Evaluation of functionalized mesoporous silicas for reverse phase high performance liquid chromatography: An application for the separation of steroids

Microchemical Journal

Volumn 114, Issue , 2014, Pages 53-58

  Gañán, Judith ^a   Morante Zarcero, Sonia ^a   Pérez Quintanilla, Damián ^a   Sierra, Isabel ^a  

^a UNIVERSIDAD REY JUAN CARLOS   (Spain)

Author keywords

Functionalized mesoporous silica; High performance liquid chromatography; Reversed phase column; Steroids

Indexed keywords

EID: 84891085138     PISSN: 0026265X     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.microc.2013.12.003     Document Type: Article

References (15)

1. Sierra I., Pérez-Quintanilla D. Heavy metal complexation on hybrid mesoporous silicas: an approach to analytical applications. Chem. Soc. Rev. 2013, 42:3792-3807.
2. Van Der Voort P., Esquivel D., De Canck E., Goethals F., Van Driessche I., Romero-Salguero F.J. Periodic mesoporous organosilicas: from simple to complex bridges; a comprehensive overview of functions, morphologies and applications. Chem. Soc. Rev. 2013, 42:3913-3955.
3. Ide M., Wallaert E., Van Driessche I., Lynen F., Sandra P., Van Der Voort P. Spherical mesoporous silica particles by spray drying: doubling the retention factor of HPLC columns. Microporous Mesoporous Mater. 2011, 14:282-291.
4. Galarneau A., Iapichella J., Bonhomme K., Di Renzo F., Kooyman P., Teresaki O., Fajula F. Controlling the morphology of mesostructured silicas by pseudomorphic transformation: a route towards applications. Adv. Funct. Mater. 2006, 16:1657-1667.
5. Yasmin T., Müller K. Synthesis and surface modification of mesoporous mcm-41 silica material. J. Chromatogr. A 2010, 1217:3362-3374.
6. Yang L., Wang Y., Luo G., Dai Y. Preparation and functionalization of mesoporous silica spheres as packing materials for HPLC. Particuology 2008, 6:143-148.
7. Wan H., Liu L., Li C., Xue X., Liang X. Facile synthesis of mesoporous SBA-15 silica spheres and its application for high-performance liquid chromatography. J. Colloid Interface Sci. 2009, 337:420-426.
8. Zhang Y., Jin Y., Yu H., Dai P., Ke Y., Liang X. Pore expansion of highly monodisperse phenylene-bridged organosilica spheres for chromatographic application. Talanta 2009, 81:824-830.
9. Chen S., Zhang X., Han Q., Ding M.Y. Synthesis of highly dispersed mesostructured cellular foam silica sphere and its application in high-performance liquid chromatography. Talanta 2012, 101:396-404.
10. Ma Y., Qi L., Ma J., Wu Y., Liu O., Cheng H. Large-pore mesoporous silica spheres: synthesis and application in HPLC. Colloids Surf. A 2003, 229:1-8.
11. Zhu G., Yang Q., Yang J., Zhang L., Li Y., Li C. Synthesis of bifunctionalized mesoporous organosilica spheres for high-performance liquid chromatography. J. Chromatogr. A 2006, 1103:257-264.
12. Ide M., El-Roz M., De Canck E., Vicente A., Plankaert T., Bogaerts T., Van Driessche I., Lynen F., Van Speybroeck V., Thybault-Starzyk F., Van Der Voort P. Quantification of silanol sites for the most common mesoporous ordered silicas and organosilicas: total versus accessible silanols. Phys. Chem. Chem. Phys. 2013, 15:642-650.
13. Li C., Hao W., Yan F., Su M. Aminopropyl-functionalized ethane-bridged periodic mesoporous organosilica spheres: preparation and application in liquid chromatography. J. Chromatogr. A 2011, 121:408-415.
14. Meyer V.R. Practical High-Performance Liquid Chromatography 2004, Wiley-VCH, Switzerland.
15. Ko J.H., Baik Y.S., Park S.T., Cheong W.J. Ground, sieved and C18 modified silica particles for packing material of microcolumn hig-performance liquid chormatography. J. Chromatogr. A 2007, 1144:269-274.