Characterization of NIST food-matrix standard reference materials for their vitamin C content

Analytical and Bioanalytical Chemistry

Volumn 405, Issue 13, 2013, Pages 4539-4548

  Thomas, Jeanice B ^a   Yen, James H ^a   Sharpless, Katherine E ^a  

^a NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

Author keywords

Absorbance detection; Ascorbic acid; Food; Liquid chromatography; Reference material; Standard reference material

Indexed keywords

ASCORBIC ACID; CEREAL PRODUCTS; DAIRIES; FATTY ACIDS; FOOD PRODUCTS; QUALITY ASSURANCE;

ABSORBANCE DETECTION; BREAKFAST CEREALS; FOOD-MATRIX STANDARDS; MEASUREMENT TRACEABILITY; NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY; REFERENCE MATERIAL; STANDARD REFERENCE MATERIAL; VITAMIN C CONTENTS;

LIQUID CHROMATOGRAPHY;

ASCORBIC ACID;

ARTICLE; DIET SUPPLEMENTATION; ELEMENTAL DIET; HUMAN; INFANT; LIQUID CHROMATOGRAPHY; QUALITY CONTROL; REFERENCE VALUE; REPRODUCIBILITY; STANDARD;

ASCORBIC ACID; CHROMATOGRAPHY, LIQUID; DIETARY SUPPLEMENTS; FOOD, FORMULATED; HUMANS; INFANT; QUALITY CONTROL; REFERENCE STANDARDS; REFERENCE VALUES; REPRODUCIBILITY OF RESULTS;

EID: 84885942793     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-013-6891-4     Document Type: Article

References (27)

1. Office of Dietary Supplements/National Institutes of Health Dietary Supplement Fact Sheet: Vitamin C. http://ods.od.nih.gov/factsheets/vitaminc- HealthProfessional/. Accessed April 2012
2. Jacob RA, SotoudehG(2002)Vitamin C function and status in chronic disease. Nutr Clin Care 5:66-74. http://www.ncbi.nlm.nih.gov/pubmed/12134712
3. United States Department of Agriculture National Nutrient Database for Standard Reference, Release 24. https://www.ars.usda.gov/SP2UserFiles/Place/ 12354500/Data/SR24/nutrlist/sr24a401.pdf
4. Food and Nutrition Board, Institute of Medicine, National Academies, Dietary Reference Intakes: Vitamins. http://www.iom.edu/Activities/Nutrition/ SummaryDRIs/-/media/Files/Activity%20Files/Nutri t ion/DRIs/New%20Material/7- %20Nutrients%20Summary.pdf
5. United States Food and Drug Administration, Code of Federal Regulations Title 21: 21CFR101.54. http://www.accessdata.fda.gov/scripts/cdrh/cfdocs/cfCFR/ CFRSearch.cfm?fr=101.54&utm-campaign=Google2&utm-source= fdaSearch&utm-medium=website&utm-term=antioxidant%20label&utm- content=5
6. Sharpless KE, Gill LM, Margolis SA, Wise SA, Elkins E (1999) Preparation of standard reference material 2383 baby food composite and use of an interlaboratory comparison exercise for value assignment of its nutrient concentrations. JAOAC Int 82:276-287
7. Sharpless KE, Thomas JB, Christopher SJ, Greenberg RR, Sander LC, SchantzMM,WelchMJ,Wise SA (2007) Standard referencematerials for foods and dietary supplements. Anal Bioanal Chem 389:171-178
8. Certificate of Analysis, Standard Reference Material 2385 Slurried Spinach (2003) Gaithersburg, MD, USA, Standard Reference Materials Program, National Institute of Standards and Technology. http://www.nist.gov/srm
9. Certificate of Analysis, Standard Reference Material 1549a Whole Milk Powder (2013) Gaithersburg, MD, USA; Standard Reference Materials Program, National Institute of Standards and Technology
10. Certificate of Analysis, Standard Reference Material 1849 Infant/Adult Nutritional Formula (2010) Gaithersburg, MD, USA; Standard Reference Materials Program, National Institute of Standards and Technology. http://www.nist.gov/srm
11. Certificate of Analysis, Standard Reference Material 1849a Infant/Adult Nutritional Formula (2012) Gaithersburg, MD, USA; Standard Reference Materials Program, National Institute of Standards and Technology. http://www.nist.gov/srm
12. Sharpless KE, Lindstrom RM, Nelson BC, Phinney KW, Ca R, Sander LC, Schantz MM, Spatz RO, Thomas JB, Turk GC, Wise SA, Wood LJ (2010) Preparation and characterization of standard reference material 1849 Infant/Adult Nutritional Formula. J AOAC INTERNATIONAL 93(4):1262-1274
13. Certificate of Analysis, Standard Reference Material 3233 Fortified Breakfast Cereal (2013) Gaithersburg, MD, USA; Standard Reference Materials Program, National Institute of Standards and Technology.
14. Wolf WR (1993) In: Sullivan DM, Carpenter DE (eds) Methods of analysis for nutrition labeling. AOAC International, Arlington, pp 111-122
15. Wolf WR, Andrews KW (1995) Fresenius J Anal Chem 352:73-76
16. Sharpless KE, Schiller SB, Margolis SA, Thomas JB, Iyengar GV, Colbert JC, Gills TE, Wise SA, Tanner JT, Wolf WR (1997) Certification of nutrients in standard reference material 1846: infant formula. JAOAC Int 80:611-621
17. Margolis SA, Schapira RM (1997) Liquid chromatographic measurement of L-ascorbic and D-ascorbic acid in biological samples. J Chromatogr B 690:25-33
18. Washko PW, Welch RW, Dhariwal KR, Wang Y, Levine M (1992) Anal Biochem 204:1-14
19. Sander LC, Sharpless KE, Wise SA, Nelson BC, Phinney KW, Porter BJ, Rimmer CA, Thomas JB, Wood LJ, Yen JH, Duewer DL, Atkinson R, Chen P, Goldschmidt R, Wolf WR, Ho I-P, Betz JM (2011) Anal Chem 83:99-108
20. Thomas JB, Sharpless KE, Yen JH, Rimmer CA (2011) J AOAC INTERNATIONAL 94:815-822
21. Phinney KW, Rimmer CA, Thomas JB, Sander LC, Sharpless KE, Wise SA (2011) Anal Chem 83:92-98
22. May W, Parris R, Beck II C, Fassett J, Greenberg R, Guenther F, Kramer G, Wise S, Gills T, Colbert J, Gettings R, MacDonald B (2000) Definition of Terms and Modes Used at NIST for Value-Assignment of Reference Materials for Chemical Measurements, NIST Special Publication 260-136. http://www.nist.gov/srm/upload/ SP260-136.PDF
23. Thompson A, Taylor BN (2008) Guide for the Use of the International System of Units (SI), NIST Special Publication 811, U.S. Government Printing Office, Washington, DC. http://www.nist.gov/pml/pubs/sp811/index.cfm
24. JCGM 100 (2008) Evaluation of measurement data-guide to the expression of uncertainty in measurement (ISO GUM 1995 with Minor Corrections); Joint Committee for Guides in Metrology. http://www.bipm.org/utils/common/documents/ jcgm/JCGM-100- 2008-E.pdf. Accessed Jan 2012;
25. see also Taylor BN and Kuyatt CE (1994) Guidelines for evaluating and expressing the uncertainty of NIST measurement results; NIST technical note 1297, U.S. Government Printing Office, Washington, DC. http://www.nist.gov/pml/ pubs
26. JCGM 101(2008) Evaluation of measurement data-supplement 1 to the guide to expression of uncertainty in measurement; propagation of distributions using a Monte Carlo method, Joint Committee for Guides in Metrology (BIPM, IEC, IFCC, ILAC, ISO, IUPAC, IUPAP and OIML), International Bureau of Weights and Measures (BIPM), Sèvres, France. http://www.bipm.org/utils/common/documents/jcgm/ JCGM-101-2008-E.pdf
27. Efron B, Tibshirani RJ (1993) An Introduction to the bootstrap. Chapman & Hall, London