Determination of phosphate phases in sewage sludge ash-based fertilizers by Raman microspectroscopy

Applied Spectroscopy

Volumn 67, Issue 9, 2013, Pages 1101-1105

  Vogel, Christian ^a   Adam, Christian ^b   McNaughton, Don ^a  

^a MONASH UNIVERSITY   (Australia)

^b BAM FEDERAL INSTITUTE FOR MATERIALS RESEARCH AND TESTING   (Germany)

Author keywords

Fertilizer; Phosphate; Raman microspectroscopy; Sewage sludge ash

Indexed keywords

APATITE STRUCTURES; CHEMICAL FORMS; LATERAL RESOLUTION; PURE SUBSTANCES; RAMAN MAPPING; RAMAN MICROSPECTROSCOPY; REFERENCE SPECTRUM; SEWAGE SLUDGE ASH;

FERTILIZERS; PHOSPHATE MINERALS; PHOSPHATES; QUARTZ; SEWAGE SLUDGE;

PHOSPHATE FERTILIZERS;

CALCIUM PYROPHOSPHATE; FERTILIZER; MAGNESIUM DERIVATIVE; MAGNESIUM PYROPHOSPHATE; PHOSPHATE; PYROPHOSPHORIC ACID DERIVATIVE;

ARTICLE; CHEMISTRY; METHODOLOGY; RAMAN SPECTROMETRY; SEWAGE;

CALCIUM PYROPHOSPHATE; DIPHOSPHATES; FERTILIZERS; MAGNESIUM COMPOUNDS; PHOSPHATES; SEWAGE; SPECTRUM ANALYSIS, RAMAN;

EID: 84883326362     PISSN: 00037028     EISSN: 19433530     Source Type: Journal    
DOI: 10.1366/12-06955     Document Type: Article

References (19)

1. D. Cordell, J.-O. Drangert, S. White. "The Story of Phosphorus: Global Food Security and Food for Thought". Global Environ. Change. 2009. 19(2):292-305.
2. SUSAN. http://www.susan. bam.de [accessed Dec. 05 2012].
3. C. Adam, G. Kley, F.-G. Simon. "Thermal Treatment of Municipal Sewage Sludge Aiming at Marketable P-fertilisers". Mater. Trans. 2008. 48(12):3056-3061.
4. C. Vogel, C. Adam. "Heavy Metal Removal from Sewage Sludge Ash by Thermochemical Treatment with Gaseous Hydrochloric Acid". Environ. Sci. Technol. 2011. 45(17):7445-7450.
5. C. Vogel, R. M. Exner, C. Adam. "Heavy Metal Removal from Sewage Sludge Ash by Thermochemical Treatment with Polyvinylchloride". Environ. Sci. Technol. 2013. 47(1):563-567.
6. C. Adam, C. Vogel, S. Wellendorf, J. Schick, S. Kratz, E. Schnug. "Phosphorus Recovery by Thermo-Chemical Treatment of Sewage Sludge Ash-Results of the European FP6-Project SUSAN". In: K. Ashley, S. Mavinic, F. Koch, editors. International Conference on Nutrient Recovery from Wastewater Streams. London: IWA Publishing, 2009. Pp. 417-430.
7. B. Peplinski, C. Adam, M. Michaelis, G. Kley, F. Emmerling, F.-G. Simon. "Reaction Sequences in the Thermochemical Treatment of Sewage Sludge Ashes Revealed by X-ray Powder Diffraction-A Contribution to the European Project SUSAN". Z. Kristallogr. Suppl. 2009. 30:459-464.
8. C. Vogel, A. Kohl, C. Adam. "Spectroscopic Investigation in the Mid-and Far-Infrared Regions of Phosphorus Fertilizers Derived from Thermochemically Treated Sewage Sludge Ash". Appl. Spectrosc. 2011. 65(3):265-271.
9. B. Wopenka, J. D. Pasteris. "A Mineralogical Perspective on the Apatite in Bone". Mat. Sci. Eng. C. 2005. 25(2):131-143. (Pubitemid 40584235)
10. F. Gilchrist, A. Santini, K. Harley, C. Deery. ""The Use of Micro-Raman Spectroscopy to Differentiate Between Sound and Eroded Primary Enamel". Int. J. Paediatr. Dent. 2007. 17(4):274-280.
11. 8: Application to Natural Sanidine and Anorthoclase". Eur. J. Mineral. 2008. 20(6):1055-1065.
12. L. N. Kowalcyk, R. A. Condrate. "Vibrational Spectra of Spodiosite Analogs". J. Am. Ceram. Soc. 1974. 57(2):102-105.
13. 2 Prepared from Mg-Substituted Ca-Deficient Apatite". J. Am. Ceram. Soc. 2006. 89(9):2757-2761. (Pubitemid 44266417)
14. A. A. Chaudhry, J. Goodall, M. Vickers, J. K. Cockcroft, I. Rehman, J. C. Knowles, J. A. Darr. "Synthesis and Characterisation of Magnesium Substituted Calcium Phosphate Bioceramic Nanoparticles Made via Continuous Hydrothermal Flow Synthesis". J. Mater. Chem. 2008. 18(48):5900-5908.
15. V. A. Sinyayev, E. S. Shustikova, D. Griggs, D. V. Dorofeev. "The Nature of P-O Bonds in the Precipitated Amorphous Calcium Phosphates and Calcium Magnesium Phosphates". Glass Phys. Chem. 2005. 31(5):671-675. (Pubitemid 41641590)
16. J. Li. Structural Characterisation of Apatite-Like Materials. [M. Res. Thesis]. Birmingham, UK: University of Birmingham, 2009.
17. H. El Feki, M. Amami, A. Ben Salah, M. Jemal. "Synthesis of Potassium Chloroapatites, IR, X-ray and Raman Studies". Phys. Status Solidi C. 2004. 1(7):1985-1988.
18. D. De Waal, C. Hutter. "Vibrational Spectra of a Solid Solution of Cadmium and Calcium Pyrophosphate". Mat. Res. Bull. 1994. 29(11):1129-1135.
19. B. C. Cornilsen, R. A. Condrate. "The Vibrational Spectra of Magnesium Pyrophosphate Polymorphs". J. Phys. Chem. Solids. 1977. 38(12):1327-1332.