Novel chiral core-shell silica microspheres with trans-(1R,2R)-diaminocyclohexane bridged in the mesoporous shell: Synthesis, characterization and application in high performance liquid chromatography

Journal of Chromatography A

Volumn 1299, Issue , 2013, Pages 78-84

  Wu, Xiabing ^a   You, Linjun ^a   Di, Bin ^a   Hao, Weiqiang ^b   Su, Mengxiang ^a   Gu, Yu ^a   Shen, Lingling ^a  

^a CHINA PHARMACEUTICAL UNIVERSITY   (China)

^b NANJING UNIVERSITY   (China)

Author keywords

Chiral core shell silica; Chiral stationary phase; Enantiomers separation; Trans (1R,2R) diaminocyclohexane

Indexed keywords

CHIRAL STATIONARY PHASE; CHIRAL STATIONARY PHASIS; CORE-SHELL SILICAS; ENANTIOMERS SEPARATION; LAYER-BY-LAYER METHODS; OCTADECYLTRIMETHYLAMMONIUM; PERIODIC MESOPOROUS ORGANOSILICAS; TRANS-(1R ,2R)-DIAMINOCYCLOHEXANE;

CHLORINE COMPOUNDS; CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MESOPOROUS MATERIALS; MICROSPHERES; NAPHTHOL; POLYETHYLENE OXIDES; PROPYLENE; SILICA;

SHELLS (STRUCTURES);

1,1' BI 2,2' NAPHTHOL; 1,1' BI 2,2' PHENANTHROL; 6,6' DIBROMO 1,1' BI 2 NAPHTHOL; AMMONIUM CHLORIDE; COPOLYMER; CYCLOHEXANE; DIAMINOCYCLOHEXANE; MICROSPHERE; N,N' BIS [(TRIETHOXYSILYL)PROPYL] TRANS BIS (UREIDO) CYCLOHEXANE; NAPHTHOL DERIVATIVE; OCTADECYLTRIMETHYLAMMONIUM; ORGANOSILICON DERIVATIVE; PHENANTHROLINE DERIVATIVE; SILICON DIOXIDE; TETRAETHOXYSILANE; TRIBLOCK POLY(ETHYLENE OXIDE) B POLY(PROPYLENE OXIDE) B POLY(ETHYLENE OXIDE) COPOLYMER; UNCLASSIFIED DRUG;

ARTICLE; BIOSEPARATION; CHEMICAL ANALYSIS; CHEMICAL REACTION; CHEMICAL STRUCTURE; CHIRALITY; ENANTIOMER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; SYNTHESIS;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MICROSPHERES; POROSITY; SILICON DIOXIDE; STEREOISOMERISM;

EID: 84879462892     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.05.051     Document Type: Article

References (18)

1. Li C., Di B., Hao W., Yan F., Su M. J. Chromatogr. A 2011, 1218:408.
2. Huang L., Lu J., Di B., Feng F., Su M., Yan F. J. Sep. Sci. 2011, 34:2523.
3. Rebbin V., Schmidt R., Froba M. Angew. Chem. Int. Ed. 2006, 45:5210.
4. Ran R., You L., Di B., Hao W., Su M., Yan F., Huang L. J. Sep. Sci. 2012, 35:1854.
5. Zhu G., Jiang D., Yang Q., Yang J., Li C. J. Chromatogr. A 2007, 1149:219.
6. Zhu G., Zhong H., Yang Q., Li C. Micropor. Mesopor. Mater. 2008, 116:36.
7. Fekete S., Fekete J., Ganzler K. J. Pharm. Biomed. Anal. 2009, 50:703.
8. Yang P., Litwinski G.R., Pursch M., McCabe T., Kuppannan K. J. Sep. Sci. 2009, 32:1816.
9. Yang P., McCabe T., Pursch M. J. Sep. Sci. 2011, 34:2975.
10. Fekete S., Berky R., Fekete J., Veuthey J.L., Guillarme D. J. Chromatogr. A 2012, 1236:177.
11. Schuster S.A., Boyes B.E., Wagner B.M., Kirkland J.J. J. Chromatogr. A 2012, 1228:232.
12. Wang X., Barber W.E., Long W.J. J. Chromatogr. A 2012, 1228:72.
13. Fanali S., D'Orazio G., Farkas T., Chankvetadze B. J. Chromatogr. A 2012, 1269:136.
14. Lomsadze K., Jibuti G., Farkas T., Chankvetadze B. J. Chromatogr. A 2012, 1234:50.
15. Reischl R.J., Hartmanova L., Carrozzo M., Huszar M., Fruhauf P., Lindner W. J. Chromatogr. A 2011, 1218:8379.
16. Moreau J.J., Vellutini L., Wong Chi Man M., Bied C. Chemistry 2003, 9:1594.
17. D.J. Anderson, O. Lawn Ill, US Patent, US005425930A (1995).
18. Guiochon G., Gritti F. J. Chromatogr. A 2011, 1218:1915.