A battery-driven, low-field NMR unit for thermally and hyperpolarized samples

Magnetic Resonance Materials in Physics, Biology and Medicine

Volumn 26, Issue 5, 2013, Pages 491-499

  Borowiak, Robert ^a   Schwaderlapp, Niels ^a   Huethe, Frank ^a   Lickert, Thomas ^a   Fischer, Elmar ^a   Bär, Sébastien ^a   Hennig, Jürgen ^a   Von Elverfeldt, Dominik ^a   Hövener, Jan Bernd ^a  

^a UNIVERSITY OF FREIBURG   (Germany)

Author keywords

Hyperpolarization; Low field NMR; NMR; Parahydrogen; PASADENA; PHIP; SABRE

Indexed keywords

SOLENOIDEA;

HYDROGEN;

ARTICLE; CHEMISTRY; COMPUTER PROGRAM; EQUIPMENT; EQUIPMENT DESIGN; HEAT; MAGNETIC FIELD; MAGNETISM; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POWER SUPPLY; REPRODUCIBILITY; SIGNAL PROCESSING; TIME;

ELECTRIC POWER SUPPLIES; EQUIPMENT DESIGN; HOT TEMPERATURE; HYDROGEN; MAGNETIC FIELDS; MAGNETIC RESONANCE SPECTROSCOPY; MAGNETICS; REPRODUCIBILITY OF RESULTS; SIGNAL PROCESSING, COMPUTER-ASSISTED; SOFTWARE; TIME FACTORS;

EID: 84885613770     PISSN: 09685243     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10334-013-0366-7     Document Type: Article

References (42)

1. Savukov IM, Seltzer SJ, Romalis MV (2007) Detection of NMR signals with a radio-frequency atomic magnetometer. J Magn Reson 185(2):214-220
2. Asfour A, Hyacinte J-N, Leviel J-L (2006) Development of a fully digital and low-frequency NMR system for polarization measurement of hyperpolarized gases. In: Proceedings of the IEEE instrumentation and measurement technology conference, pp 1839-1843
3. Asfour A (2008) A new DAQ-based and versatile low-cost NMR spectrometer working at very-low magnetic field (4.5 mT): a palette of potential applications. In: IEEE instrumentation and measurement technology conference proceedings, pp 697-701
4. Parnell SR, Boag S, McKetterick TJ, Wild JM (2011) Low magnetic field manipulation of 3He spins using digital methods. J Phys Conf Ser 294:012010
5. Parnell SR, Woolley EB, Boag S, Frost CD (2008) Digital pulsed NMR spectrometer for nuclear spin-polarized 3He and other hyperpolarized gases. Meas Sci Technol 19(4):045601
6. McDermott R, Trabesinger AH, Mück M, Hahn EL, Pines A, Clarke J (2002) Liquid-state NMR and scalar couplings in microtesla magnetic fields. Science 295(5563):2247-2249
7. Glöggler S, Blümich B, Appelt S (2012) NMR spectroscopy for chemical analysis at low magnetic fields. In: Topics in current chemistry, Springer, Berlin, pp 1-22
8. Appelt S, Kühn H, Häsing FW, Blümich B (2006) Chemical analysis by ultrahigh-resolution nuclear magnetic resonance in the Earth's magnetic field. Nat Phys 2(2):105-109
9. Bidinosti CP, Choukeife J, Tastevin G, Nacher P-J, Vignaud A (2004) MRI of the lung using hyperpolarized 3He at very low magnetic field (3 mT). Magn Reson Mater Phys 16(6):255-258
10. Bouchiat MA, Carver TR, Varnum CM (1960) Nuclear polarization in He3 gas induced by optical pumping and dipolar exchange. Phys Rev Lett 5(8):373-375
11. Bachert P, Schad LR, Bock M, Knopp MV, Ebert M, Grobmann T, Heil W, Hofmann D, Surkau R, Otten EW (1996) Nuclear magnetic resonance imaging of airways in humans with use of hyperpolarized 3He. Magn Reson Med 36(2):192-196
12. Ruset IC, Ketel S, Hersman FW (2006) Optical pumping system design for large production of hyperpolarized {129}Xe. Phys Rev Lett 96(5):053002
13. Schröder L, Lowery TJ, Hilty C, Wemmer DE, Pines A (2006) Molecular imaging using a targeted magnetic resonance hyperpolarized biosensor. Science 314(5798):446-449
14. Abragam A, Goldman M (1978) Principles of dynamic nuclear-polarization. Rep Prog Phys 41(3):395-467
15. Comment A, Rentsch J, Kurdzesau F, Jannin S, Uffmann K, Van Heeswijk RB, Hautle P, Konter JA, Van den Brandt B, Van der Klink JJ (2008) Producing over 100 ml of highly concentrated hyperpolarized solution by means of dissolution DNP. J Magn Reson 194(1):152-155
16. Batel M, Krajewski M, Weiss K, With O, Däpp A, Hunkeler A, Gimersky M, Pruessmann KP, Boesiger P, Meier BH, Kozerke S, Ernst M (2012) A multi-sample 94 GHz dissolution dynamic-nuclear-polarization system. J Magn Reson 214:166-174
17. Ardenkjær-Larsen JH, Fridlund B, Gram A, Hansson G, Hansson L, Lerche MH, Servin R, Thaning M, Golman K (2003) Increase in signal-to-noise ratio of >10,000 times in liquid-state NMR. Proc Natl Acad Sci USA 100(18):10158-10163
18. Goldman M, Johannesson H (2005) Conversion of a proton pair para order into C-13 polarization by rf irradiation, for use in MRI. C R Physique 6(4-5):575-581
19. Goldman M, Johannesson H, Axelsson O, Karlsson M (2006) Design and implementation of C-13 hyperpolarization from para-hydrogen, for new MRI contrast agents. C R Chimie 9(3-4):357-363
20. Kadlecek S, Vahdat V, Nakayama T, Ng D, Emami K, Rizi R (2011) A simple and low-cost device for generating hyperpolarized contrast agents using parahydrogen. NMR Biomed 24(8):933-942
21. Callaghan PT, Eccles CD, Seymour JD (1997) An earth's field nuclear magnetic resonance apparatus suitable for pulsed gradient spin echo measurements of self-diffusion under Antarctic conditions. Rev Sci Instrum 68(11):4263-4270
22. Callaghan PT, Eccles CD (1996) NMR studies on antarctic sea ice. Bull Magn Reson 18:62-64
23. Waddell KW, Coffey AM, Chekmenev EY (2011) In situ detection of PHIP at 48 mT: demonstration using a centrally controlled polarizer. J Am Chem Soc 133(1):97-101
24. Chekmenev EY, Hövener J, Norton VA, Harris K, Batchelder LS, Bhattacharya P, Ross BD, Weitekamp DP (2008) PASADENA hyperpolarization of succinic acid for MRI and NMR spectroscopy. J Am Chem Soc 130(13):4212-4213
25. Hövener J-B, Chekmenev EY, Harris KC, Perman WH, Tran TT, Ross BD, Bhattacharya P (2009) Quality assurance of PASADENA hyperpolarization for 13C biomolecules. Magn Reson Mater Phy 22(2):123-134
26. Hövener J-B, Chekmenev E, Harris K, Perman WH, Robertson LH, Ross BD, Bhattacharya P (2009) PASADENA hyperpolarization of 13C biomolecules: equipment design and installation. Magn Reson Mater Phys 22(2):111-121
27. Dücker EB, Kuhn LT, Münnemann K, Griesinger C (2012) Similarity of SABRE field dependence in chemically different substrates. J Magn Reson 214:159-165
28. Adams RW, Duckett SB, Green RA, Williamson DC, Green GGR (2009) A theoretical basis for spontaneous polarization transfer in non-hydrogenative parahydrogen-induced polarization. J Chem Phys 131(19):194505-194515
29. Adams RW, Aguilar JA, Atkinson KD, Cowley MJ, Elliott PIP, Duckett SB, Green GGR, Khazal IG, López-Serrano J, Williamson DC (2009) Reversible interactions with para-hydrogen enhance NMR sensitivity by polarization transfer. Science 323(5922):1708-1711
30. Bowers CR, Weitekamp DP (1986) Transformation of symmetrization order to nuclear-spin magnetization by chemical-reaction and nuclear-magnetic-resonance. Phys Rev Lett 57(21):2645-2648
31. Bowers CR, Weitekamp DP (1987) Para-hydrogen and synthesis allow dramatically enhanced nuclear alignment. J Am Chem Soc 109(18):5541-5542
32. Natterer J, Bargon J (1997) Parahydrogen induced polarization. Prog Nucl Magn Reson Spectrosc 31:293-315
33. Kadlecek S, Emami K, Ishii M, Rizi R (2010) Optimal transfer of spin-order between a singlet nuclear pair and a heteronucleus. J Magn Reson 205(1):9-13
34. Bär S, Lange T, Leibfritz D, Hennig J, Elverfeldt DV, Hövener J-B (2012) On the Spin-order transfer from parahydrogen to another nucleus. J Magn Reson 225:25-35
35. Hövener J-B (2008) Strategies to prolong the T1 time of hyperpolarized molecules. In: Proceedings of the 16th scientific meeting, international society for magnetic resonance in medicine, Toronto, Canada, p 336
36. Bergeman T, Erez G, Metcalf HJ (1987) magentostatic trapping fields for neutral atoms. Phys Rev A 35(4):1535-1546
37. Friebolin H (1999) Ein Und Zwei Dim Nmr Spektroskopie 3 Auflage. Wiley-VCH
38. Levitt MH (2007) Spin dynamics. Wiley, Chichester
39. Hövener J-B, Bär S, Leupold J, Jenne K, Leibfritz D, Hennig J, Duckett SB, Von Elverfeldt D (2013) A continuous-flow, high-throughput, high-pressure parahydrogen converter for hyperpolarization in a clinical setting. NMR Biomed 26:124-131
40. Cowley MJ, Adams RW, Atkinson KD, Cockett MCR, Duckett SB, Green GGR, Lohman JAB, Kerssebaum R, Kilgour D, Mewis RE (2011) Iridium N-heterocyclic carbene complexes as efficient catalysts for magnetization transfer from para-hydrogen. J Am Chem Soc 133(16):6134-6137
41. Hoult D, Richards R (1976) The signal-to-noise ratio of the nuclear magnetic resonance experiment. J Magn Reson 24(1):71-85
42. Hoult DI (2009) The origins and present status of the radio wave controversy in NMR. Concept Magn Reson A 34A(4):193-216