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3. 19,577 reflections were measured with ω-scans, in the range of 1.91 ≤ θ ≤ 25.00 (- 24 < = h < = 25, - 12 < = k < = 12, - 26 < = l < = 15), 4235 independent reflections (Rint = 0.1603). Final R1 = 0.0769, wR2 = 0.1749 [I > 2σ (I)], and the goodness-of-fit on F2 is 1.014. CCDC reference no. is 950580. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge, CB21EZ, UK (fax: + 44-1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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