Sedimentation and resuspendability evaluation of pharmaceutical suspensions by low-field one dimensional pulsed field gradient NMR profilometry

Pharmaceutical Development and Technology

Volumn 18, Issue 4, 2013, Pages 787-797

  Wuxin, Zhu ^a   Martins, José ^a   Saveyn, Pieter ^a   Govoreanu, Ruxandra ^b   Verbruggen, Katrien ^b   Ariën, Tina ^b   Verliefde, Arne ^a   Van Der Meeren, Paul ^a  

^a GHENT UNIVERSITY   (Belgium)

^b JANSSEN RESEARCH AND DEVELOPMENT   (Belgium)

Author keywords

Nuclear magnetic resonance; Pulsed field gradient; Resuspendability; Sediment characterization; Sedimentation; Suspension

Indexed keywords

PALIPERIDONE;

ARTICLE; DISPERSION; NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL; SEDIMENT; SEDIMENTATION; SIGNAL NOISE RATIO; SPECTROMETER; SUSPENSION; VISCOSITY; WATER CONTENT;

ANTIPSYCHOTIC AGENTS; CHLORIDES; ELECTRON SPIN RESONANCE SPECTROSCOPY; ISOXAZOLES; MAGNETIC RESONANCE SPECTROSCOPY; MANGANESE COMPOUNDS; PALMITATES; SUSPENSIONS; WATER;

EID: 84877843003     PISSN: 10837450     EISSN: 10979867     Source Type: Journal    
DOI: 10.3109/10837450.2011.614252     Document Type: Article

References (33)

1. Duro R, Gomez-Amoza JL, Martinez-Pacheco R, Souto C, Concheiro A. Adsorption of polysorbate 80 on pyrantelpamoate: Effects on suspension stability. Int J Pharm 1998;165:211-216.
2. Deicke A, Süverkrüp R. Dose uniformity and redispersibility of pharmaceutical suspensions 2: Assessment of three commercial erythromycin ethyl succinate oral liquids. Eur J Pharm Biopharm 2000;49:73-78.
3. Deicke A, Süverkrüp R. Dose uniformity and redispersibility of pharmaceutical suspensions. I: Quantification and mechanical modelling of human shaking behaviour. Eur J Pharm Biopharm 1999;48:225-232.
4. Mengual O, Meunier G, Cayre I, Puech K, Snabre P. Characterisation of instability of concentrated dispersions by a new optical analyser: The TURBISCAN MA 1000. Colloid Surf A-Physicochem Eng Asp 1999;152:111-123.
5. Lerche, D. Dispersion stability and particle characterization by sedimentation kinetics in a centrifugal field. J Dispers Sci Technol 2002; 23:699-709.
6. Shi TM, Simons SJR, Dickin FJ, Williams RA. Electrical sensing of dispersion behavior. Colloid Surf A-Physicochem Eng Asp 1993;77:9-27.
7. Xie CG, Williams RA, Simons SJR, Beck MS, Bragg R. A novel sedimentation analyzer. Meas Sci Technol 1990;1:1216-1227.
8. Amziane S, Perrot A, Lecompte T. A novel settling and structural build-up measurement method. Meas Sci Technol 2008;19:105702.
9. Acosta-Cabronero J, Hall LD. Measurements by MRI of the settling and packing of solid particles from aqueous suspensions. AIChE J 2009;55:1426-1433.
10. Bobroff S, Phillips RJ. Nuclear magnetic resonance imaging investigation of sedimentation of concentrated suspensions in non-Newtonian fluids. J Rheol 1998;42:1419-1436.
11. d'Avila MA, Powell RL, Phillips RJ, Shapley NC, Walton JH, Dungan SR. Magnetic resonance imaging (MRI): A technique to study flow an microstructure of concentrated emulsions. Braz J Chem Eng 2005;22:49-60.
12. Mackay R, Zhang H, Wu Q, Li YZ. NMR investigation of concentrated alumina and silica slurries. Colloid Surf A-Physicochem Eng Asp 2004;250:343-348.
13. Turney MA, Cheung MK, McCarthy MJ, Powell RL. Magnetic- Resonance-Imaging study of sedimenting suspensions of noncolloidal spheres. Phys Fluids 1995;7:904-911.
14. Samtani MN, Vermeulen A, Stuyckens K. Population pharmacokinetics of intramuscular paliperidone palmitate in patients with schizophrenia: A novel once-monthly, long-acting formulation of an atypical antipsychotic. Clin Pharmacokinet 2009;48:585-600.
15. Sarin P, Taeusch HW, Lu KW, Goerke J, Clements JA. Polyethylene glycol (PEG) results in concentration-dependent sedimentation of Survanta and improvement of its function. Pediatr Res 1999;45:1882.
16. Traini D, Young PM, Rogueda P, Price R. Investigation into the influence of polymeric stabilizing excipients on inter-particulate forces in pressurised metered dose inhalers. Int J Pharm 2006;320:58-63.
17. Pelton R, Xiao HN, Brook NA, Hamielec A. Flocculation of polystyrene latex with mixtures of poly(p-vinylphenol) and poly(ethylene oxide). Langmuir 1996;12:5756-5762.
18. Xiao HN, Pelton R, Hamielec A. Flocculation of polystyrene latex by polyacrylamide-copolyethylene glycol. J Colloid Interface Sci 1995;175:166-172.
19. Zhang ZT, Yang LM, Wang YJ, Luo GS, Dai YY. Morphology controlling of micrometer-sized mesoporous silica spheres assisted by polymers of polyethylene glycol and methyl cellulose. Microporous Mesoporous Mat 2008;115:447-453.
20. Allisy-Roberts PJ, Williams J, Farr RF. Farr's physics for medical imaging. Amsterdam: Elsevier Health Sciences; 2007:170.
21. Wolfe RR, Chinkes DL. (2004). Isotope tracers in metabolic research: Principles and practice of kinetic analysis. New York: Wiley.
22. Ruan RR, Chen PL. (1998). Water in foods and biological materials - a nuclear magnetic resonance approach. Florida: CRC.
23. Blumich B. (2003). NMR imaging of materials. Oxford: Oxford University Press.
24. Mingtao W, Feindel KW, Bergens SH, Wasylishen RE. In situ quantification of the in-plane water content in the Nafion® membrane of an operating polymer-electrolyte membrane fuel cell using 1H μ-magnetic resonance imaging experiments. J Power Sources 2010;195:7316-7322.
25. Odintsov BM, Temnikov AN, Idiyatullin ZS, Kashaev RS, Belford RL, Ceroke PJ, Ceroke PJ, Kuriashkin IV, Clarkson RB. Particle size effect on transverse NMR relaxation in aqueous char suspensions. Colloid Surf A-Physicochem Eng Asp 1999;157:177-183.
26. Muller RN, Gillis P, Moiny F, Roch A. Transverse relaxivity of particulate MRI contrast media: From theories to experiments. Magn Reson Med 1991;22:178-182.
27. Veith SR, Hughes E, Vuataz G, Pratsinis SE. Restricted diffusion in silica particles measured by pulsed field gradient NMR. J Colloid Interface Sci 2004;274:216-228.
28. Watson AT, Chang CTP. Characterizing porous media with NMR methods. Prog Nucl Magn Reson Spectrosc 1997;31:343-386.
29. Schuerman G, Theunissen T, Stokbroekx S, Brewster T. Crystal structure determination from powder x-ray diffraction data. The pharmaceutical powder X-ray diffraction symposium; Barcelona, Spain 2007.
30. Fitch B. Sedimentation of flocculent suspensions - state of the art. AIChE J 1979;25:913-930.
31. Lianos P, Modes S, Staikos G, Brown W. Interaction of poly(oxyethylene glycol) with cyclohexane pentanol sodium dodecyl-sulfate waterin- oil microemulsions. Langmuir 1992;8:1054-1059.
32. Papoutsi D, Lianos P, Brown W. Interaction of α-hydro- ω-hydroxypoly(oxy-1,2-ethanediyl) with water-in-oil microemulsions.2. medium-size polymer-chain - cyclohexane and toluene microemulsions. Langmuir 1993;9:663-668.
33. Papoutsi D, Lianos P, Brown W. Interaction of polyethylene-glycol with water-in-oil microemulsions.3. Effect of polymer size and polymer concentration. Langmuir 1994;10:3402-3405.