Peri-substituted phosphino-phosphonium salts: Synthesis and reactivity

Organometallics

Volumn 32, Issue 12, 2013, Pages 3481-3492

  Ray, Matthew J ^a   Slawin, Alexandra M Z ^a   Bühl, Michael ^a   Kilian, Petr ^a  

^a UNIVERSITY OF ST ANDREWS   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

ACENAPHTHENE; CLEAN REACTIONS; ELEVATED TEMPERATURE; HETEROLEPTIC; IONIC STRUCTURE; SINGLE CRYSTAL X-RAY STRUCTURES; THROUGH-SPACE COUPLING;

COUPLINGS; MOLYBDENUM COMPOUNDS; PHOSPHORUS COMPOUNDS; SYNTHESIS (CHEMICAL);

SALTS;

EID: 84879491809     PISSN: 02767333     EISSN: 15206041     Source Type: Journal    
DOI: 10.1021/om400259h     Document Type: Article

References (50)

1. Protasiewicz, J. D. Eur. J. Inorg. Chem. 2012, 4539-4549
2. Wang, Y.; Robinson, G. H. Chem. Commun. 2009, 5201-5213
3. Back, O.; Donnadieu, B.; Parameswaran, P.; Frenking, G.; Bertrand, G. Nat. Chem. 2010, 2, 369-373
4. For a review of phospheniums see: Multiple Bonds and Low Coordination in Phosphorus Chemistry; Regitz, M.; Scherer, O. J., Eds.; Georg Thieme Verlag: Stuttgart, Germany, 1990; pp 129-148.
5. Kopp, R. W.; Bond, A. C.; Parry, R. W. Inorg. Chem. 1976, 15, 3042-3046
6. Schultz, C. W.; Parry, R. W. Inorg. Chem. 1976, 15, 3046-3050
7. Cowley, A. H.; Lattman, M.; Wilburn, J. C. Inorg. Chem. 1981, 20, 2916-2919
8. Baxter, S. G.; Collins, R. L.; Cowley, A. H.; Sena, S. F. J. Am. Chem. Soc. 1981, 103, 714-715
9. Baxter, S. G.; Collins, R. L.; Cowley, A. H.; Sena, S. F. Inorg. Chem. 1983, 22, 3475-3479
10. Schomburg, C. Acta Crystallogr., Sect. A 1984, 40, C265
11. Dyker, C. A.; Burford, N. Chem. Asian J. 2008, 3, 28-36
12. Burford, N.; Ragogna, P. J. Dalton Trans. 2002, 4307-4315
13. Ellis, B. D.; Macdonald, C. L. B. Coord. Chem. Rev. 2007, 251, 936-973
14. Carpenter, Y.; Dyker, C. A.; Burford, N.; Lumsden, M. D.; Decken, A. J. Am. Chem. Soc. 2008, 130, 15732-15741
15. Weigand, J. J.; Burford, N.; Davidson, R. J.; Cameron, T. S.; Seelheim, P. J. Am. Chem. Soc. 2009, 131, 17943-17953
16. Seidel, W. Z. Anorg. Allg. Chem. 1964, 330, 141-150
17. Spangenberg, S. F.; Sisler, H. H. Inorg. Chem. 1969, 8, 1006-1010
18. Summers, J. C.; Sisler, H. H. Inorg. Chem. 1970, 9, 862-869
19. Chitnis, S. S.; MacDonald, E.; Burford, N.; Werner-Zwanziger, U.; McDonald, R. Chem. Commun. 2012, 48, 7359-7361
20. Weigand, J. J.; Riegel, S. D.; Burford, N.; Decken, A. J. Am. Chem. Soc. 2007, 129, 7969-7976
21. Burford, N.; Ragogna, P. J.; McDonald, R.; Ferguson, M. J. J. Am. Chem. Soc. 2003, 125, 14404-14410
22. Schomburg, D.; Bettermann, G.; Ernst, L.; Schmutzler, R. Angew. Chem., Int. Ed. Engl. 1985, 24, 975-976
23. Alder, R. W.; Ganter, C.; Harris, C. J.; Orpen, A. G. Chem. Commun. 1992, 1172-1174
24. Alder, R. W.; Ganter, C.; Gil, M.; Gleiter, R.; Harris, C. J.; Harris, S. E.; Lange, H.; Orpen, A. G.; Taylor, P. N. J. Chem. Soc., Perkin Trans. 1 1998, 1643-1655
25. Alder, R. W.; Ellis, D. D.; Gleiter, R.; Harris, C. J.; Lange, H.; Orpen, A. G.; Read, D.; Taylor, P. N. J. Chem. Soc., Perkin Trans. 1 1998, 1657-1668
26. Burford, N.; Cameron, T. S.; Ragogna, P. J. J. Am. Chem. Soc. 2001, 123, 7947-7948
27. Slattery, J. M.; Fish, C.; Green, M.; Hooper, T. N.; Jeffery, J. C.; Kilby, R. J.; Lynam, J. M.; McGrady, J. E.; Pantazis, D. A.; Russell, C. A.; Willans, C. E. Chem. Eur. J. 2007, 13, 6967-6974
28. Abrams, M. B.; Scott, B. L.; Baker, R. T. Organometallics 2000, 19, 4944-4956
29. Karacar, A.; Freytag, M.; Thoennessen, H.; Jones, P. G.; Bartsch, R.; Schmutzler, R. J. Organomet. Chem. 2002, 643, 68-80
30. Van der Winkel, Y.; van der Laarse, J.; de Kanter, F. J. J.; van der Does, T.; Bickelhaupt, F.; Smeets, W. J. J.; Spek, A. L. Heteroat. Chem. 1991, 2, 17-28
31. Kilian, P.; Slawin, A. M. Z.; Woollins, J. D. Dalton Trans. 1996, 2175-2183
32. Charrier, C.; Maigrot, N.; Mathey, F.; Robert, F.; Jeannin, Y. Organometallics 1986, 5, 623-630
33. Kilian, P.; Knight, F. R.; Woollins, J. D. Chem. Eur. J. 2011, 17, 2302-2328
34. Kilian, P.; Knight, F. R.; Woollins, J. D. Coord. Chem. Rev. 2011, 1387-1413
35. Somisara, D. M. U. K.; Buehl, M.; Lebl, T.; Richardson, N. V.; Slawin, A. M. Z.; Woollins, J. D.; Kilian, P. Chem. Eur. J. 2011, 17, 2666-2677
36. Wawrzyniak, P.; Fuller, A. L.; Slawin, A. M. Z.; Kilian, P. Inorg. Chem. 2009, 48, 2500-2506
37. Ray, M. J.; Randall, R. A. M.; Athukorala Arachchige, K. S.; Slawin, A. M. Z.; Buehl, M.; Lebl, T.; Kilian, P. Inorg. Chem. 2013, 52, 4346-4359
38. Jackson, R. D.; James, S.; Orpen, A. G.; Pringle, P. G. J. Organomet. Chem. 1993, 458, C3-C4
39. Karacar, A.; Thoennessen, H.; Jones, P. G.; Bartsch, R.; Schmutzler, R. Heteroat. Chem. 1997, 53, 539-550
40. Karacar, A.; Freytag, M.; Jones, P. G.; Bartsch, R.; Schmutzler, R. Z. Anorg. Allg. Chem. 2002, 628, 533-544
41. Jones, P. G.; Thoennessen, H.; Karacar, A.; Schmutzler, R. Acta Crystallogr., Sect. C 1997, C53, 1119-1122
42. Reiter, S. A.; Nogai, S. D.; Karaghiosoff, K.; Schmidbaur, H. J. Am. Chem. Soc. 2004, 126, 15833-15843
43. Fun, H.-K.; Chantrapromma, S.; Liu, Y.-C.; Chen, Z.-F.; Liang, H. Acta Crystallogr., Sect. E 2006, 62, m1252
44. Robertson, G. B.; Wickramasinghe, W. A. Acta Crystallogr., Sect. C 1987, 43, 1694
45. Diez, A.; Fornies, J.; Garcia, A.; Lalinde, E.; Moreno, M. T. Inorg. Chem. 2005, 44, 2443-2453
46. Liu, S.-T.; Chen, J.-T.; Peng, S.-M.; Hsiao, Y.-L.; Cheng, M. C. Inorg. Chem. 1990, 29, 1169-1172
47. Such an overestimation is typical for the level employed; see: Buehl, M.; Reimann, C.; Pantazis, D. A.; Bredow, T.; Neese, F. J. Chem. Theory Comput. 2008, 4, 1449-1459
48. PPt value is underestimated by more than 700 Hz for the pristine complex: Autschbach, J.; Ziegler, T. J. Am. Chem. Soc. 2001, 123, 3341-3349
49. 2PCl was used with adjusted molar ratios of the reactants. See: Thomaier, J.; Grutzmacher, H. In Synthetic Methods of Organometallic and Inorganic Chemistry; Herrmann, W. A.; Karsch, H. H., Eds.; Georg Thieme Verlag: New York, 1996; Vol. 3, pp 73-74.
50. Drew, D.; Doyle, J. R. Inorg. Synth. 1972, 13, 47-49