메뉴 건너뛰기




Volumn 115, Issue , 2014, Pages 70-77

Development and validation of a multi-residue method for determination of 18 β-agonists in bovine urine by UPLC-MS/MS

Author keywords

Bovine urine; Solid phase extraction; UPLC MS MS; Validation; agonists

Indexed keywords


EID: 84896386940     PISSN: 0026265X     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.microc.2014.02.012     Document Type: Article
Times cited : (34)

References (44)
  • 1
    • 0003192964 scopus 로고
    • Council Regulation 1990/2377/EEC of 26 June 1990 laying down a community procedure for the establishment of maximum residue limits of veterinary medicinal products in foodstuffs of animal origin
    • Council of the European Union
    • Council of the European Union Council Regulation 1990/2377/EEC of 26 June 1990 laying down a community procedure for the establishment of maximum residue limits of veterinary medicinal products in foodstuffs of animal origin. Off. J. Eur. Communities 1990, L224:1-136.
    • (1990) Off. J. Eur. Communities , vol.L224 , pp. 1-136
  • 2
    • 77952193613 scopus 로고    scopus 로고
    • Commission Regulation 2010/37/EC of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin
    • Council of the European Union
    • Council of the European Union Commission Regulation 2010/37/EC of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin. Off. J. Eur. Communities 2010, L15:1-72.
    • (2010) Off. J. Eur. Communities , vol.L15 , pp. 1-72
  • 3
    • 84896382487 scopus 로고    scopus 로고
    • Council Directive 1996/22/EC of 29 April 1996 concerning the prohibition on the use in stockfarming of certain substances having a hormonal or thyrostatic action and of beta-agonists
    • Council of the European Union
    • Council of the European Union Council Directive 1996/22/EC of 29 April 1996 concerning the prohibition on the use in stockfarming of certain substances having a hormonal or thyrostatic action and of beta-agonists. Off. J. Eur. Communities 1996, L125:1-14.
    • (1996) Off. J. Eur. Communities , vol.L125 , pp. 1-14
  • 4
    • 0003178708 scopus 로고    scopus 로고
    • Council Directive 1996/23/EC of 29 April 1996 on measures to monitor certain substances and residues thereof in live animals and animal products
    • Council of the European Union
    • Council of the European Union Council Directive 1996/23/EC of 29 April 1996 on measures to monitor certain substances and residues thereof in live animals and animal products. Off. J. Eur. Communities 1996, L125:10-32.
    • (1996) Off. J. Eur. Communities , vol.L125 , pp. 10-32
  • 5
    • 0025147569 scopus 로고
    • Food poisoning related to consumption of illicit beta-agonist in liver
    • Martinez-Navarro J.F. Food poisoning related to consumption of illicit beta-agonist in liver. Lancet 1990, 336:1311.
    • (1990) Lancet , vol.336 , pp. 1311
    • Martinez-Navarro, J.F.1
  • 10
    • 0000738068 scopus 로고
    • Use of a β-agonist to alter fat and muscle deposition in steers
    • Ricks C.A., Dalrymple R.H., Baker P.K., Ingle D.L. Use of a β-agonist to alter fat and muscle deposition in steers. J. Anim. Sci. 1984, 59:1247-1255.
    • (1984) J. Anim. Sci. , vol.59 , pp. 1247-1255
    • Ricks, C.A.1    Dalrymple, R.H.2    Baker, P.K.3    Ingle, D.L.4
  • 11
    • 0031607382 scopus 로고    scopus 로고
    • Overview of the effects of β-adrenergic receptor agonists on animal growth including mechanisms of action
    • Mersmann H.J. Overview of the effects of β-adrenergic receptor agonists on animal growth including mechanisms of action. J. Anim. Sci. 1998, 76:160-172.
    • (1998) J. Anim. Sci. , vol.76 , pp. 160-172
    • Mersmann, H.J.1
  • 13
    • 0027535409 scopus 로고
    • Application of an enzyme-linked immunosorbent assay kit for β-agonist screening of bovine urines in north-eastern Italy
    • Angeletti R., Paleologo Oriundi M., Piro R., Bagnati R. Application of an enzyme-linked immunosorbent assay kit for β-agonist screening of bovine urines in north-eastern Italy. Anal. Chim. Acta. 1993, 275:215-219.
    • (1993) Anal. Chim. Acta. , vol.275 , pp. 215-219
    • Angeletti, R.1    Paleologo Oriundi, M.2    Piro, R.3    Bagnati, R.4
  • 14
    • 0029742901 scopus 로고    scopus 로고
    • Development of a tube enzyme immunoassay for "on-site" screening of urine samples in the presence of beta-agonists
    • Haasnoot W., Streppel L., Cazemier G., Salden M., Stouten P., Essers M., van Wichen P. Development of a tube enzyme immunoassay for "on-site" screening of urine samples in the presence of beta-agonists. Analyst 1996, 121:1111-1114.
    • (1996) Analyst , vol.121 , pp. 1111-1114
    • Haasnoot, W.1    Streppel, L.2    Cazemier, G.3    Salden, M.4    Stouten, P.5    Essers, M.6    van Wichen, P.7
  • 15
    • 0026024987 scopus 로고
    • Development of a specific radioimmunoassay for the detection of clenbuterol residues in treated cattle
    • Delahaut P., Dubois M., Pri-Bar O., Buchman I., Degand G., Ectors F. Development of a specific radioimmunoassay for the detection of clenbuterol residues in treated cattle. Food Addit. Contam. 1991, 8:43-53.
    • (1991) Food Addit. Contam. , vol.8 , pp. 43-53
    • Delahaut, P.1    Dubois, M.2    Pri-Bar, O.3    Buchman, I.4    Degand, G.5    Ectors, F.6
  • 16
    • 0032733674 scopus 로고    scopus 로고
    • Solid phase extraction of clenbuterol from plasma using immunoaffinity followed by HPLC
    • Rashid B.A., Kwasowski P., Stevenson D. Solid phase extraction of clenbuterol from plasma using immunoaffinity followed by HPLC. J. Pharm. Biomed. Anal. 1999, 21:635-639.
    • (1999) J. Pharm. Biomed. Anal. , vol.21 , pp. 635-639
    • Rashid, B.A.1    Kwasowski, P.2    Stevenson, D.3
  • 17
    • 0025011411 scopus 로고
    • Rapid determination of clenbuterol residues in urine by high-performance liquid chromatography with on-line automated sample processing using immunoaffinity chromatography
    • Haasnoot W., Ploum M.E., Paulussen R.J., Schilt R., Huf F.A. Rapid determination of clenbuterol residues in urine by high-performance liquid chromatography with on-line automated sample processing using immunoaffinity chromatography. J. Chromatogr. 1990, 519:323-335.
    • (1990) J. Chromatogr. , vol.519 , pp. 323-335
    • Haasnoot, W.1    Ploum, M.E.2    Paulussen, R.J.3    Schilt, R.4    Huf, F.A.5
  • 18
    • 0037466576 scopus 로고    scopus 로고
    • Detection of multi-β-agonist residues in liver matrix by use of a surface plasma resonance biosensor
    • Traynor I.M., Crooks S.R.H., Bowers J., Elliott C.T. Detection of multi-β-agonist residues in liver matrix by use of a surface plasma resonance biosensor. Anal. Chim. Acta. 2003, 483:187-191.
    • (2003) Anal. Chim. Acta. , vol.483 , pp. 187-191
    • Traynor, I.M.1    Crooks, S.R.H.2    Bowers, J.3    Elliott, C.T.4
  • 20
    • 0033624882 scopus 로고    scopus 로고
    • 2-agonists in bovine urine: comparison of two extraction/clean-up procedures for high-resolution gas chromatography-mass spectrometry analysis
    • 2-agonists in bovine urine: comparison of two extraction/clean-up procedures for high-resolution gas chromatography-mass spectrometry analysis. J. Anal. Toxicol. 2000, 24:146-152.
    • (2000) J. Anal. Toxicol. , vol.24 , pp. 146-152
    • Spisso, B.F.1    Lopes, C.C.2    Marques, M.A.3    Neto, F.R.4
  • 21
    • 0013285756 scopus 로고    scopus 로고
    • Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results
    • Council of the European Union
    • Council of the European Union Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off. J. Eur. Communities 2002, L221:8-36.
    • (2002) Off. J. Eur. Communities , vol.L221 , pp. 8-36
  • 22
    • 84855922034 scopus 로고    scopus 로고
    • Quick screening of priority beta-agonists in urine using automated TurboFlow™ LC/Exactive mass spectrometry
    • Bernsmann T., Furst P., Godula M. Quick screening of priority beta-agonists in urine using automated TurboFlow™ LC/Exactive mass spectrometry. Food Addit. Contam. A 2011, 28:1352-1363.
    • (2011) Food Addit. Contam. A , vol.28 , pp. 1352-1363
    • Bernsmann, T.1    Furst, P.2    Godula, M.3
  • 23
    • 0030175741 scopus 로고    scopus 로고
    • Detection and confirmation of β-agonists in bovine retina using LC/APCI-MS
    • Doerge D.R., Churchwell M.I., Holder C.L., Rowe L., Bajic S. Detection and confirmation of β-agonists in bovine retina using LC/APCI-MS. Anal. Chem. 1996, 68:1918-1923.
    • (1996) Anal. Chem. , vol.68 , pp. 1918-1923
    • Doerge, D.R.1    Churchwell, M.I.2    Holder, C.L.3    Rowe, L.4    Bajic, S.5
  • 24
    • 0028079971 scopus 로고
    • Determination of beta sympathomimetics in liver and urine by immunoaffinity chromatography and gas chromatography-mass-selective detection
    • Hooijerink H., Schilt R., van Bennekom E.O., Huf F.A. Determination of beta sympathomimetics in liver and urine by immunoaffinity chromatography and gas chromatography-mass-selective detection. J. Chromatogr. B 1994, 660:303-313.
    • (1994) J. Chromatogr. B , vol.660 , pp. 303-313
    • Hooijerink, H.1    Schilt, R.2    van Bennekom, E.O.3    Huf, F.A.4
  • 25
    • 0037279414 scopus 로고    scopus 로고
    • Simultaneous determination of Zilpaterol and other beta agonists in calf eye by gas chromatography/tandem mass spectrometry
    • Bocca B., Fiori M., Cartoni C., Brambilla G. Simultaneous determination of Zilpaterol and other beta agonists in calf eye by gas chromatography/tandem mass spectrometry. J. AOAC Int. 2003, 86:8-14.
    • (2003) J. AOAC Int. , vol.86 , pp. 8-14
    • Bocca, B.1    Fiori, M.2    Cartoni, C.3    Brambilla, G.4
  • 26
    • 84859768275 scopus 로고    scopus 로고
    • Simultaneous detection of residues of 25 beta-agonists and 23 beta-blockers in animal foods by high-performance liquid chromatography coupled with linear ion trap mass spectrometry
    • Sai F., Hong M., Yunfeng Z., Huijing C., Yongning W. Simultaneous detection of residues of 25 beta-agonists and 23 beta-blockers in animal foods by high-performance liquid chromatography coupled with linear ion trap mass spectrometry. J. Agric. Food Chem. 2012, 60:1898-1905.
    • (2012) J. Agric. Food Chem. , vol.60 , pp. 1898-1905
    • Sai, F.1    Hong, M.2    Yunfeng, Z.3    Huijing, C.4    Yongning, W.5
  • 28
    • 0031866114 scopus 로고    scopus 로고
    • Screening and confirmatory determination of ractopamine residues in calves treated with growth promoting doses of the β-agonist
    • Elliott C.T., Thompson C.S., Arts C.J.M., Crooks S.R.H., van Baak M.J., Verheij E.R., Baxter G.A. Screening and confirmatory determination of ractopamine residues in calves treated with growth promoting doses of the β-agonist. Analyst 1998, 123:1103-1107.
    • (1998) Analyst , vol.123 , pp. 1103-1107
    • Elliott, C.T.1    Thompson, C.S.2    Arts, C.J.M.3    Crooks, S.R.H.4    van Baak, M.J.5    Verheij, E.R.6    Baxter, G.A.7
  • 29
    • 8844257322 scopus 로고    scopus 로고
    • Multiresidue quantification and confirmation of beta-agonists in bovine retina and liver using LC-ES/MS/MS
    • Williams L.D., Churchwell M.I., Doerge D.R. Multiresidue quantification and confirmation of beta-agonists in bovine retina and liver using LC-ES/MS/MS. J. Chromatogr. B 2004, 813:35-45.
    • (2004) J. Chromatogr. B , vol.813 , pp. 35-45
    • Williams, L.D.1    Churchwell, M.I.2    Doerge, D.R.3
  • 30
    • 25644452696 scopus 로고    scopus 로고
    • Multi-residue liquid chromatography/tandem mass spectrometric analysis of beta-agonists in urine using molecular imprinted polymers
    • Van Hoof N., Courtheyn D., Antignac J.P., Van de Wiele M., Poelmans S., Noppe H., De Brabander H. Multi-residue liquid chromatography/tandem mass spectrometric analysis of beta-agonists in urine using molecular imprinted polymers. Rapid Commun. Mass Sp. 2005, 19:2801-2808.
    • (2005) Rapid Commun. Mass Sp. , vol.19 , pp. 2801-2808
    • Van Hoof, N.1    Courtheyn, D.2    Antignac, J.P.3    Van de Wiele, M.4    Poelmans, S.5    Noppe, H.6    De Brabander, H.7
  • 31
    • 12844271331 scopus 로고    scopus 로고
    • Determination of clenbuterol, ractopamine and zilpaterol in liver and urine by liquid chromatography tandem mass spectrometry
    • Blanca J., Muñoz P., Morgado M., Méndez N., Aranda A., Reuvers T., Hooghuis H. Determination of clenbuterol, ractopamine and zilpaterol in liver and urine by liquid chromatography tandem mass spectrometry. Anal. Chim. Acta. 2005, 529:199-205.
    • (2005) Anal. Chim. Acta. , vol.529 , pp. 199-205
    • Blanca, J.1    Muñoz, P.2    Morgado, M.3    Méndez, N.4    Aranda, A.5    Reuvers, T.6    Hooghuis, H.7
  • 32
    • 42449117989 scopus 로고    scopus 로고
    • Multiresidue analysis of beta-agonists in bovine and porcine urine, feed and hair using liquid chromatography electrospray ionisation tandem mass spectrometry
    • Nielen M.W.F., Lasaroms J.J.P., Essers M.L., Oosterink J.E., Meijer T., Sanders M.B., Zuidema T., Stolker A.A.M. Multiresidue analysis of beta-agonists in bovine and porcine urine, feed and hair using liquid chromatography electrospray ionisation tandem mass spectrometry. Anal. Bioanal. Chem. 2008, 391:199-210.
    • (2008) Anal. Bioanal. Chem. , vol.391 , pp. 199-210
    • Nielen, M.W.F.1    Lasaroms, J.J.P.2    Essers, M.L.3    Oosterink, J.E.4    Meijer, T.5    Sanders, M.B.6    Zuidema, T.7    Stolker, A.A.M.8
  • 33
    • 59649118023 scopus 로고    scopus 로고
    • Multi-residual analysis of 16 β-agonists in pig liver, kidney and muscle by ultra performance liquid chromatography tandem mass spectrometry
    • Shao B., Jia X., Zhang J., Meng J., Wu Y., Duan H., Tu X. Multi-residual analysis of 16 β-agonists in pig liver, kidney and muscle by ultra performance liquid chromatography tandem mass spectrometry. Food Chem. 2009, 114:1115-1121.
    • (2009) Food Chem. , vol.114 , pp. 1115-1121
    • Shao, B.1    Jia, X.2    Zhang, J.3    Meng, J.4    Wu, Y.5    Duan, H.6    Tu, X.7
  • 34
    • 26444507780 scopus 로고    scopus 로고
    • Improving LC-MS sensitivity through increases in chromatographic performance: comparisons of UPLC-ES/MS/MS to HPLC ES/MS/MS
    • Churchwell M.I., Twaddle N.C., Meeker L.R., Doerge D.R. Improving LC-MS sensitivity through increases in chromatographic performance: comparisons of UPLC-ES/MS/MS to HPLC ES/MS/MS. J. Chromatogr. B 2005, 825:134-143.
    • (2005) J. Chromatogr. B , vol.825 , pp. 134-143
    • Churchwell, M.I.1    Twaddle, N.C.2    Meeker, L.R.3    Doerge, D.R.4
  • 36
    • 84860125813 scopus 로고    scopus 로고
    • UPLC-MS/MS determination of ractopamine residues in retinal tissue of treated food-producing pigs
    • Vulić A., Pleadina J., Perši N., Milić D., Radeck W. UPLC-MS/MS determination of ractopamine residues in retinal tissue of treated food-producing pigs. J. Chromatogr. B 2012, 895-896:102-107.
    • (2012) J. Chromatogr. B , pp. 102-107
    • Vulić, A.1    Pleadina, J.2    Perši, N.3    Milić, D.4    Radeck, W.5
  • 37
    • 0031944741 scopus 로고    scopus 로고
    • Assessment of detection methods in trace analysis by means of a statistically based in-house validation concept
    • Jülicher B., Gowik P., Uhlig S. Assessment of detection methods in trace analysis by means of a statistically based in-house validation concept. Analyst 1998, 123:173-179.
    • (1998) Analyst , vol.123 , pp. 173-179
    • Jülicher, B.1    Gowik, P.2    Uhlig, S.3
  • 38
    • 0032918630 scopus 로고    scopus 로고
    • A top-down in-house validation based approach for the investigation of the measurement uncertainty using fractional factorial experiments
    • Jülicher B., Gowik P., Uhlig S. A top-down in-house validation based approach for the investigation of the measurement uncertainty using fractional factorial experiments. Analyst 1999, 124:537-545.
    • (1999) Analyst , vol.124 , pp. 537-545
    • Jülicher, B.1    Gowik, P.2    Uhlig, S.3
  • 39
    • 84896364782 scopus 로고    scopus 로고
    • InterValplus, quo data GmbH, Dresden, Germany, (accessed 7 November)
    • InterValplus Software for In-house Validation 2012, quo data GmbH, Dresden, Germany, (http://www.quodata.de, accessed 7 November).
    • (2012) Software for In-house Validation
  • 41
    • 0031612355 scopus 로고    scopus 로고
    • The pharmacokinetics, metabolism, and tissue residues of beta-adrenergic agonists in livestock
    • Smith D.J. The pharmacokinetics, metabolism, and tissue residues of beta-adrenergic agonists in livestock. J. Anim. Sci. 1998, 76:173-194.
    • (1998) J. Anim. Sci. , vol.76 , pp. 173-194
    • Smith, D.J.1
  • 43
    • 84866049525 scopus 로고    scopus 로고
    • Wide-range screening of banned veterinary drugs in urine by ultra high liquid chromatography coupled to high-resolution mass spectrometry
    • León N., Roca M., Igualada C., Martins C.P.B., Pastor A., Yusá V. Wide-range screening of banned veterinary drugs in urine by ultra high liquid chromatography coupled to high-resolution mass spectrometry. J. Chromatogr. A 2012, 1258:55-65.
    • (2012) J. Chromatogr. A , vol.1258 , pp. 55-65
    • León, N.1    Roca, M.2    Igualada, C.3    Martins, C.P.B.4    Pastor, A.5    Yusá, V.6
  • 44
    • 84866553902 scopus 로고    scopus 로고
    • Simultaneous determination of 10 _2-agonists in swine urine using liquid chromatography-tandem mass spectrometry and multi-walled carbon nanotubes as a reversed dispersive solid phase extraction sorbent
    • Du X.-D., Wu Y.-L., Yang H.-J., Yang T. Simultaneous determination of 10 _2-agonists in swine urine using liquid chromatography-tandem mass spectrometry and multi-walled carbon nanotubes as a reversed dispersive solid phase extraction sorbent. J. Chromatogr. A 2012, 1260:25-32.
    • (2012) J. Chromatogr. A , vol.1260 , pp. 25-32
    • Du, X.-D.1    Wu, Y.-L.2    Yang, H.-J.3    Yang, T.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.