Establishing two-stage interaction between fly ash and NaOH by X-ray and infrared analyses

Frontiers of Environmental Science and Engineering

Volumn 9, Issue 2, 2015, Pages 216-221

  Jha, Bhagwanjee ^a   Koshy, Nevin ^a   Singh, Devendra Narain ^a  

^a INDIAN INSTITUTE OF TECHNOLOGY BOMBAY   (India)

Author keywords

alkali activation; fly ash zeolites; hydrothermal treatment; X ray diffraction (XRD) and Fourier transform infrared radiation (FT IR) spectroscopy

Indexed keywords

EID: 84891636976     PISSN: 20952201     EISSN: 2095221X     Source Type: Journal    
DOI: 10.1007/s11783-014-0630-8     Document Type: Article

References (30)

1. Nugteren H W, Moreno N, Sebastia E, Querol X. Determination of the Available Si and Al from Coal Fly Ashes under Alkaline Conditions with the Aim of Synthesizing Zeolites Products. Lexington, USA: Int. Ash Utilization Symposium, University of Kentuchy, Centre for Applied Energy Research, 2001, Paper No. 71
2. Adamczyk Z, Bialecka B. Hydrothermal synthesis of zeolites from polish coal fly ash. Polish Journal of Environmental Studies, 2005, 14(6): 713–719
3. Inada M, Eguchi Y, Enomoto N, Hojo J. Synthesis of zeolite from coal fly ashes with different silica-alumina composition. Fuel, 2005, 84(2–3): 299–304
4. Hollman G G, Steenbruggen G, Janssen-Jurkovicova M. A twosteps process for the synthesis of zeolites from coal fly ash. Fuel, 1999, 78(10): 1225–1230
5. Mimura H, Yokota K, Akiba K, Onodera Y. Alkali hydrothermal synthesis of zeolites from coal fly ash and their uptake properties of Cesium ion. Journal of Nuclear Science and Technology, 2001, 38 (9): 766–772
6. Murayama N, Yamamoto H, Shibata J. Mechanism of zeolite synthesis from coal fly ash by alkali hydrothermal reaction. International Journal of Mineral Processing, 2002, 64(1): 1–17
7. Singh D N, Kolay P K. Simulation of ash water interaction and its influence on ash characteristics. Progress in Energy and Combustion Science, 2002, 28(3): 267–299
8. Rayalu S S, Udhoji J S, Meshram S U, Naidu R R, Devotta S. Estimation of crystallinity in fly ash-based zeolite-A using XRD and IR spectroscopy. Research Communication. Current Science, 2005, 89(12): 2147–2151
9. Querol X, Moreno N, Uman J C, Alastuey A, Hernandez E, Lopez-Solar A, Plana F. Synthesis of zeolites from coal fly ash: an overview. International Journal of Coal Geology, 2002, 50(1–4): 413–423
10. Querol X, Moreno N, Alastuey A, Juan R, Andres J M, Lopez-Soler A, Ayora C, Medinaceli A, Valero A. Synthesis of high ion exchange zeolites from coal fly ash. Geologica Acta, 2007, 5(1): 49–57
11. Mortier W J. Zeolite electronegativity related to physicochemical properties. Journal of Catalysis, 1978, 55(2): 138–145
12. Li G. FT-IR studies of zeolite materials: characterization and environmental applications. Dissertation for the Doctoral Degree, Iowa City: University of Iowa, 2005
13. 2O ratio Part I: FTIR study. Microporous and Mesoporous Materials, 2007, 106(1–3): 180–191
14. Kumar P, Mal N, Oumi Y, Yamana K, Sano T. Mesoporous materials prepared using coal fly ash as the silicon and aluminum source. Journal of Materials Chemistry, 2001, 11(12): 3285–3290
15. Watek T T, Saito F, Zhang O. The effect of low solid/liquid ratio on hydrothermal synthesis of zeolites from fly ash. Fuel, 2008, 87(15–16): 3194–3199
16. Somerset V S, Petrik L F, White R A, Klink M J, Key D, Iwuoha E. The use of X-ray fluorescence (XRF) analysis in predicting the alkaline hydrothermal conversion of fly ash precipitates into zeolites. Talanta, 2004, 64(1): 109–114
17. Grutzeck M W, Siemer D D. Zeolites Synthesized from Class F fly ash and Sodium aluminate slurry. Journal of the American Ceramic Society, 1997, 80(9): 2449–2453
18. Ojha K, Pradhan N C, Samanta A N. Zeolite from fly ash synthesis and characterization. Bulletin of Materials Science, 2004, 27(6): 555–564
19. El-Naggar M R, El-Kamash A M, El-Dessouky M I, Ghonaim A K. Two-step methods for preparation of Na A-X zeolite blend from fly ash for removal of Cesium ions. Journal of Hazardous Materials, 2008, 154(1–3): 963–972
20. Scott J, Guang D, Naeramitmarnsuk K, Thabuot M, Amal R. Zeolite synthesis from coal fly ash for the removal of lead ions from aqueous solution. Journal of Chemical Technology and Biotechnology, 2002, 77(1): 63–69
21. Coates J. Interpretation of infrared spectra, a practical approach, encyclopedia of analytical chemistry. In: Meyers R A, ed. Encyclopedia of Analytical Chemistry. Chichester, USA: John Wiley & Sons Ltd., 2000, 10815–10837
22. 2 solutions. Fuel, 2006, 85(3): 360–366
23. Jacobs P A, Mortier W J. An attempt to rationalize stretching frequencies of lattice hydroxyl groups in hydrogen zeolites. Zeolite, 1982, 2(3): 226–230
24. Da-Ming S. An analysis of the structure of 13X molecular sieve in ion exchange. Vacuum, 1993, 44(2): 75–78
25. Da-Ming S. Dependence of X zeolite adsorption properties on electronegativity and vibration frequency. Vacuum, 1994, 45(12): 1175–1179
26. Jha B, Singh D N. A review on synthesis, characterization and industrial application of fly ash zeolites. Journal of Material Education, 2011, 33(1–2): 65–132
27. Jha B, Singh D N. Zeolitization characteristics of fly ashes from wetand dry-disposal systems. Acta Geotechnica Slovenica, 2012, 9(2): 63–71
28. Singh D N, Jha B, Srinivas K. Determination of crystallinity of alkali activated fly ash by XRD and FTIR studies. In: Yang Q, Zhang J M, Zheng H, Yao Y, eds. Constitutive Modeling of Geomaterials.: Springer Series in Geomechanics and Geoengineering. Beijing: Tsinghua University, 2013, 477–481
29. ASTM International. ASTM Standard C618-12a, Standard specification for coal fly ash and raw or calcined natural pozzolan for use in concrete. West Conshohocken, PA: ASTM International, 1994
30. ICDD. Powder diffraction file inorganic and organic data book, Set 60. In: Kabekkodu S, ed. International Centre for Diffraction Data. Newtown Square, PA USA: ICDD, 2010