Solvothermal conversion of magadiite into zeolite omega in a glycerol-water system

Journal of Chemical Technology and Biotechnology

Volumn 89, Issue 3, 2014, Pages 419-424

  Cui, Miao ^a   Wang, Yu ^a   Liu, Xiaoyu ^a   Zhu, Jiang ^a   Sun, Jiangbo ^a   Lv, Nan ^a   Meng, Changgong ^a  

^a DALIAN UNIVERSITY OF TECHNOLOGY   (China)

Author keywords

Characterization; Crystallization; Synthesis; Zeolites

Indexed keywords

CHARACTERIZATION; CRYSTALLIZATION; SYNTHESIS (CHEMICAL); WATERWORKS; ZEOLITES;

HIGHLY ORDERED PORES; MOLAR COMPOSITIONS; ORGANIC SPECIES; QUATERNARY AMMONIUM COMPOUND; SIX-MEMBERED RINGS; STRUCTURE DIRECTING AGENTS; SYNTHESIS METHOD; TETRAMETHYLAMMONIUM;

GLYCEROL;

ALUMINUM; GLYCEROL; INDUSTRIAL CHEMICAL; INFUSORIAL EARTH; INORGANIC COMPOUND; MAGADIITE; QUATERNARY AMMONIUM DERIVATIVE; SILICON DIOXIDE; SODIUM HYDROXIDE; SOLVENT; TETRAMETHYLAMMONIUM; UNCLASSIFIED DRUG; WATER; ZEOLITE;

ALKALINITY; ARTICLE; CATALYST; CRYSTALLIZATION; DESORPTION; REACTION TIME; SCANNING ELECTRON MICROSCOPY; SYNTHESIS; TEMPERATURE SENSITIVITY; THERMAL ANALYSIS; THERMOGRAVIMETRY; WATER CONTENT; X RAY DIFFRACTION; X RAY POWDER DIFFRACTION;

EID: 84895072482     PISSN: 02682575     EISSN: 10974660     Source Type: Journal    
DOI: 10.1002/jctb.4134     Document Type: Article

References (40)

1. Martucci A, Alberti A, Guzman-Castillo ML, Di Renzo F and Fajula F, Crystal structure of zeolite omega, the synthetic counterpart of the natural zeolite mazzite. Micropor Mesopor Mater 63:33-42 (2003).
2. Fajula F, Ibarra R, Figueras F and Gueguen C, Hydration of n-butenes using zeolite catalysts. Influence of the aluminium content on activity. J Catal 89:60-68 (1984).
3. Solinas V, Monaci R, Marongiu B and Forni L, Isomerisation of 1-methylnaphthalene over synthetic zeolites. Appl Catal 9:109-117 (1984).
4. Flanigen EM and Kellberg ER, Synthetic crystalline zeolite and process for preparing same. US Patent 4241036 (1980).
5. Cole JF and Kouwenhoven HW, Synthesis and properties of zeolite omega, in Molecular Sieves, ACS Symposium, vol. 121, ed by Meier WM and Uytterhoeven JB. American Chemical Society, Washington DC, 583-595 (1973).
6. Goossens AM, Feijen EJP, Verhoeven G, Wouters BH, Grobet PJ, Jacobs PA and Martens JA, Crystallization of MAZ-type zeolites using tetramethylammonium, sodium and n-hexane derivatives as structure- and composition-directing agents. Micropor Mesopor Mater 35-36:555-572 (2000).
7. Edmunds MPW, Hill SJ, Latham K and Williams CD, Synthesis of zeolite omega in an alcohol-water system. Zeolites 14:529-532 (1994).
8. Nicolas S, Massiani P, Vera-Pacheco M, Fajula F and Figueras F, A new synthesis route to zeolite omega. Stud Surf Sci Catal 37:115-122 (1988).
9. Araya A, Barber TJ, Lowe BM, Sinclair DM and Varma A, The synthesis and thermal behaviour of zeolite omega. Zeolites 4:263-268 (1984).
10. Fajula F, Vera-Pacheco M and Figueras F, Synthesis of zeolite omega. Influence of the temperature and the reagents on the crystallization kinetics. Zeolites 7:203-208 (1987).
11. Perrotta AJ, Kibby C, Mitchell BR and Tucci ER, The synthesis, characterization, and catalytic activity of omega and ZSM-4 zeolites. J Catal 55:240-249 (1978).
12. Huang LM, Chen XY and Li QZ, Synthesis of microporous molecular sieves by surfactant decomposition. J Mater Chem 11:610-615 (2001).
13. Guzman-Castillo ML, Di Renzo F, Fajula F and Bousquet J, Crystallization kinetics of zeolite omega, the synthetic analog of mazzite. Micropor Mesopor Mater 90:221-228 (2006).
14. 2O. Micropor Mater 10:247-257 (1997).
15. Xu H, Dong P, Liu L, Wang JG, Deng F and Dong JX, Synthesis of mazzite-type zeolites in the presence of organic solvents: study of the structure directing role of p-dioxane. J Porous Mater 14:97-101 (2007).
16. 2O glycerol. Micropor Mater 9:273-286 (1997).
17. Yang S and Evmiridis NP, Synthesis of omega zeolite without use of tetramethylammonium (TMA) ions. Stud Surf Sci Catal 84:155-162 (1994).
18. Tsitsishvili GV and Charkviani MK, Preparation and properties of a new synthetic analogue of natural zeolite mazzite. Stud Surf Sci Catal 28:161-167 (1986).
19. Selvam T, Bandarapu B, Mabande GTP, Toufar H and Schwieger W, Hydrothermal transformation of a layered sodium silicate, kanemite, into zeolite Beta (BEA). Micropor Mesopor Mater 64:41-50 (2003).
20. Pál-Borbély G, Szegedi Á and Beyer HK, Solid-state recrystallization of aluminum-containing kanemite varieties to ferrierite. Micropor Mesopor Mater 35-36:573-584 (2000).
21. Feng F and Balkus KJ, Recrystallization of layered silicates to silicalite-1. Micropor Mesopor Mater 69:85-96 (2004).
22. Pál-Borbély G, Beyer HK, Kiyozumi Y and Mizukami F, Recrystallization of magadiite varieties isomorphically substituted with aluminum to MFI and MEL zeolites. Micropor Mater 11:45-51 (1997).
23. Pál-Borbély G, Beyer HK, Kiyozumi Y and Mizukami F, Synthesis and characterization of a ferrierite made by recrystallization of an aluminium-containing hydrated magadiite. Micropor Mesopor Mater 22:57-68 (1998).
24. Onyestyák G, Pál-Borbély G and Rees LVC, Dynamic and catalytic studies of H-ferrierites made by hydrothermal and dry state syntheses. Micropor Mesopor Mater 43:73-81 (2001).
25. Ko Y, Kim SJ, Kim MH, Park J-H, Parise JB and Uh YS, New route for synthesizing Mn-silicalite-1. Micropor Mesopor Mater 30:213-218 (1999).
26. Selvam T and Schwieger W, Synthesis and characterization of mordenite (MOR) zeolite derived from a layered silicate, Na-magadiite. Stud Surf Sci Catal 142:407-414 (2002).
27. Selvam T, Mabande GTP, Schwieger W, Sugi Y, Toyama I, Kubota Y, Lee H-S and Kim JH, Selective isopropylation of biphenyl to 4, 4'-DIPB over mordenite (MOR) type zeolite obtained from a layered sodium silicate magadiite. Catal Lett 94:17-24 (2004).
28. Kooli F, Mizukami F, Kiyozumi Y and Akiyama Y, Hydrothermal conversion of Na-magadiite to a new silicate layered structure in a TMAOH-water-1, 4-dioxane system. J Mater Chem 11:1946-1950 (2001).
29. 2O system. New J Chem 25:1613-1620 (2001).
30. Kooli F, Kiyozumi Y and Mizukami F, Conversion of protonated magadiite to a crystalline microporous silica phase via a new layered silicate. Chem Phys Chem 2:549-551 (2001).
31. Kooli F, Kiyozumi Y and Mizukami F, Effect of alkali cations on the conversion of H-magadiite in tetramethylammonium hydroxide-water-1, 4-dioxane system. Mater Chem Phys 7:134-140 (2002).
32. Kooli F, Kyozumi Y, Rives V and Mizukami F, Synthesis and textural characterization of a new microporous silica material. Langmuir 18:4103-4110 (2002).
33. Wang Y, Shang YS, Wu J, Zhu J, Yang Y and Meng CG, Recrystallization of magadiite into offretite in the presence of tetramethylammonium cations. J Chem Technol Biotechnol 85:279-282 (2010).
34. 2O system. Solid State Sci 13:2124-2128 (2011).
35. Wang Y, Wu J, Zhu J, Yang Y, Qi L, Ji SH and Meng CG, The Influence of short-chain tetraalkylammonium cations on the recrystallization of magadiite into zeolites. Micropor Mesopor Mater 135:143-148 (2010).
36. Wang Y, Shang YS, Zhu J, Wu J, Ji SH and Meng CG, Synthesis of magadiite using a natural diatomite material. J Chem Technol Biotechnol 84:1894-1898 (2009).
37. Zelent B, Nucci NV and Vanderkooi JM, Liquid and ice water and glycerol/water glasses compared by infrared spectroscopy from 295 to 12 K. J Phys Chem A 108:11141-11150 (2004).
38. Salou M, Kiyozumi Y, Mizukami F, Nair P, Maeda K and Niwa S, Influence of solid-state transformation time on the nucleation and growth of silicalite-1 prepared from layered silicate. J Mater Chem 8:2125-2132 (1998).
39. 27Al MAS n.m.r. study of the distribution of Si and Al atoms in various forms of synthetic zeolite omega. Zeolites 8:332-337 (1988).
40. Massiani P, Fajula F and Di Renzo F, Zoning of aluminium among different crystallographic sites in zeolite omega. J Chem Soc Chem Commun 814-815 (1988).