Determination of phenolic compounds in olive oil: New method based on liquid-liquid micro extraction and ultra high performance liquid chromatography-triple-quadrupole mass spectrometry

LWT

Volumn 57, Issue 1, 2014, Pages 49-57

  Becerra Herrera, Mercedes ^a   Sánchez Astudillo, María ^a   Beltrán, Rafael ^a   Sayago, Ana ^a  

^a UNIVERSITY OF HUELVA   (Spain)

Author keywords

Liquid liquid micro extraction; Matrix effect; Olive oil; Phenolic compounds; UHPLC ESI MS MS

Indexed keywords

EFFICIENCY; ELECTROSPRAY IONIZATION; EXTRACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; PHENOLS; QUALITY CONTROL;

ELECTROSPRAY IONIZATION SOURCES; LIQUID CHROMATOGRAPHY ELECTROSPRAY; LIQUID-LIQUID MICRO EXTRACTION; LIQUID-LIQUIDS; MATRICES EFFECT; MICROEXTRACTION; PHENOLIC COMPOUNDS; STANDARD SOLUTIONS; ULTRA HIGH PERFORMANCE LIQUID CHROMATOGRAPHY-ELECTROSPRAY IONIZATION SOURCE-MS/MS; ULTRA-HIGH PERFORMANCE LIQUID CHROMATOGRAPHIES;

OLIVE OIL;

EID: 84894267320     PISSN: 00236438     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.lwt.2014.01.016     Document Type: Article

References (36)

1. Alarcón M.I., Romero-González R., Garrido A., Martínez J.L. Analysis of phenolic compounds in olive oil by solid-phase extraction and ultra-high performance liquid chromatography-tandem mass spectrometry. Food Chemistry 2012, 134:2465-2472.
2. Angerosa F., Mostallino R., Basti C., Vito R. Virgin olive oil odour notes: their relationships with volatile compounds from the lipoxygenase pathway and secoiridoid compounds. Food Chemistry 2000, 68:283-287.
3. Antolovich M., Bedgood J.D.R., Bishop A.G., Jardine D., Prenzler P.D., Robards K. LC-MS investigation of oxidation products of phenolic antioxidants. Journal of Agricultural and Food Chemistry 2004, 52:962-971.
4. Armbruster D.A., Tillman M.D., Hubbs L.M. Limit of detection (LOD)/limit of quantitation (LOQ): comparison of the empirical and the statistical methods exemplified with GC-MS assays of abused drugs. Clinical Chemistry 1994, 40:1233-1238.
5. Barceló-Barrachina E., Moyano E., Puignou L., Galceran M.T. Evaluation of reversed-phase columns for the analysis of heterocyclic aromatic amines by liquid chromatography-electrospray mass spectrometry. Journal of Chromatography B 2004, 802:45-59.
6. Burham D.L., Price P.I., Rudewicz P.J. Quantitation of SR 27417 in human plasma using electrospray liquid chromatography-tandem mass spectrometry: a study of ion suppression. Journal of the American Society for Mass Spectrometry 1996, 7:1099-1105.
7. Choi B.K., Hercules D.M., Gusev A.I. Effect of liquid chromatography separation of complex matrices on liquid chromatography-tandem mass spectrometry signal suppression. Journal of Chromatography A 2001, 907:337-342.
8. Cicerale S., Lucas L., Keast R. Biological activities of phenolic compounds present in virgin olive oil. International Journal of Molecular Science 2010, 11:458-479.
9. Cunha S.C., Lehotay S.J., Mastovska K., Fernandes J.O., Oliveira M.P.P. Evaluation of the QuECHERS sample preparation approach for the analysis of pesticide residues in olives. Journal of Separation Science 2007, 30:620-632.
10. Ferrer C., Gómez M.J., García-Reyes J.F., Ferrer I., Thurman E.M., Fernández-Alba A.R. Determination of pesticide residues in olives and olive oil by matrix solid-phase dispersion followed by gas chromatography/mass spectrometry and liquid chromatography/tandem mass spectrometry. Journal of Chromatography A 2005, 1069:183-194.
11. Fu I., Woolf E.J., Matuszewski B.K. Effect of the sample matrix on the determination of indinavir in human urine by HPLC with turbo ion spray tandem mass spectrometric detection. Journal of Pharmaceutical and Biomedical Analysis 1998, 18:347-357.
12. García-Villalba R., Carrasco-Pancorbo A., Oliveras-Ferraros C., Vázquez-Martín A., Menéndez J.A., Segura-Carretero A., et al. Characterization and quantification of phenolic compounds of extra-virgin olive oils with anticancer properties by a rapid and resolutive LC-ESI-TOF MS method. Journal of Pharmaceutical and Biomedical Analysis 2010, 51:416-429.
13. Hajšlová J., Zrostlíková J. Matrix effects in (ultra)trace analysis of pesticide residues in food and biotic matrices. Journal of Chromatography A 2003, 1000:181-197.
14. Herrero M., Temirzoda T.N., Segura-Carretero A., Quirantes R., Plaza M., Ibáñez E. New possibilities for the valorization of olive oil by-products. Journal of Chromatography A 2011, 1218:7511-7520.
15. Jerman T., Trebše P., MozetičVodopivec B. Ultrasound-assisted solid liquid extraction (USLE) of olive fruit (Olea europaea) phenolic compounds. Food Chemistry 2010, 123:175-182.
16. Lavelli V., Bondesan L. Secoiridoids, tocopherols, and antioxidant activity of monovarietal extra virgin olive oils extracted from destoned fruits. Journal of Agricultural and Food Chemistry 2005, 53:1102-1107.
17. Leenen R., Roodenburg A.J.C., Vissers M.N., Schuurbiers J.A.E., Van Putte K.P.A.M., Wiseman S.A., et al. Supplementation of plasma with olive oil phenols and extracts: influence on LDL oxidation. Journal of Agricultural and Food Chemistry 2002, 50:1290-1297.
18. Long G.L., Winefordner J.D. Limit of detection: a closer look at the IUPAC definition. Analytical Chemistry 1983, 55:712-724.
19. Mateos R., Espartero J.L., Trujillo M., Ríos J.J., León-Camacho M., Alcudia F., et al. Determination of phenols, flavones, and lignans in virgin olive oils by solid-phase extraction and high-performance liquid chromatography with diode array ultraviolet detection. Journal of Organic Chemistry 2001, 49:2185-2192.
20. Matuszewski B.K., Constanzer M.L., Chavez-Eng C.M. Strategies for the assessment of matrix effect in quantitative bioanalytical methods based on HPLC-MS/MS. Analytical Chemistry 2003, 75:3019-3030.
21. Mazzotti F., Benabdelkamel H., Di Donna L., Maiuolo L., Napoli A., Sindona G. Assay of tyrosol and hydroxytyrosol in olive oil by tandem mass spectrometry and isotope dilution method. Food Chemistry 2012, 135:1006-1010.
22. Motilva M.J., Serra A., Macia A. Analysis of food polyphenols by ultra high-performance liquid chromatography coupled to mass spectrometry: an overview. Journal of Chromatography A 2013, 1292:66-82.
23. Nováková L., Matysová L., Solich P. Advantages of application of UPLC in pharmaceutical analysis. Talanta 2006, 68:908-918.
24. Perri E., Raffaelli A., Sindona G. Quantitation of oleuropein in virgin olive oil by ionspray mass spectrometry-selected reaction monitoring. Journal of Agricultural and Food Chemistry 1999, 47:4156-4160.
25. Pizarro M.L., Becerra M., Sayago A., Beltrán M., Beltrán R. Comparison of different extraction methods to determine phenolic compounds in virgin olive oil. Food Analytical Methods 2013, 6:123-132.
26. Romani A., Mulinacci N., Pinelli P., Vincieri F.F., Cimato A. Polyphenolic content in five tuscany cultivars of Olea europaea L. Journal of Agricultural and Food Chemistry 1999, 47:964-967.
27. Ryan D., Robards K. Phenolic compounds in olives. Analyst 1998, 123:31-44.
28. Savarese M., De Marco E., Sacchi R. Characterization of phenolic extracts from olives (Olea europaea cv. Pisciottana) by electrospray ionization mass spectrometry. Food Chemistry 2007, 105:761-770.
29. Servili M., Baldioli M., Selvaggini R., Miniati E., Machioni A., Montedoro G.F. High-performance liquid chromatography evaluation of phenols in olive fruit, virgin olive oil, vegetation waters, and pomace and 1D- and 2D-nuclear magnetic resonance characterization. Journal of the American Oil Chemists' Society 1999, 76:873-882.
30. Servili M., Montedoro G.F. Contribution of phenolic compounds to virgin olive oil quality. European Journal of Lipid Science and Technology 2002, 104:602-613.
31. Škerget M., Kotnik P., Hadolin M., Hraš A.R., Simonič M., Knez Ž. Phenols, proanthocyanidins, flavones and flavonols in some plant materials and their antioxidant activities. Food Chemistry 2005, 89:191-198.
32. Suárez M., Macià A., Romero M.P., Motilva M.J. Improved liquid chromatography tandem mass spectrometry method for the determination of phenolic compounds in virgin olive oil. Journal of Chromatography A 2008, 1214:90-99.
33. Suárez M., Romero M.P., Macià A., Valls R.M., Fernández S., Solà R., et al. Improved method for identifying and quantifying olive oil phenolic compounds and their metabolites in human plasma by microelution solid-phase extraction plate and liquid chromatography-tandem mass spectrometry. Journal of Chromatography B 2009, 877:4097-4106.
34. Tang L., Kebarle P. Dependence of ion intensity in electrospray mass spectrometry on the concentration of the analytes in the electrosprayed solution. Analytical Chemistry 1993, 65:3654-3668.
35. Taylor P.J. Matrix effects: the Achilles heel of quantitative high-performance liquid chromatography-electrospray-tandem mass spectrometry. Clinical Biochemistry 2005, 38:328-334.
36. Vázquez Roncero A., Janer Del Valle C., Janer Del Valle M.L. Determinación de polifenoles totales en el aceite de oliva. Grasas Y Aceites 1973, 24:350-357.