Probing the relationship between silicalite-1 defects and polyol adsorption properties

Langmuir

Volumn 29, Issue 22, 2013, Pages 6546-6555

  Mallon, Elizabeth E ^a   Jeon, Mi Young ^a   Navarro, Marta ^b   Bhan, Aditya ^a   Tsapatsis, Michael ^a  

^a University of Minnesota   (United States)

^b UNIVERSITY OF ZARAGOZA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

ADSORPTION AFFINITY; ADSORPTION PROPERTIES; ALKALINE SYNTHESIS; DILUTE CONCENTRATIONS; FLUORIDE SYNTHESIS; HENRY'S CONSTANTS; HYDROPHILIC MOLECULES; SILICALITE-1 CRYSTALS;

ADSORPTION; ADSORPTION ISOTHERMS; ALCOHOLS; CATALYST SELECTIVITY; DEFECT DENSITY; HYSTERESIS; MOLECULES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYOLS; SILICATE MINERALS; SILICON; SURFACE PROPERTIES; WATER VAPOR; ZEOLITES;

DRIERS (MATERIALS);

EID: 84878665162     PISSN: 07437463     EISSN: 15205827     Source Type: Journal    
DOI: 10.1021/la4001494     Document Type: Article

References (53)

1. Sherman, J. D. Synthetic zeolites and other microporous oxide molecular sieves Proc. Natl. Acad. Sci. U.S.A. 1999, 96 (7) 3471
2. Vane, L. M. A review of pervaporation for product recovery from biomass fermentation processes J. Chem. Technol. Biotechnol. 2005, 80 (6) 603
3. Huang, H.-J.; Ramaswamy, S.; Tschirner, U. W.; Ramarao, B. V. A review of separation technologies in current and future biorefineries Sep. Purif. Technol. 2008, 62 (1) 1
4. Zhang, K.; Lively, R. P.; Noel, J. D.; Dose, M. E.; McCool, B. A.; Chance, R. R.; Koros, W. J. Adsorption of water and ethanol in MFI-type zeolites Langmuir 2012, 28 (23) 8664
5. Bowen, T. C.; Noble, R. D.; Falconer, J. L. Fundamentals and applications of pervaporation through zeolite membranes J. Membr. Sci. 2004, 245 (1-2) 1
6. Baerlocher, C.; McCusker, L. B., Database of Zeolite Structures: http://www.iza-structure.org/databases/.
7. Lin, X.; Chen, X. S.; Kita, H.; Okamoto, K. Synthesis of silicalite tubular membranes by in situ crystallization AIChE J. 2003, 49 (1) 237
8. Mallon, E. E.; Bhan, A.; Tsapatsis, M. Driving forces for adsorption of polyols onto zeolites from aqueous solutions J. Phys. Chem. B 2010, 114 (5) 1939
9. Mallon, E. E.; Babineau, I. J.; Kranz, J. I.; Guefrachi, Y.; Siepmann, J. I.; Bhan, A.; Tsapatsis, M. Correlations for adsorption of oxygenates onto zeolites from aqueous solutions J. Phys. Chem. B 2011, 115 (39) 11431
10. Trzpit, M.; Soulard, M.; Patarin, J.; Desbiens, N.; Cailliez, F.; Boutin, A.; Demachy, I.; Fuchs, A. H. The effect of local defects on water adsorption in silicalite-1 zeolite: A joint experimental and molecular simulation study Langmuir 2007, 23 (20) 10131
11. Chezeau, J. M.; Delmotte, L.; Guth, J. L.; Gabelica, Z. Influence of synthesis conditions and postsynthesis treatments on the nature and quantity of structural defects in highly siliceous MFI zeolites: A high-resolution solid state Si-29 NMR study Zeolites 1991, 11 (6) 598
12. Koller, H.; Lobo, R. F.; Burkett, S. L.; Davis, M. E. SIO-HOSI Hydrogen bonds in as-synthesized high-silica zeolites J. Phys. Chem. 1995, 99 (33) 12588
13. Flanigen, E. M.; Patton, R. L. U.S. Patent No. 4,073,865, 1978.
14. Lee, C. C.; Gorte, R. J.; Farneth, W. E. Calorimetric study of alcohol and nitrile adsorption complexes in H-ZSM-5 J. Phys. Chem. B 1997, 101 (19) 3811
15. Dubinin, M. M.; Rakhmatkariev, G. U.; Isirikyan, A. A. Differential heats of adsorption and adsorption-isotherms of alcohols on silicalite Bull. Acad. Sci. USSR Div. Chem. Sci. 1989, 38 (9) 1950
16. Thamm, H. Calorimetric study on the state of C-1-C-4 alcohols sorbed on silicalite J. Chem. Soc., Faraday Trans. I 1989, 85, 1
17. Chen, X.; Ping, Z. H.; Long, Y. C. Separation properties of alcohol-water mixture through silicalite-I-filled silicone rubber membranes by pervaporation J. Appl. Polym. Sci. 1998, 67 (4) 629
18. Chezeau, J. M.; Delmotte, L.; Guth, J. L.; Soulard, M. High-resolution solid-state Si-29 and C-13 NMR on highly siliceous MFI-type zeolites synthesized in nonalkaline fluoride medium Zeolites 1989, 9 (1) 78
19. Navarro, M.; Mayoral, A.; Mateo, E.; Lahoz, R.; de la Fuente, G. F.; Coronas, J. Laser control of zeolite nucleation ChemPhysChem 2012, 13 (3) 736
20. Materials Studio, Release 6.0.; Accelyrs Software Inc.: San Diego, 2011.
21. Vankoningsveld, H.; Vanbekkum, H.; Jansen, J. C. On the location and disorder of the tetrapropylammonium (TPA) ion in zeolite ZSM-5 with improved framework accuracy Acta Crystallogr., Sect. B 1987, 43, 127
22. Vankoningsveld, H.; Jansen, J. C.; Vanbekkum, H. The monoclinic framework structure of zeolite H-ZSM-5: Comparison with the orthorhombic framework of as-synthesized ZSM-5 Zeolites 1990, 10 (4) 235
23. Origin, Release 8.5.1; OriginLab: Northampton, 2011.
24. Curme, G. O.; Johnston, F. Glycols; Reinhold: New York, 1953; p 398
25. Hay, D. G.; Jaeger, H. Orthorhombic monoclinic phase-changes in ZSM-5 zeolite silicalite J. Chem. Soc., Chem. Commun. 1984, 21, 1433
26. 29Si MAS NMR Bull. Chem. Soc. Jpn. 2009, 82 (9) 1160
27. Heitmann, G. P.; Dahlhoff, G.; Holderich, W. F. Catalytically active sites for the Beckmann rearrangement of cyclohexanone oxime to ε-caprolactam J. Catal. 1999, 186 (1) 12
28. Engelhardt, G.; Vankoningsveld, H. Interpretation of Si-29 MAS NMR-spectra by X-Ray data- Application to the monoclinic and orthorhombic framework of zeolite ZSM-5 Zeolites 1990, 10 (7) 650
29. Wu, E. L.; Lawton, S. L.; Olson, D. H.; Rohrman, A. C.; Kokotailo, G. T. ZSM-5-Type materials: Factors affecting crystal symmetry J. Phys. Chem. 1979, 83 (21) 2777
30. Engelhardt, G.; Michel, D. High-Resolution Solid-State NMR of Silicates and Zeolites; John Wiley and Sons: Chichester, 1987.
31. Saito, A.; Foley, H. C. High-resolution nitrogen and argon adsorption on ZSM-5 zeolites- Effects of cation-exchange and Si/Al ratio Microporous Mater. 1995, 3 (4-5) 543
32. Llewellyn, P. L.; Coulomb, J. P.; Grillet, Y.; Patarin, J.; Andre, G.; Rouquerol, J. Adsorption by MFI-type zeolites examined by isothermal microcalorimetry and neutron-diffraction 0.2. Nitrogen and carbon-monoxide Langmuir 1993, 9 (7) 1852
33. Borghard, W. S.; Reischman, P. T.; Sheppard, E. W. Argon sorption in ZSM-5 J. Catal. 1993, 139 (1) 19
34. Llewellyn, P.; Coulomb, J. P.; Reichert, H.; Patarin, J.; Grillet, Y.; Rouquerol, J. A microcalorimetric study of the different states of argon and nitrogen adsorbed at 77-K on silicalite-1 and ZSM-5 J. Therm. Anal. 1992, 38 (4) 683
35. Muller, U.; Reichert, H.; Robens, E.; Unger, K. K.; Grillet, Y.; Rouquerol, F.; Rouquerol, J.; Pan, D. F.; Mersmann, A. High-resolution sorption studies of argon and nitrogen on large crystals of microporous zeolite ZSM-5 Fresenius' Z. Anal. Chem. 1989, 333 (4-5) 433
36. Mueller, U.; Unger, K. K. Preliminary studies on the synthesis of alkaline-free large crystals of ZSM-5 Zeolites 1988, 8 (2) 154
37. Guth, J. L.; Kessler, H.; Wey, R. In New Developments in Zeolite Science and Technology; Murakami, Y.; Iijima, A.; Ward, J. W., Eds.; Elsevier: Amsterdam, 1986; p 121.
38. Pellenq, R. J. M.; Nicholson, D. Grand ensemble Monte-Carlo simulation of simple molecules adsorbed in silicalite-1 zeolite Langmuir 1995, 11 (5) 1626
39. Garcia-Perez, E.; Parra, J. B.; Ania, C. O.; Dubbeldam, D.; Vlugt, T. J. H.; Castillo, J. M.; Merkling, P. J.; Calero, S. Unraveling the argon adsorption processes in MFI-type zeolite J. Phys. Chem. C 2008, 112 (27) 9976
40. Hay, D. G.; Jaeger, H.; West, G. W. Examination of the monoclinic orthorhombic transition in silicalite using XRD and silicon NMR J. Phys. Chem. 1985, 89 (7) 1070
41. Xiong, R.; Sandler, S. I.; Vlachos, D. G. Molecular screening of alcohol and polyol adsorption onto MFI-type zeolites Langmuir 2012, 28 (9) 4491
42. Long, Y. C.; Jiang, H. W.; Zeng, H. Sorbate/framework and sorbate/sorbate interaction of organics on siliceous MFI type zeolite Langmuir 1997, 13 (15) 4094
43. Llano-Restrepo, M.; Mosquera, M. A. Accurate correlation, thermochemistry, and structural interpretation of equilibrium adsorption isotherms of water vapor in zeolite 3A by means of a generalized statistical thermodynamic adsorption model Fluid Phase Equilib. 2009, 283 (1-2) 73
44. Rouquérol, F.; Rouquerol, J.; Sing, K. S. W. Adsorption by Powders and Porous Solids: Principles, Methodology and Applications; Academic Press: New York, 1999.
45. Halasz, I.; Kim, S.; Marcus, B. Uncommon adsorption isotherm of methanol on a hydrophobic Y-zeolite J. Phys. Chem. B 2001, 105 (44) 10788
46. Ahunbay, M. G. Monte Carlo simulation of water adsorption in hydrophobic MFI zeolites with hydrophilic sites Langmuir 2011, 27 (8) 4986
47. Kuhn, J.; Castillo-Sanchez, J. M.; Gascon, J.; Calero, S.; Dubbeldam, D.; Vlugt, T. J. H.; Kapteijn, F.; Gross, J. Adsorption and diffusion of water, methanol, and ethanol in all-silica DD3R: Experiments and simulation J. Phys. Chem. C 2009, 113 (32) 14290
48. Xiong, R.; Sandler, S. I.; Vlachos, D. G. Alcohol adsorption onto silicalite from aqueous solution J. Phys. Chem. C 2011, 115 (38) 18659
49. Krishna, R.; van Baten, J. M. Hydrogen bonding effects in adsorption of water-alcohol mixtures in zeolites and the consequences for the characteristics of the Maxwell-Stefan diffusivities Langmuir 2010, 26 (13) 10854
50. Romero, C. M.; Paez, M. S.; Perez, D. A comparative study of the volumetric properties of dilute aqueous solutions of 1-propanol, 1,2-propanediol, 1,3-propanediol, and 1,2,3-propanetriol at various temperatures J. Chem. Thermodyn. 2008, 40 (12) 1645
51. Romero, C. M.; Lozano, J. M.; Giraldo, G. I. Effect of temperature on partial molar volumes and viscosities of dilute aqueous solutions of 1-butanol, 1,2-butanediol, 1,4-butanediol, 1,2,4-butanetriol, and butanetetrol Phys. Chem. Liq. 2008, 46 (1) 78
52. Ambrosone, L.; Sartorio, R.; Vescio, A.; Vitagliano, V. Volumetric properties of aqueous solutions of ethylene glycol oligomers at 25 C J. Chem. Soc., Faraday Trans. I 1996, 92 (7) 1163
53. Suleiman, D.; Eckert, C. A. Limiting activity coefficients of diols in water by a dew point technique J. Chem. Eng. Data 1994, 39 (4) 692