Fluid distribution and pore wettability of monolithic carbon xerogels measured by 1H NMR relaxation

Carbon

Volumn 68, Issue , 2014, Pages 542-552

  Bardenhagen, Ingo ^a,b   Dreher, Wolfgang ^b   Fenske, Daniela ^a   Wittstock, Arne ^b   Bäumer, Marcus ^b  

^a FRAUNHOFER INSTITUTE FOR MANUFACTURING TECHNOLOGY AND ADVANCED MATERIALS IFAM   (Germany)

^b UNIVERSITY OF BREMEN   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

DIFFERENT SIZES; DIMETHYL SULFOXIDE (DMSO); ELECTRODE PERFORMANCE; FLUID DISTRIBUTION; GAS DIFFUSION ELECTRODES; NON-UNIFORM DISTRIBUTION; POROUS STRUCTURES; RELAXATION STRENGTH;

DIFFUSION IN LIQUIDS; DIMETHYL SULFOXIDE; ORGANIC SOLVENTS; POROSITY; CARBON; DIFFUSION IN GASES; ELECTRODES; PORE SIZE; XEROGELS;

WETTING;

EID: 84891558652     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carbon.2013.11.033     Document Type: Article

References (30)

1. J. Han, J. Fu, and R.B. Schoch Molecular sieving using nanofilters: past, present and future Lab Chip 8 1 2007 23
2. A. Wittstock, J. Biener, J. Erlebacher, and M. Bäumer Nanoporous Gold: From an Ancient Technology to a Novel Material 2012 RSC Oxfordshire
3. M. Mirzaeian, and P.J. Hall Characterizing capacity loss of lithium oxygen batteries by impedance spectroscopy J Power Sources 195 19 2010 6817 6824
4. C. Tran, X. Yang, and D. Qu Investigation of the gas-diffusion-electrode used as lithium/air cathode in non-aqueous electrolyte and the importance of carbon material porosity J Power Sources 195 7 2010 2057 2063
5. R. Padbury, and X. Zhang Lithium-oxygen batteries-Limiting factors that affect performance J Power Sources 196 10 2011 4436 4444
6. R.W. Pekala Organic aerogels from the polycondensation of resorcinol with formaldehyde J Mater Sci 24 9 1989 3221 3227
7. S. Al-Muhtaseb, and J. Ritter Preparation and properties of resorcinol-formaldehyde organic and carbon gels Adv Mater 15 2 2003 101 114
8. X. Yang, P. He, and Y. Xia Preparation of mesocellular carbon foam and its application for lithium/oxygen battery Electrochem Commun 11 6 2009 1127 1130
9. 2 and Li-S batteries with high energy storage Nat Mater 11 1 2011 19 29
10. J. Howard Quantitative estimates of porous media wettability from proton NMR measurements Magn Reson Imaging 16 5-6 1998 529 533
11. A. Watson, and C. Chang Characterizing porous media with NMR methods Prog Nucl Magn Reson Spectrosc 31 4 1997 343 386
12. K. Brownstein, and C. Tarr Spin-lattice relaxation in a system governed by diffusion J Magn Reson (1969) 26 1 1977 17 24
13. B. Boddenberg, R. Haul, and G. Oppermann Surface diffusion and NMR relaxation times of benzene adsorbed on modified silica surfaces Adv Mol Relax Processes 3 1-4 1972 61 74
14. S. Chen, H. Liaw, and A.T. Watson Fluid saturation-dependent nuclear magnetic resonance spin-lattice relaxation in porous media and pore structure analysis J Appl Phys 74 3 1993 1473
15. F. D'Orazio, S. Bhattacharja, W. Halperin, K. Eguchi, and T. Mizusaki Molecular diffusion and nuclear-magnetic-resonance relaxation of water in unsaturated porous silica glass Phys Rev B 42 16 1990 9810 9818
16. S. Bhattacharja, F. D'Orazio, J.C. Tarczon, W.P. Halperin, and R. Gerhardt Internal structure of porous silica: a model system for characterization by nuclear magnetic resonance J Am Ceram Soc 72 11 1989 2126 2130
17. M. Simina, R. Nechifor, and I. Ardelean Saturation-dependent nuclear magnetic resonance relaxation of fluids confined inside porous media with micrometer-sized pores Magn Reson Chem 49 6 2011 314 319
18. 1H spin-lattice relaxation as a fingerprint of porous media Magn Reson Imaging 8 4 1990 435 447
19. 2 cells J Am Chem Soc 135 1 2013 494 500
20. P.C. Hansen The L-curve and its use in the numerical treatment of inverse problems P. Johnston, Computational Inverse Problems in Electrocardiology 2001 WIT Press Southampton 119 142
21. E. Sternin Use of Inverse Theory Algorithms in the Analysis of Biomembrane NMR Data JM Walker, AM Dopico, Methods in Membrane Lipids Vol. 400 2007 Humana Press (Methods in Molecular Biology™) Totowa, NJ 103 125
22. Chen S, Li R, Yu J, Wang H, Zhang X. Study of Uncertainities in the Inversion Algorithms for Transverse Relaxation Distribution, 4th International Conference on Bioinformatics and Biomedical Engineering. Chengdu, China; 2010; p. 1-4.
23. C. Alegre, D. Sebastián, E. Baquedano, M.E. Gálvez, R. Moliner, and M. Lázaro Tailoring synthesis conditions of carbon xerogels towards their utilization as Pt-catalyst supports for oxygen reduction reaction (ORR) Catalysts 2 4 2012 466 489
24. M. Matthews, M. Pimenta, G. Dresselhaus, M. Dresselhaus, and M. Endo Origin of dispersive effects of the Raman D band in carbon materials Phys Rev B 59 10 1999 R6585
25. A.C. Ferrari, and J. Robertson Raman spectroscopy of amorphous, nanostructured, diamond-like carbon, and nanodiamond Philos Trans R Soc A 2004 362 1824 2477 2512
26. K. McCall, D. Johnson, and R. Guyer Magnetization evolution in connected pore systems Phys Rev B 44 14 1991 7344 7355
27. E. Grunewald, and R. Knight A laboratory study of NMR relaxation times and pore coupling in heterogeneous media Geophysics 74 6 2009 E215
28. P. Pacak Polarizability and molecular radius of dimethyl-sulfoxide and dimethylformamide from refractive index data J Solution Chem 16 1 1987 71 77
29. H. Schubert Kapillarität in porösen Feststoffsystemen 1982 Springer Berlin
30. H. Liaw, R. Kulkarni, S. Chen, and A.T. Watson Characterization of fluid distributions in porous media by NMR techniques AIChE J 42 2 1996 538 546