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Volumn 229, Issue 1-3, 2013, Pages 13-20

Profiling counterfeit Cialis, Viagra and analogs by UPLC-MS

Author keywords

Chemical profile; Cialis1 ; Counterfeit medicines; Mass spectrometry; Ultra performance liquid chromatography; Viagra1

Indexed keywords

COUNTERFEIT DRUG; LAZAR; LIBIDEN; MAXFIL; METHANOL; PHOSPHODIESTERASE V INHIBITOR; PLENOVIT; POTENT 75; PRAMIL; PRAMIL 75; SILDENAFIL; TADALAFIL; UNCLASSIFIED DRUG; VIMAX;

EID: 84886936389     PISSN: 03790738     EISSN: 18726283     Source Type: Journal    
DOI: 10.1016/j.forsciint.2013.03.024     Document Type: Article
Times cited : (24)

References (24)
  • 1
    • 79955478694 scopus 로고    scopus 로고
    • Analytical challenges in drug counterfeiting and falsification - the NMR approach
    • U. Holzgrabe, M. Malet-Martino, Analytical challenges in drug counterfeiting and falsification - the NMR approach, J. Pharm. Biomed. Anal. 55 (2011) 679-687.
    • (2011) J. Pharm. Biomed. Anal. , vol.55 , pp. 679-687
    • Holzgrabe, U.1    Malet-Martino, M.2
  • 2
    • 85168049157 scopus 로고    scopus 로고
    • Surveillance Agency (ANVISA), Counterfeit Medicines, Ministry of Health, Brasilia
    • Surveillance Agency (ANVISA), Counterfeit Medicines, Ministry of Health, Brasilia, 2008 http://www.anvisa.gov.br/medicamentos/falsificados/index.htm.
    • (2008)
  • 4
    • 0034744118 scopus 로고    scopus 로고
    • Determinaton of sildenafil citrate and related substances in the commercial products and tablet dosage form using HPLC
    • N. Daraghmeh, M. Al-Omari, A.A. Badwan, A.M.Y. Jaber, Determinaton of sildenafil citrate and related substances in the commercial products and tablet dosage form using HPLC, J. Pharm. Biomed. Anal. 25 (2001) 483-492.
    • (2001) J. Pharm. Biomed. Anal. , vol.25 , pp. 483-492
    • Daraghmeh, N.1    Al-Omari, M.2    Badwan, A.A.3    Jaber, A.M.Y.4
  • 5
    • 0037053811 scopus 로고    scopus 로고
    • Extractive spectrophotometric methods for the assay of sildenafil citrate (Viagra) in pure form and in pharmaceutical formulations
    • N. Dinesh, P. Nagaraja, N.M. Gowda, K.S. Rangappa, Extractive spectrophotometric methods for the assay of sildenafil citrate (Viagra) in pure form and in pharmaceutical formulations, Talanta 57 (2002) 757-764.
    • (2002) Talanta , vol.57 , pp. 757-764
    • Dinesh, N.1    Nagaraja, P.2    Gowda, N.M.3    Rangappa, K.S.4
  • 6
    • 8144221420 scopus 로고    scopus 로고
    • Determination of tadalafil in pharmaceutical preparation by HPLC using monolithic silica column
    • H. Aboul-Enein, I. Ali, Determination of tadalafil in pharmaceutical preparation by HPLC using monolithic silica column, Talanta 65 (2005) 276-280.
    • (2005) Talanta , vol.65 , pp. 276-280
    • Aboul-Enein, H.1    Ali, I.2
  • 7
    • 23644439778 scopus 로고    scopus 로고
    • 1H 13C, 15N NMR analysis of sildenafil base and citrate (Viagra) in solution, solid state and pharmaceutical dosage forms
    • I. Wawer, M. Pisklak, Z. Chilmonczyk, 1H 13C, 15N NMR analysis of sildenafil base and citrate (Viagra) in solution, solid state and pharmaceutical dosage forms, J. Pharm. Biomed. Anal. 38 (2005) 865-870.
    • (2005) J. Pharm. Biomed. Anal. , vol.38 , pp. 865-870
    • Wawer, I.1    Pisklak, M.2    Chilmonczyk, Z.3
  • 8
    • 32944463014 scopus 로고    scopus 로고
    • D. de Kaste, Screening suspected counterfeit Viagra and imitations of Viagra with near-infrared spectroscopy
    • M.J. Vredenbregt, L. Blok-Tip, R. Hoogerbrugge, D.M. Barends, D. de Kaste, Screening suspected counterfeit Viagra and imitations of Viagra with near-infrared spectroscopy, J. Pharm. Biomed. Anal. 40 (2006) 840-849.
    • (2006) J. Pharm. Biomed. Anal. , vol.40 , pp. 840-849
    • Vredenbregt, M.J.1    Blok-Tip, L.2    Hoogerbrugge, R.3    Barends, D.M.4
  • 9
    • 33847123253 scopus 로고    scopus 로고
    • The usefulness of simple X-ray powder diffraction analysis for counterfeit control - the Viagra example
    • J. Maurin, F. Plucinski, A. Mazurek, Z. Fijalek, The usefulness of simple X-ray powder diffraction analysis for counterfeit control - the Viagra example, J. Pharm. Biomed. Anal. 43 (2007) 1514-1518.
    • (2007) J. Pharm. Biomed. Anal. , vol.43 , pp. 1514-1518
    • Maurin, J.1    Plucinski, F.2    Mazurek, A.3    Fijalek, Z.4
  • 11
    • 58149279469 scopus 로고    scopus 로고
    • Strategies for characterizing sildenafil, vardenafil, tadalafil and their analogues in herbal dietary supplements, and detecting counterfeit products containing these drugs
    • S. Singh, B. Prasad, A. Savaliya, R. Shah, V. Gohil, A. Kaur, Strategies for characterizing sildenafil, vardenafil, tadalafil and their analogues in herbal dietary supplements, and detecting counterfeit products containing these drugs, Trends Anal. Chem. 28 (2009) 13-28.
    • (2009) Trends Anal. Chem. , vol.28 , pp. 13-28
    • Singh, S.1    Prasad, B.2    Savaliya, A.3    Shah, R.4    Gohil, V.5    Kaur, A.6
  • 12
    • 41549127581 scopus 로고    scopus 로고
    • Analysis of illegally manufactured formulations of tadalafil (cialis) by 1H NMR, 2D DOSY 1H NMR and Raman spectroscopy
    • S. Trefi, C. Routaboul, S. Hamieh, V. Gilard, M. Malet-Martino, R. Martino, Analysis of illegally manufactured formulations of tadalafil (cialis) by 1H NMR, 2D DOSY 1H NMR and Raman spectroscopy, J. Pharm. Biomed. Anal. 47 (2008) 103-113.
    • (2008) J. Pharm. Biomed. Anal. , vol.47 , pp. 103-113
    • Trefi, S.1    Routaboul, C.2    Hamieh, S.3    Gilard, V.4    Malet-Martino, M.5    Martino, R.6
  • 15
    • 77950178011 scopus 로고    scopus 로고
    • Determinaçaõ de citrato de sildenafila e de tadalafila por cromatografia líquida de ultraeficiência com detecçaõ por arranjo de diodos (CLUE-DAD)
    • R.S. Ortiz, M.V. Antunes, R. Linden, Determinaçaõ de citrato de sildenafila e de tadalafila por cromatografia líquida de ultraeficiência com detecçaõ por arranjo de diodos (CLUE-DAD), Química Nova 33 (2010) 389-393.
    • (2010) Química Nova , vol.33 , pp. 389-393
    • Ortiz, R.S.1    Antunes, M.V.2    Linden, R.3
  • 16
    • 30744464832 scopus 로고    scopus 로고
    • Simultaneous determination of synthetic phosphodiesterase-5 inhibitors found in a dietary supplement and pre-mixed bulk powders for dietary supplements using high-performance liquid chromatography with diode array detection and liquid chromatography-electrospray ionization tandem mass spectrometry
    • P. Zou, S.S. Oh, P. Hou, M. Low, H. Koh, Simultaneous determination of synthetic phosphodiesterase-5 inhibitors found in a dietary supplement and pre-mixed bulk powders for dietary supplements using high-performance liquid chromatography with diode array detection and liquid chromatography-electrospray ionization tandem mass spectrometry, J. Chromatogr. A 1104 (2006) 113-122.
    • (2006) J. Chromatogr. A , vol.1104 , pp. 113-122
    • Zou, P.1    Oh, S.S.2    Hou, P.3    Low, M.4    Koh, H.5
  • 18
    • 84875579391 scopus 로고    scopus 로고
    • Chemical fingerprinting of counterfeits of Viagra and Cialis tablets and analogues via electrospray ionization mass spectrometry
    • R.S. Ortiz, K.C. Mariotti, W. Romaõ, M.N. Eberlin, R.P. Limberger, P. Mayorga, Chemical fingerprinting of counterfeits of Viagra and Cialis tablets and analogues via electrospray ionization mass spectrometry, Am. J. Anal. Chem. 2 (2011) 919-928.
    • (2011) Am. J. Anal. Chem. , vol.2 , pp. 919-928
    • Ortiz, R.S.1    Mariotti, K.C.2    Romaõ, W.3    Eberlin, M.N.4    Limberger, R.P.5    Mayorga, P.6
  • 19
    • 66849099833 scopus 로고    scopus 로고
    • Recent Developments in Counterfeits and Imitations of Viagra, Cialis and Levitra: a 2005-2006 Update
    • National Institute for Public Health and the Environment (RIVM), Bilthoven, The Netherlands
    • B.J. Venhuis, D.M. Barends, M.E. Zwaagstra, D. de Kaste, Recent Developments in Counterfeits and Imitations of Viagra, Cialis and Levitra: a 2005-2006 Update, National Institute for Public Health and the Environment (RIVM), Bilthoven, The Netherlands, 2007.
    • (2007)
    • Venhuis, B.J.1    Barends, D.M.2    Zwaagstra, M.E.3    de Kaste, D.4
  • 20
    • 77951262876 scopus 로고    scopus 로고
    • Fingerprinting of yogurt products by laser desorption spray post-ionization mass spectrometry
    • J. Liu, B. Qiu, H. Luo, Fingerprinting of yogurt products by laser desorption spray post-ionization mass spectrometry, Rapid Commun. Mass Spectrom. 24 (2010) 1365-1370.
    • (2010) Rapid Commun. Mass Spectrom. , vol.24 , pp. 1365-1370
    • Liu, J.1    Qiu, B.2    Luo, H.3
  • 21
    • 77956233739 scopus 로고    scopus 로고
    • Fast screening and secure confirmation of milk powder adulteration with maltodextrin via electrospray ionization-mass spectrometry [ESI(+)-MS] and selective enzymatic hydrolysis
    • G.B. Sanvido, J.S. Garcia, Y.E. Corilo, B.G. Vaz, J.J. Zacca, R.G. Cosso, M.N. Eberlin, M.G. Peter, Fast screening and secure confirmation of milk powder adulteration with maltodextrin via electrospray ionization-mass spectrometry [ESI(+)-MS] and selective enzymatic hydrolysis, J. Agric. Food Chem. 58 (2010) 9407-9412.
    • (2010) J. Agric. Food Chem. , vol.58 , pp. 9407-9412
    • Sanvido, G.B.1    Garcia, J.S.2    Corilo, Y.E.3    Vaz, B.G.4    Zacca, J.J.5    Cosso, R.G.6    Eberlin, M.N.7    Peter, M.G.8
  • 22
    • 77949985719 scopus 로고    scopus 로고
    • The Analysis of excipients in Ecstasy tablets and their contribuition in a drug profiling context
    • These de Doctorat, Universite de Lausanne, Faculte de Droit et des Sciences Criminelles, Institut de Police Scientifique
    • I. Baer, The Analysis of excipients in Ecstasy tablets and their contribuition in a drug profiling context, These de Doctorat, Universite de Lausanne, Faculte de Droit et des Sciences Criminelles, Institut de Police Scientifique, 2007.
    • (2007)
    • Baer, I.1
  • 24
    • 44749083713 scopus 로고    scopus 로고
    • 4th ed., 1st Supplement, Monographs: Dosage forms: General monographs: Tablets, World Health Organization, Geneva
    • The International Pharmacopoea, 4th ed., 1st Supplement, Monographs: Dosage forms: General monographs: Tablets, World Health Organization, Geneva, 2008.
    • (2008) The International Pharmacopoea


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.