Determination of parabens in waters by magnetically confined hydrophobic nanoparticle microextraction coupled to gas chromatography/mass spectrometry

Microchemical Journal

Volumn 110, Issue , 2013, Pages 643-648

  Alcudia Leon M C ^a   Lucena, R ^a   Cardenas S ^a   Valcarcel M ^a  

^a UNIVERSITY OF CÓRDOBA   (Spain)

Author keywords

Magnetically confined nanoparticles; Octadecyl silica; Parabens; Sea water; Swimming pool water

Indexed keywords

EID: 84883634676     PISSN: 0026265X     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.microc.2013.07.011     Document Type: Article

References (31)

1. Darbre P.D., Aljarrah A., Miller W.R., Coldham N.G., Sauer M.J., Pope G.S. Concentrations of parabens in human breast tumours. J. Appl. Toxicol. 2004, 24:5-13.
2. Darbre P.D. Underarm cosmetics and breast cancer. J. Appl. Toxicol. 2003, 23:89-95.
3. Darbre P.D., Harvey P.W. Paraben esters: review of recent studies of endocrine toxicity, absorption, esterase and human exposure, and discussion of potential human health risks. J. Appl. Toxicol. 2008, 28:561-578.
4. Routledge E.J., Parker J., Odum J., Ashby J., Sumpter J.P. Some alkyl hydroxyl benzoate preservatives (parabens) are estrogenic. Toxicol. Appl. Pharmacol. 1998, 153:12-19.
5. Golden R., Gandy J., Vollmer G. A review of the endocrine activity of parabens and implications for potential risks to human health. Crit. Rev. Toxicol. 2005, 35:435-458.
6. Brausch J.M., Rand G.M. A review of personal care products in the aquatic environment: environmental concentrations and toxicity. Chemosphere 2011, 82:1518-1532.
7. Canosa P., Rodríguez I., Rubí E., Cela R. Optimization of solid-phase microextraction conditions for the determination of triclosan and possible related compounds in water samples. J. Chromatogr. A 2005, 1072:107-115.
8. Canosa P., Rodríguez I., Rubí E., Bollaín M.H., Cela R. Optimisation of a solid-phase microextraction method for the determination of parabens in water samples at the low ng per litre level. J. Chromatogr. A 2006, 1124:3-10.
9. González-Mariño I., Quintana J.B., Rodríguez I., Cela R. Simultaneous determination of parabens, triclosan and triclocarban in water by liquid chromatography/electrospray ionisation tandem mass spectrometry. Rapid Commun. Mass Spectrom. 2009, 23:1756-1766.
10. Lee H.B., Peart T.E., Svoboda M.L. Determination of endocrine-disrupting phenols, acidic pharmaceuticals, and personal-care products in sewage by solid-phase extraction and gas chromatography-mass spectrometry. J. Chromatogr. A 2005, 1094:122-129.
11. Regueiro J., Llompart M., Psillakis E., García-Monteagudo J.C., García-Jares C. Ultrasound-assisted emulsification-microextraction of phenolic preservatives in water. Talanta 2009, 79:1387-1397.
12. González-Mariño I., Quintana J.B., Rodríguez I., Schrader S., Moeder M. Fully automated determination of parabens, triclosan and methyl triclosan in wastewater by microextraction by packed sorbents and gas chromatography-mass spectrometry. Anal. Chim. Acta 2011, 684:50-57.
13. Montes R., Rodríguez I., Rubí E., Cela R. Dispersive liquid-liquid microextraction applied to the simultaneous derivatization and concentration of triclosan and methyltriclosan in water samples. J. Chromatogr. A 2009, 1216:205-210.
14. Kasprzyk-Hordern B., Dinsdale R.M., Guwy A.J. The effect of signal suppression and mobile phase composition on the simultaneous analysis of multiple classes of acidic/neutral pharmaceuticals and personal care products in surface water by solid-phase extraction and ultra performance liquid chromatography-negative electrospray tandem mass spectrometry. Talanta 2008, 74:1299-1312.
15. Danovaro R., Bongiorni L., Corinaldesi C., Giovannelli D., Damiani E., Astolfi P., Greci L., Pusceddu A. Sunscreens cause coral bleaching by promoting viral infections. Environ. Health Perspect. 2008, 116:441-447.
16. Terasaki M., Makino M. Determination of chlorinated by-products of parabens in swimming pool water. Int. J. Environ. Anal. Chem. 2008, 88:911-922.
17. Pedrouzo M., Borrull F., Marce R.M., Pocurull E. Ultra-high performance liquid chromatography-tandem mass spectrometry for determining the presence of eleven personal care products in surface and wastewater. J. Chromatogr. A 2009, 1216:6994-7000.
18. Paxéus N. Organic pollutants in the effluents of large wastewater treatment plant in Sweden. Water Res. 1996, 30:1115-1122.
19. Eriksson E., Auffarth K., Eilersen A.M., Henze M., Ledin A. Household chemical and personal care products as sources for xenobiotic organic compounds in grey wastewater. Water SA 2003, 29:135-146.
20. Benijts T., Lambert W., De-Leenheer A. Analysis of multiple endocrine disruptors in environmental waters via wide-spectrum solid-phase extraction and dual-polarity ionization LC-ion trap-MS/MS. Anal. Chem. 2004, 76:704-711.
21. Benijts T., Günther W., Lambert W., De-Leenheer A. Sonic spray ionization applied to liquid chromatography/mass spectrometry analysis of endocrine-disrupting chemical in environmental water samples. Rapid Commun. Mass Spectrom. 2003, 17:1866-1872.
22. Canosa P., Rodríguez I., Rubí E., Negreira N., Cela R. Formation of halogenated by-products of parabens in chlorinated water. Anal. Chim. Acta 2006, 575:106-113.
23. Saraji M., Mirmahdieh S. Single-drop microextraction followed by in-syringe derivatization and GC-MS detection for the determination of parabens in water and cosmetic products. J. Sep. Sci. 2009, 32:988-995.
24. Villaverde-de-Saa E., González-Mariño I., Quintana J.B., Rodil R., Rodríguez I., Cela R. In-sample acetylation-non-porous membrane-assisted liquid-liquid extraction for the determination of parabens and triclosan in water samples. Anal. Bioanal. Chem. 2010, 397:2559-2568.
25. Alcudia-León M.C., Lucena R., Cárdenas S., Valcárcel M. Magnetically confined hydrophobic nanoparticles for the microextraction of endocrine-disrupting phenols from environmental waters. Anal. Bioanal. Chem. 2013, 405:2729-2734.
26. Jain R., Mudiam M.K.R., Chauhan A., Ch R., Murthy R.C., Khan H.A. Simultaneous derivatisation and preconcentration of parabens in food and other matrices by isobutyl chloroformate and dispersive liquid-liquid microextraction followed by gas chromatographic analysis. Food Chem. 2013, 141:436-443.
27. Abbasghorbani M., Attaran A., Payehghadr M. Solvent assisted dispersive micro-SPE by using aminopropyl-functionalized magnetite nanoparticle followed by GC-PID for quantification of parabens in aqueous matrices. J. Sep. Sci. 2013, 36:311-319.
28. Ebrahimpour B., Yamini Y., Esrafili A. Emulsification liquid phase microextraction followed by on-line phase separation coupled to high performance liquid chromatography. Anal. Chim. Acta 2012, 751:79-85.
29. Çabuk H., Akyüz M., Ata S. A simple solvent collection technique for a dispersive liquid-liquid microextraction of parabens from aqueous samples using low-density organic solvents. J. Sep. Sci. 2012, 35:2645-2652.
30. 4 nanoparticles: an ion exchange magnetic sorbent for solid phase extraction. J. Sep. Sci. 2012, 35:2256-2265.
31. Ramírez N., Borrull F., Marcé R.M. Simultaneous determination of parabens and synthetic musks in water by stir-bar sorptive extraction and thermal desorption-gas chromatography-mass spectrometry. J. Sep. Sci. 2012, 358:580-588.