Quantification of free sialic acid in human plasma through a robust quinoxalinone derivatization and LC-MS/MS using isotope-labeled standard calibration

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 944, Issue , 2014, Pages 75-81

  Wang, Dan ^a   Zhou, Xiang ^a   Wang, Lin ^b   Wang, Sihe ^c   Sun, Xue Long ^a  

^a CLEVELAND STATE UNIVERSITY   (United States)

^b CHINA MEDICAL UNIVERSITY   (China)

^c LERNER RESEARCH INSTITUTE   (United States)

Author keywords

Free sialic acid; Human plasma; Isotope labeled standard calibration; Liquid chromatography tandem mass spectrometry; Quinoxaline derivatization

Indexed keywords

CALIBRATION; CARBOXYLIC ACIDS; CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOTOPES; MASS SPECTROMETRY;

DERIVATIZATIONS; HUMAN PLASMAS; ISOTOPE-LABELED STANDARD; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; SIALIC ACIDS;

PLASMA (HUMAN);

QUINOXALINE DERIVATIVE; QUINOXALINONE DERIVATIVE; SIALIC ACID; STABLE ISOTOPE; UNCLASSIFIED DRUG;

ARTICLE; COST EFFECTIVENESS ANALYSIS; DERIVATIZATION; ELECTROSPRAY; HUMAN; ISOTOPE LABELED STANDARD CALIBRATION; ISOTOPE LABELING; LIMIT OF QUANTITATION; PLASMA; PRIORITY JOURNAL; QUALITY CONTROL; TANDEM MASS SPECTROMETRY; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY;

12-DIAMINO-4,5-METHYLENEDIOXYBENZENE; 3,4-DIAMINOTOLUENE; COEFFICIENT OF VARIATION; CV; DAT; DMB; ELECTROSPRAY IONIZATION; ESI; FREE SIALIC ACID; HUMAN PLASMA; ILSC; INTERNAL STANDARD; IS; ISOTOPE-LABELED STANDARD CALIBRATION; KDN; KETODEOXYNONULOSONIC ACID; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; LLOQ; LOWER LIMIT OF QUANTIFICATION; MRM; MULTIPLE REACTION MONITORING; PAD; PPT; PROTEIN PRECIPITATION; PULSED AMPEROMETRIC DETECTION; QC; QUALITY CONTROL; QUINOXALINE DERIVATIZATION; RE; RELATIVE ERROR; ROOM TEMPERATURE; RT; SA; SIALIC ACID; UHPLC; ULTRA HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

CALIBRATION; CHROMATOGRAPHY, LIQUID; HUMANS; LINEAR MODELS; N-ACETYLNEURAMINIC ACID; QUINOXALINES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY;

EID: 84896964250     PISSN: 15700232     EISSN: 1873376X     Source Type: Journal    
DOI: 10.1016/j.jchromb.2013.11.016     Document Type: Article

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