Comparison of different mesoporous silicas for off-line solid phase extraction of 17β-estradiol from waters and its determination by HPLC-DAD

Journal of Hazardous Materials

Volumn 260, Issue , 2013, Pages 609-617

  Gañán, Judith ^a   Pérez Quintanilla, Damián ^a   Morante Zarcero, Sonia ^a   Sierra, Isabel ^a  

^a UNIVERSIDAD REY JUAN CARLOS   (Spain)

Author keywords

17 Estradiol; Mesoporous silica; Solid phase extraction; Water

Indexed keywords

ANALYTE CONCENTRATION; CORRELATION COEFFICIENT; INSTRUMENTAL DETECTION; MESOPOROUS SILICA; OFF-LINE SOLID PHASE EXTRACTION; PHOTODIODE ARRAY DETECTORS; RELATIVE STANDARD DEVIATIONS; SOLID-PHASE EXTRACTION;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PHASE SEPARATION; SILICA; SORBENTS; SORPTION; WATER;

EXTRACTION;

ESTRADIOL; TAP WATER;

ALCOHOL; AQUEOUS SOLUTION; ARRAY; COMPARATIVE STUDY; CONCENTRATION (COMPOSITION); SILICA; VOLUME;

ADSORPTION; ARTICLE; CALIBRATION; COMPARATIVE STUDY; CONTROLLED STUDY; COVALENT BOND; DESORPTION; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROGEN BOND; HYDROPHOBICITY; ISOTHERM; LIMIT OF QUANTITATION; PARTICLE SIZE; PH; PHOTODIODE ARRAY DETECTOR; SCANNING ELECTRON MICROSCOPY; SIGNAL NOISE RATIO; SOLID PHASE EXTRACTION; SOLID STATE; THERMOSTABILITY; X RAY DIFFRACTION;

17Β-ESTRADIOL; 3-AMINOPROPYLTRIETHOXYSILANE; ACETONITRILE; ACN; APTES; BARRET-JOYNER-HALENDA; BET SURFACE AREA; BJH; C(18); CAPACITY FACTOR; CETYLTRIMETHYLAMMONIUM BROMIDE; CTAB; DAD; DCM; DEAD TIME; DICHLOROMETHANE; FOURIER TRANSFORM INFRARED; FTIR; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HPLC; K′; K(OW); K(W); MEOH; MESOPOROUS SILICA; METHANOL; OCTADECYL-MODIFIED SILICA; OCTANOL-WATER PARTITION COEFFICIENT; PHOTODIODE ARRAY DETECTOR; POLYTETRAFLUOROETHYLENE; PTFE; RELATIVE STANDARD DEVIATION; RETENTION FACTOR IN WATER; RETENTION TIME; RSD; S(BET); SCANNING ELECTRON MICROSCOPY; SEM; SOLID-PHASE EXTRACTION; SPE; T(0); T(R); TEM; TEOS; TETRAETHYLORTHOSILICATE; TGA; THERMOGRAVIMETRIC ANALYSIS; TRANSMISSION ELECTRON MICROGRAPH; WATER; X-RAY DIFFRACTION; XRD;

ADSORPTION; CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; ENVIRONMENTAL MONITORING; ESTRADIOL; MAGNETIC RESONANCE SPECTROSCOPY; PHOTOCHEMISTRY; PRESSURE; REPRODUCIBILITY OF RESULTS; SILANES; SILICON DIOXIDE; SOLID PHASE EXTRACTION; SOLVENTS; WATER; WATER POLLUTANTS, CHEMICAL; WATER PURIFICATION; WATER SUPPLY; X-RAY DIFFRACTION;

EID: 84880021806     PISSN: 03043894     EISSN: 18733336     Source Type: Journal    
DOI: 10.1016/j.jhazmat.2013.06.016     Document Type: Article

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