Quantitative analysis of organochlorine pesticides in human serum using headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry

Chemosphere

Volumn 92, Issue 3, 2013, Pages 279-285

  Kim, Miok ^a   Song, Na Rae ^a,b   Hong, Jongki ^c   Lee, Jeongae ^a   Pyo, Heesoo ^a  

^a Korea Institute of Science and Technology   (South Korea)

^b UNIVERSITY OF CALIFORNIA   (United States)

^c Kyung Hee University   (South Korea)

Author keywords

GC MS; HS SPME; Human serum; Organochlorine pesticides

Indexed keywords

DRUG PRODUCTS; MASS SPECTROMETRY; METABOLITES; PESTICIDES;

DICHLORODIPHENYLTRICHLOROETHANE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GC-MS; HEAD-SPACE SOLID-PHASE MICROEXTRACTION; HS-SPME; HUMAN SERUM; ORGANOCHLORINE PESTICIDES; PERSISTENT ORGANOCHLORINE PESTICIDES;

GAS CHROMATOGRAPHY;

CARBON 13; CHLORPHENOTANE; HEXACHLOROBENZENE; ORGANOCHLORINE PESTICIDE;

BIOMONITORING; CARBON ISOTOPE; DDE; DDT; ENDOCRINE DISRUPTOR; GAS CHROMATOGRAPHY; HEALTH IMPACT; HEALTH RISK; HEXACHLOROBENZENE; MASS SPECTROMETRY; METABOLITE; ORGANOCHLORINE; PESTICIDE; POLLUTION EXPOSURE; QUANTITATIVE ANALYSIS; SERUM;

ADULT; ARTICLE; BLOOD LEVEL; CONCENTRATION (PARAMETERS); FEMALE; GROUPS BY AGE; HUMAN; MALE; MASS FRAGMENTOGRAPHY; QUANTITATIVE ANALYSIS; SOLID PHASE MICROEXTRACTION; STANDARD;

KOREA;

EID: 84877715825     PISSN: 00456535     EISSN: 18791298     Source Type: Journal    
DOI: 10.1016/j.chemosphere.2013.02.052     Document Type: Article

References (24)

1. Arrebola J.P., Cuellar M., Claure E., Quevedo M., Antelo S.R., Mutch E., Ramirez E., Fernandez M.F., Olea N., Mercado L.A. Concentrations of organochlorine pesticides and polychlorinated biphenyls in human serum and adipose tissue from Bolivia. Environ Res 2012, 112:40-47.
2. Bates M.N., Buckland S.J., Garrett N., Ellis H., Needham L.L., Patterson D.G., Turner W.E., Russell D.G. Persistent organochlorines in the serum of the non-occupationally exposed New Zealand population. Chemosphere 2004, 54:1431-1443.
3. Campo L., Mercadante R., Rossella F., Fustinoni S. Quantification of 13 priority polycyclic aromatic hydrocarbons in human urine by headspace solid-phase microextraction gas chromatography-isotope dilution mass spectrometry. Anal Chim Acta 2009, 631:196-205.
4. Cao L.L., Yan C.H., Yu X.D., Tian Y., Zhao L., Liu J.X., Shen X.M. Relationship between serum concentrations of polychlorinated biphenyls and organochlorine pesticides and dietary habits of pregnant women in Shanghai. Sci Total Environ 2011, 409:2997-3002.
5. CDC Fourth National Report on Human Exposure to Environmental Chemicals 2009, Atlanta, GA.
6. Chen P.S., Huang S.P., Fuh M.R., Huang S.D. Determination of organochlorine pesticides in water using dynamic hook-type liquid-phase microextraction. Anal Chim Acta 2009, 647:177-181.
7. Choi S.-N., Lee J.T., Yu S.-D., Pyo H.-S. Analysis of PAHs and PCBs in human blood sample by gas chromatography/mass spectrometry with SPME. Earth Environ Res 2011, 5(1):29-41.
8. Cohn B.A., Wolff M.S., Cirillo P.M., Sholtz R.I. DDT and breast cancer in young women: new data on the significance of age at exposure. Environ Health Perspect 2007, 115:1406-1414.
9. Hong J.E., Pyo H.S., Park S.J., Lee W. Solid-phase microextraction with on-fiber derivatization for the determination of hydroxyl-polychlorinated biphenyl compounds in urine. Anal Chim Acta 2005, 539:55-60.
10. Jaksyn P., Goni F., Etxeandia A., Vives A., Millan E., Lopez R., Amiano P., Ardanaz E., Barricarte A., Chirlaque M.D., Dorronsoro M., Larranaga N., Martinez C., Navarro C., Rodriguez L., Sanchez M.J., Tormo M.J., Gonzalez C.A., Agudo A. Serum levels of organochlorine pesticides in healthy adults from five regions of Spain. Chemosphere 2009, 76:1518-1524.
11. Kamel F., Hoppin J.A. Association of pesticide exposure with neurologic dysfuntion and disease. Environ Health Perspect 2004, 112:950-958.
12. Kang J.-H., Park H., Chang Y.S., Choi J.W. Distribution of organochlorine pesticides and polychlorinated biphenyls in human serum from urban areas in Korea. Chemosphere 2008, 73:1625-1631.
13. Kang T.-W., Pyo H.-S, Hong J.-K Development of an analytical method of organochlorine pesticides in human bloods using head space solid phase microextraction coupled with gas chromatography mass spectrometry. Anal Sci Technol 2008, 21(4):259-271.
14. Lee S.A., Dai Q., Zheng W., Gao Y.T., Blair A., Tessari J.D., Ji B.T., Shu X.O. Association of serum concentration of organochlorine pesticides with dietary intake and other lifestyle factors among urban Chinese women. Environ Int 2007, 33:157-163.
15. Lopez F.J., Pitarch E., Egea S., Beltran J., Hernandez F. Gas chromatographic determination of organochlorine and organophosphorus pesticides in human fluids using solid phase microextraction. Anal Chim Acta 2001, 433:217-226.
16. Mishra K., Sharma R.C., Kumar S. Organochlorine pollutants in human blood and their relation with age, gender and habitat from North-East India. Chemosphere 2011, 85:454-464.
17. Mishra K., Sharma R.C. Assessment of organochlorine pesticides in human milk and risk exposure to infants from North-East India. Sci Total Environ 2011, 409:4939-4949.
18. Mueller J.F., Harden F., Toms L.-M., Symons R., Furst P. Persistent organochlorine pesticides in human milk samples from Australia. Chemosphere 2008, 70:712-720.
19. Petrik J., Drobna B., Pavuk M., Jursa S., Wimmerova S., Chovancova J. Serum PCBs and organochlorine pesticides in Slovakia: age, gender, and residence as determinants of organochlorine concentrations. Chemosphere 2006, 65:410-418.
20. Qu W., Suri R.P.S., Bi X., Sheng G., Fu J. Exposure of young mothers and newborns to organochlorine pesticides in Guangzhou, China. Sci Total Environ 2010, 408:3133-3138.
21. Sylvie M.A., Shihua Q. Occurrence, distribution and sources of organochlorine pesticides in karst cave. Acad Arena 2009, 1(1):46-56.
22. Tsukino H., Hanaoka T., Sasaki H., Motoyama H., Hiroshima M., Tanaka T., Kabuto M., Turner W., Patterson D.G., Needham L., Tsugane S. Fish intake and serum levels of organochlorines among Japanese Women. Sci Total Environ 2006, 359:90-100.
23. Zhao G., Xu Y., Li W., Han G., Ling B. PCBs and OCPs in human milk and selected foods from Luqiao and Pingqiao in Zhejiang, China. SciTotal Environ 2007, 378:281-292.
24. Zumbado M., Goethals M., Alvarez-Leon E.E., Luzardo O.P., Cabrera F., Serra-Majem L., Dominguez-Boada L. Inadvertent exposure to organo chlorine pesticides DDT and derivatives in people from the Canary Islands(Spain). Sci Total Environ 2005, 339:49-62.