Chromatographic methods for simultaneous determination of diiodohydroxyquinoline and Metronidazole in their binary mixture

Pakistan Journal of Pharmaceutical Sciences

Volumn 26, Issue 5, 2013, Pages 865-871

  Ali, Nouruddin Wageih ^a   Gamal, Mohammed ^a   Abdelkawy, Mohammed ^b  

^a Beni Suef University   (Egypt)

^b CAIRO UNIVERSITY   (Egypt)

Author keywords

Diiodohydroxyquinoline and metronidazole; RP HPLC; TLC spectrodensitometry

Indexed keywords

ACETIC ACID; ACETONE; CHLOROFORM; DIIODOHYDROXYQUIN; METHANOL; METRONIDAZOLE; SILICA GEL; WATER; BUFFER; SOLVENT;

ARTICLE; CHROMATOGRAPHY; DENSITOMETRY; DRUG DETERMINATION; DRUG FORMULATION; FLOW RATE; POWDER; QUALITY CONTROL; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; THIN LAYER CHROMATOGRAPHY; CALIBRATION; CHEMISTRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MEDICINAL CHEMISTRY; PH; PHARMACEUTICS; PROCEDURES; REPRODUCIBILITY; REVERSED PHASE LIQUID CHROMATOGRAPHY; STANDARD; STANDARDS; ULTRAVIOLET SPECTROPHOTOMETRY;

BUFFERS; CALIBRATION; CHEMISTRY, PHARMACEUTICAL; CHROMATOGRAPHY; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, REVERSE-PHASE; CHROMATOGRAPHY, THIN LAYER; HYDROGEN-ION CONCENTRATION; IODOQUINOL; METRONIDAZOLE; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SOLVENTS; SPECTROPHOTOMETRY, ULTRAVIOLET; TECHNOLOGY, PHARMACEUTICAL;

EID: 84892609887     PISSN: 1011601X     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (33)

1. Argekar AP, Raj SV and Kapadia SU (1996). Simultaneous Determination of Metronidazole and Nalidixic Acid in Pharmaceutical Dosage Forms by HPTLC. Indian Drugs, 33: 167-170. (Pubitemid 26165109)
2. Belal F (1984). Spectrophotometric determination of halogenated 8-hydroxyquinoline derivatives. Talanta, 3(8): 648-650.
3. Bhowal SK and Das TK (1990). Spectrophotometric determination of clioquinol, iodoquinol and broxyquinoline in pharmaceutical preparations after complexation with some bivalent metal ions. IJPS, 52(4): 200-204
4. Chatterjee PK, Jain CL and Sethi PD (1986). Simultaneous spectrophotometric estimation of diiodohydroxyquinoline and metronidazole or their analogues derivatives in combined dosage forms. IJPS,48(6): 195-197. (Pubitemid 17039599)
5. Daeseleire E, De-Ruyck H and Van-Renterghem R (2000). Rapidconfirmatory assay for the simultaneous detection of ronidazole, metronidazole and dimetridazole in eggs using liquidchromatographytandem mass spectrometry. Analyst, 125(9): 1533-1535.
6. Erk N and Altun MLN (2001). Spectrophotometric resolution of metronidazole and miconazole nitrate in ovules using ratio spectra derivative spectrophotometry and RP-LC. J. Pharm. Biomed. Anal., 25(1): 115-122. (Pubitemid 32234406)
7. Frasey AM, Boyer-Grand A, Pouget MP, Vennat B, Lartigue C and Galmier MS (2004). Validation of a Reversed-phase liquid chromatographic method for the determination of metronidazole in transparent oilwater-gel formulations Microchimica. Acta., 144(1): 171-176. (Pubitemid 40792555)
8. ICH Harmonised Tripartite Guideline: Validation of Analytical Procedures: Text and Methodology, Q2(R1) Geneva 2005.
9. Jin WR, Dong Q, Yu DQ, Ye XY and Li W (2000). Capillary electrophoresis/electrochemical detection system with on-line deoxygenation. Electrophoresis, 21(8): 1540-1544. (Pubitemid 30340976)
10. Kavarana HH (1959). Assay of diiodohydroxyquin by non-aqueous titration. American journal of pharmacy and the sciences supporting public health,(Please proper abbreviation)131(5): 184-187.
11. Khashaba PY, Refaat I H C, Emara K M and Gaber H M (1999). ,Utility of Diazotized 4-Amino-6-Chloro-1,3-Benzene Disulphonamide for the Spectrophotometric Determination of 8-Hydroxquinolines and Dibenzazepines, Analytical Letters,32(15): 3029-3047.
12. Liu G, Zhang QM, Wu W, Zhang J, Jiang R and Tan ST (2003). HPLC Determination of Metronidazole, Chloramphenicol and Hydrocortisone in Nasal Cavities Lotion,Yaowu Fenxi Zazhi,23(4): 317-319.
13. López-De-Alba P L, Wróbel K, López-Martínez L, Wróbel K, Yepez-Murrieta M L, Amador-Hernández J (1997). Application of the bivariate spectrophotometric method for the determination of metronidazole, furazolidone and di-iodohydroxyquinoline in pharmaceutical formulations. JPBA, 16(2): 349-355. (Pubitemid 27504627)
14. Lu SF, Wu KB, Dang XP and Hu SS (2004). Electrochemical Reduction and Voltammetric Determination of Metronidazole at a Nanomaterial Thin Film Coated Glassy Carbon Electrode. Talanta, 63: 653-657.
15. Martindale: The Extra Pharmacopoeia., The Complete Drug Reference (2006). 35th Ed., K. Profitt (Ed.), Royal Pharmaceutical Society, London, UK.
16. Merck Index: An Encyclopedia of Chemicals, Drugs and Biologicals (2006). 14th Ed., S. Budavari (Ed.), Merck & Co., Inc., Whitehouse Station, NJ.
17. Grinberg N (1990). Modern Thin-Layer Chromatography, Marcel Dekker Inc., New York.
18. Nagaraja P, Sunitha KR, Vasantha RA and Yathirajan HS (2002). Spectrophotometric determination of metronidazole and tinidazole in pharmaceutical preparations. J. Pharm. Biomed. Anal., 28(3-4): 527-535. (Pubitemid 34465623)
19. Nejem RM, Issa MM, El-Abadla NS, Al-Kholy M and Saleh AA (2008). Determination of diiodohydroxyquinoline using UV-visible and atomic absorption spectrometry. Asian Journal of Chemistry (AJC),20(5): 3849-3856.
20. Paranjothy KLK and Banerjee SK (1973). Estimation of diiodohydroxyquin in nonaqueous media. J Pharm Sci, 62(10): 97-1698.
21. Parimoo P, Umapathi P, Ravikumar N and Rajasehar S (1992). Determination of metronidazole and diiodohydroxyquinoline in pharmaceutical preparations by quantitative thin layer chromatography. Indian Drugs, 29(5): 228-230.
22. Rizk M, Belal F, Ibrahim F, Ahmed S and Sheribah ZA (2000). Derivative UV spectrophotometric analysis of some pharmaceutically important halogenated 8-Hdroxyquinoline derivatives via their Pd (II)-Complexes. Scientia Pharmaceutica, 68(3): 297-307.
23. Rizk M, Belal F, Ibrahim F, Ahmed S and Sheribah ZA (2002). LC of pharmaceutically important halogenated 8-hydroxyquinolines after precolumn derivatization with Pd (II). JPBA, 27(5): 813-820. (Pubitemid 34117668)
24. Saha U, Sen AK and Das TK (1988). Spectrophotometric determination of clioquinol and diodoquin in pharmaceutical preparations using uranyl acetate as a chromogenic agent. Analyst, 113(11): 653-1655.
25. Shen JZ, Yhang Y, Zhang SX, Ding SY and Xiang XH (2003). Determination of Nitroimidazoles and their metabolites in Swine tissues by liquid chromatography. J. AOAC Int. ,86(3): 505-509.
26. Shingbal DM and Natekar GB (1980). Determination of diiodohydroxyquinoline in pharmaceutical dosage forms. IJPS, 42(6): 181-183. (Pubitemid 11144514)
27. Soliman SA (1975). A simple method for the determination of 5,7-diiodoquinolin-8-ol and 5-chloro-7-iodoquinolin-8-ol (clioquinol). The Analyst, 100(1195): 696-702.
28. Storms ML and Stewart JT (2002). Development of a reversed-phase liquid chromatographic method for the analysis of amoxicillin metronidazole and pantoprazole in human plasma using solid-phaseextraction. J. Liq. Chromatogr. Rel. Tech., 25(16): 2433-2443.
29. United States Pharmacopeia (2009). The National Formulary USP, United States Pharmacopeia Convention Inc.
30. Wang JH (2001). Determination of three nitroimidazole residues in poultry meat by gas chromatography with nitrogen-phosphorus detection. J. Chromatogr A, 918(2): 435-438.
31. Windheuser JJ and Chu DY (1967). Colorimetric determination of iodochlorhydroxyquin and diiodohydroxyquin. J Pharm Sci , 6(4): 519-521.
32. Wojtowicz EJ (1984). Reverse-phase high-performance liquid chromatographic determination of halogenated 8-hydroxyquinoline compounds in pharmaceuticals and bulk drugs. J Pharm Sci , 73(10): 1430-1433. (Pubitemid 14021900)
33. Yu HY, Xia XP, Xu LY, He J and Chen FY (2002). Studies on determination of metronidazole and tinidazole in breast-feeding women. Yaowu Fenxi Zazhi, 22(2): 274-277.