed carbon dioxide, in Proceedings of the Fifth International Symposium on Supercritical Fluids, Atlanta, 2000.
85. Thiering, R. et al., The influence of operating conditions on the dense gas precipitation of model proteins, J. Chem. Technol. Biotechnol., 75, 29-41, 2000.
86. Thiering, R. et al., Solvent effects on the controlled dense gas precipitation of model proteins, J. Chem. Technol. Biotechnol., 75, 42-53, 2000.
87. Cocero, M.J., Ferrero, S. and Vicente, S., GAS crystallization of β-carotene from ethyl acetate solutions using CO2 as antisolvent, in Proceedings of the Fifth International Symposium on Supercritical Fluids, Atlanta, 2000.
88. Reverchon, E. et al., in Proceedings of the Sixth Conference on Supercritical Fluids and Their Applications, Maiori, Italy, 2001, 301.
89. Subra, P. and Vega, A., in Proceedings of the 15th International Congress on Chemical and Process Engineering, CHISA 2002, Prague, Czech Republic, 2002.
90. Pellikaan, H.C. and Wubbolts, F.E., Nozzel construction for particle formation using supercritical antisolvent precipitation, in Proceedings of the Sixth International Symposium on Supercritical Fluids, Versailles, France, 2003, 1765.
91. Reverchon, E. et al., Supercritical fluid antisolvent micronisation of some biopolymers, J. Supercrit. Fluids, 18, 239, 2000.
92. Jung, J., Clavier, J.Y. and Perrut, M., Gram to kilogram scale-up of supercritical antisolvent process, in Proceedings of the Sixth International Symposium on Supercritical Fluids, Versailles, France, 2003, 1683.
93. Magnan, C. et al., Soy lectin micronisation with a compressed fluid antisolvent- influenceof process parameters, J. Supercrit. Fluids, 19, 69, 2000.
94. Nagahama, K. and Kamoshita, C., in Proceedings of the Fourth International Symposiom on High Pressure Process Technology and Chemical Engineering, Venice, Italy, 2002.
95. Sloan, R. et al., Supercritical fluid processing: Preparation of stable protein particles, in Proceedings of the Fifth Meeting on Supercritical Fluids, Nice, France, 1998, 1, 301.
96. Reverchon, E., Supercritical anti-solvent precipitation: Its application to microparticle generation and products fractionation, in Proceedings of the Fifth Meeting on Supercritical Fluids, Nice, France, 1998, 1, 221.
97. Petermann, M. et al., CPF-Concentrated powder form-A high pressure spray agglomeration technique, in Proceedings of Spray Drying 01 Conference, Dortmund, Germany, 2001, 143.
98. Wehowski, M. and Weidner, E., Water-containing agglomerates by high pressure spraying according to the concentrated powder form (CPF) process, CIT, 77, 3, 274-278, 2005.