Isolation of (-)-patchouli alcohol from patchouli oil by fractional distillation and crystallization

Tropical Journal of Pharmaceutical Research

Volumn 13, Issue 3, 2014, Pages 359-363

  Su, Zu Qing ^a   Wu, Xiao Li ^a   Bao, Mei Jia ^b   Li, Chu Wen ^a   Kong, Song Zhi ^a   Su, Zi Ren ^a   Lai, Xiao Ping ^a   Li, Yu Cui ^a   Chen, Jian Nan ^a  

^a GUANGZHOU UNIVERSITY OF CHINESE MEDICINE   (China)

^b Guangzhou Pharmaceutical Vocational School   (China)

Author keywords

Crystallization; Fractional distillation; Isolation; Patchouli alcohol; Patchouli oil

Indexed keywords

ESSENTIAL OIL; PATCHOULI ALCOHOL; PATCHOULI OIL; SESQUITERPENE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CENTRIFUGATION; CHEMICAL COMPOSITION; CHEMICAL STRUCTURE; COOLING; CRYSTALLIZATION; DISTILLATION; FEASIBILITY STUDY; FILTRATION; FRACTIONAL DISTILLATION; FREEZING; INFRARED SPECTROSCOPY; ISOLATION AND PURIFICATION; ISOLATION PROCEDURE; MASS FRAGMENTOGRAPHY; MELTING POINT; PROTON NUCLEAR MAGNETIC RESONANCE; VACUUM;

EID: 84897567243     PISSN: 15965996     EISSN: 15969827     Source Type: Journal    
DOI: 10.4314/tjpr.v13i3.7     Document Type: Article

References (8)

1. Bhatia SP, Letizia CS, Api AM. Fragrance material review on patchouli alcohol, Food Chem Toxicol 2008; 46(11): S255-S256.
2. Liu ZH, Zhou DY. Chemical component comparison of essential oil extracted from Pogostemon cablin by supercritical CO2 extraction and stream distillation. J Anhui Agr Sci 2009; 37(19): 8816-8817.
3. Hu HY, Peng JF, Huang SL, Wu LH, Zhu BZ, Xuan YM, Yang DP. Study on purification technology of patchoul oil with molecular distillation. Chin J Chin Mater Med 2004; 29(4): 320-322.
4. Chen H, Zhang JW, Zhu HW, Song ZL. Purification of patchouli alcohol in volatile oil of Pogostemon cablin by molecular distillation. Chin Tradit Herbal Drugs 2009; 40(1): 60-63.
5. Guan L, Quan LH, Xu LZ, Cong PZ. Study on Chemical Constituents of Pogostemon cablin. Chin J Chin Mater Med 1994; 19(6): 355-356.
6. Jian T, Lei Y, Fang G, Wang ZH, Jin L, Guo WS. Selective separation of patchouli alcohol from the essential oil of Cablin potchouli by inclusion crystalline method. Nat Prod Res 2013; 27(1): 32-36.
7. Stefan Berger, Dieter Sicker editors. Classics in Spectroscopy: Isolation and Structure Elucidation of Natural Products. New York: 2009, Wiley-VCH; p. 359-481.
8. The State Pharmacopoeia Commission of the P. R. China, Pharmacopoeia of the People's Republic of China (Vol.1), Beijing: 2010, Chemical Industry Press; pp 42-373.