메뉴 건너뛰기




Volumn 230, Issue , 2013, Pages 98-110

Direct observation of 17O-185/187Re 1J-coupling in perrhenates by solid-state 17O VT MAS NMR: Temperature and self-decoupling effects

Author keywords

Dynamics; Isotropic 1J(17O 187Re) spin spin coupling in solids; KReO4 and NH 4ReO4; Reduced 1K( 17O M) isotropic spin spin couplings; Relaxation times; Self decoupling; Solid state 17O VT MAS NMR; Spectral simulations; Theory

Indexed keywords

KREO4 AND NH 4REO4; REDUCED 1K( 17O-M) ISOTROPIC SPIN-SPIN COUPLINGS; SELF-DECOUPLING; SOLID-STATE 17O VT MAS NMR; SPECTRAL SIMULATIONS; SPIN-SPIN COUPLINGS; THEORY;

EID: 84876152736     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2013.01.012     Document Type: Article
Times cited : (15)

References (50)
  • 2
    • 84876113556 scopus 로고    scopus 로고
    • Ref. [1] and the list of references cited in its Ref. (1a-1e)
    • Ref. [1] and the list of references cited in its Ref. (1a-1e)
  • 4
    • 0008823030 scopus 로고
    • A reinvestigation of the crystal structure of potassium perrhenate
    • C.J.L. Lock, and G. Turner A reinvestigation of the crystal structure of potassium perrhenate Acta Cryst. B31 1975 1764 1765
    • (1975) Acta Cryst. , vol.B31 , pp. 1764-1765
    • Lock, C.J.L.1    Turner, G.2
  • 5
    • 0001151460 scopus 로고
    • Ammonium perrhenate at 295 and 135 K
    • G.J. Kruger, and E.C. Reynhardt Ammonium perrhenate at 295 and 135 K Acta Cryst. B34 1978 259 261
    • (1978) Acta Cryst. , vol.B34 , pp. 259-261
    • Kruger, G.J.1    Reynhardt, E.C.2
  • 6
    • 4243582524 scopus 로고
    • Thermal effects in the structure of potassium perrhenate
    • R.J.C. Brown, B.M. Powell, and S.N. Stuart Thermal effects in the structure of potassium perrhenate Acta Cryst. C49 1993 214 216
    • (1993) Acta Cryst. , vol.C49 , pp. 214-216
    • Brown, R.J.C.1    Powell, B.M.2    Stuart, S.N.3
  • 8
    • 0002141743 scopus 로고    scopus 로고
    • Refinement of ammonium perrhenate structure using a pseudo-spin model for the ammonium ion orientation
    • I.P. Swainson, and R.J.C. Brown Refinement of ammonium perrhenate structure using a pseudo-spin model for the ammonium ion orientation Acta Cryst. B53 1997 76 81
    • (1997) Acta Cryst. , vol.B53 , pp. 76-81
    • Swainson, I.P.1    Brown, R.J.C.2
  • 9
    • 51149219275 scopus 로고
    • Rhenium pure quadrupole resonance spectrum of potassium perrhenate
    • M.T. Rogers, and K.V.S. Rama Rao Rhenium pure quadrupole resonance spectrum of potassium perrhenate J. Chem. Phys. 49 1968 1229 1231
    • (1968) J. Chem. Phys. , vol.49 , pp. 1229-1231
    • Rogers, M.T.1    Rama Rao, K.V.S.2
  • 10
    • 36849101286 scopus 로고
    • Pure quadrupole resonance spectra of perrhanates and periodates
    • M.T. Rogers, and K.V.S. Rama Rao Pure quadrupole resonance spectra of perrhanates and periodates J. Chem. Phys. 58 1973 3233 3235
    • (1973) J. Chem. Phys. , vol.58 , pp. 3233-3235
    • Rogers, M.T.1    Rama Rao, K.V.S.2
  • 12
    • 79960759957 scopus 로고    scopus 로고
    • 185Re NMR spectral evidence for and analysis of the origin of high-order quadrupole-induced effects for i = 5/2
    • and references cited therein
    • 185Re NMR spectral evidence for and analysis of the origin of high-order quadrupole-induced effects for I = 5/2, Phys. Chem. Chem. Phys. 13 (2011) 12413-12420 and references cited therein.
    • (2011) Phys. Chem. Chem. Phys. , vol.13 , pp. 12413-12420
    • Widdifield, C.M.1    Bain, A.D.2    Bryce, D.L.3
  • 14
    • 0037050617 scopus 로고    scopus 로고
    • Dynamic effects on the powder line shapes of half-integer nuclei: A solid-state NMR study of XO 4 - Groups
    • R.W. Schurko, S. Wi, and L. Frydman Dynamic effects on the powder line shapes of half-integer nuclei: a solid-state NMR study of XO 4 - groups J. Chem. Phys. A 106 2002 51 62
    • (2002) J. Chem. Phys. A , vol.106 , pp. 51-62
    • Schurko, R.W.1    Wi, S.2    Frydman, L.3
  • 16
    • 84989051895 scopus 로고
    • Microcomputer simulation of solid-state NMR line shapes affected by quadrupolar nuclei
    • A.C. Olivieri, L. Frydman, M. Grasselli, and L.E. Diaz Microcomputer simulation of solid-state NMR line shapes affected by quadrupolar nuclei Magn. Reson. Chem. 26 1988 615 618
    • (1988) Magn. Reson. Chem. , vol.26 , pp. 615-618
    • Olivieri, A.C.1    Frydman, L.2    Grasselli, M.3    Diaz, L.E.4
  • 17
    • 0000128232 scopus 로고
    • Quadrupolar effects in the CPMAS NMR spectra of spin-1/2 nuclei
    • A.C. Olivieri Quadrupolar effects in the CPMAS NMR spectra of spin-1/2 nuclei J. Magn. Reson. 81 1989 201 205
    • (1989) J. Magn. Reson. , vol.81 , pp. 201-205
    • Olivieri, A.C.1
  • 18
    • 2542487776 scopus 로고
    • Quadrupolar effects transferred to spin-1/2 magic-angle spinning spectra of solids
    • R.K. Harris, and A.C. Olivieri Quadrupolar effects transferred to spin-1/2 magic-angle spinning spectra of solids Prog. Nucl. Magn. Reson. Spectrosc. 24 1992 435 456
    • (1992) Prog. Nucl. Magn. Reson. Spectrosc. , vol.24 , pp. 435-456
    • Harris, R.K.1    Olivieri, A.C.2
  • 23
    • 0000507363 scopus 로고    scopus 로고
    • The influence of the heteronuclear dipolar interaction on nuclear magnetic resonance spectra of quadrupolar nuclei
    • G. Wu, and R.E. Wasylishen The influence of the heteronuclear dipolar interaction on nuclear magnetic resonance spectra of quadrupolar nuclei Mol. Phys. 95 1998 1177 1183
    • (1998) Mol. Phys. , vol.95 , pp. 1177-1183
    • Wu, G.1    Wasylishen, R.E.2
  • 24
    • 0001162743 scopus 로고    scopus 로고
    • Residual dipolar couplings between quadrupolar nuclei in high resolution solid state NMR: Description and observations in the high-field limit
    • S. Wi, and L. Frydman Residual dipolar couplings between quadrupolar nuclei in high resolution solid state NMR: description and observations in the high-field limit J. Chem. Phys. 112 2000 3248 3261
    • (2000) J. Chem. Phys. , vol.112 , pp. 3248-3261
    • Wi, S.1    Frydman, L.2
  • 25
    • 0001421829 scopus 로고
    • Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR
    • L. Frydman, and J.S. Harwood Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR J. Am. Chem. Soc. 117 1995 5367 5368
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 5367-5368
    • Frydman, L.1    Harwood, J.S.2
  • 26
    • 0001503615 scopus 로고
    • Towards high-resolution NMR of more nuclei in solids: Sample spinning with time-dependent spinner axis angle
    • A. Llor, and J. Virlet Towards high-resolution NMR of more nuclei in solids: sample spinning with time-dependent spinner axis angle Chem. Phys. Lett. 152 1988 248 253
    • (1988) Chem. Phys. Lett. , vol.152 , pp. 248-253
    • Llor, A.1    Virlet, J.2
  • 27
    • 84891567947 scopus 로고
    • High resolution solid-state NMR. Averaging of second-order effects by means of a double-rotor
    • A. Samoson, E. Lipmaa, and A. Pines High resolution solid-state NMR. Averaging of second-order effects by means of a double-rotor Mol. Phys. 65 1988 1013 1018
    • (1988) Mol. Phys. , vol.65 , pp. 1013-1018
    • Samoson, A.1    Lipmaa, E.2    Pines, A.3
  • 29
    • 80055096710 scopus 로고    scopus 로고
    • Residual dipolar coupling between quadrupolar nuclei under magic-angle spinning and double-rotation conditions
    • F.A. Perras, and D.L. Bryce Residual dipolar coupling between quadrupolar nuclei under magic-angle spinning and double-rotation conditions J. Magn. Reson. 213 2011 82 89
    • (2011) J. Magn. Reson. , vol.213 , pp. 82-89
    • Perras, F.A.1    Bryce, D.L.2
  • 30
    • 0035872812 scopus 로고    scopus 로고
    • Residual dipolar couplings between quadrupolar nuclei in solid state nuclear magnetic resonance at arbitrary fields
    • S. Wi, V. Frydman, and L. Frydman Residual dipolar couplings between quadrupolar nuclei in solid state nuclear magnetic resonance at arbitrary fields J. Chem. Phys. 114 2001 8511 8519
    • (2001) J. Chem. Phys. , vol.114 , pp. 8511-8519
    • Wi, S.1    Frydman, V.2    Frydman, L.3
  • 32
    • 36749116781 scopus 로고
    • Nuclear relaxation and spin-spin coupling in aqueous sodium molybdate
    • R.R. Vold, and R.L. Vold Nuclear relaxation and spin-spin coupling in aqueous sodium molybdate J. Chem. Phys. 61 1974 4360 4361
    • (1974) J. Chem. Phys. , vol.61 , pp. 4360-4361
    • Vold, R.R.1    Vold, R.L.2
  • 33
    • 34548410237 scopus 로고
    • 17O and other quadrupolar nuclei in oxyanions
    • 17O and other quadrupolar nuclei in oxyanions Z. Naturforsch. 31a 1976 1046 1050
    • (1976) Z. Naturforsch. , vol.31 A , pp. 1046-1050
    • Lutz, O.1    Nepple, W.2    Nolle, A.3
  • 35
    • 0021753575 scopus 로고
    • High-resolution oxygen-17 NMR of solids
    • S. Schramm, and E. Oldfield High-resolution oxygen-17 NMR of solids J. Am. Chem. Soc. 106 1984 2502 2506
    • (1984) J. Am. Chem. Soc. , vol.106 , pp. 2502-2506
    • Schramm, S.1    Oldfield, E.2
  • 36
    • 0007132137 scopus 로고
    • 183Tungsten NMR studies
    • 183Tungsten NMR studies Z. Phys. B20 1975 75 80
    • (1975) Z. Phys. , vol.20 B , pp. 75-80
    • Bank, J.1    Schwenk, A.2
  • 39
    • 0000194882 scopus 로고
    • 3. Crystalline-to-plastic phase transition induced by MAS in a double air-bearing stator
    • 3. Crystalline-to-plastic phase transition induced by MAS in a double air-bearing stator J. Magn. Reson. 84 1989 204 211
    • (1989) J. Magn. Reson. , vol.84 , pp. 204-211
    • Bjorholm, T.1    Jakobsen, H.J.2
  • 40
    • 0000325536 scopus 로고
    • 207Pb MAS spectra of solid lead nitrate. An accurate, sensitive thermometer for variable-temperature MAS
    • 207Pb MAS spectra of solid lead nitrate. An accurate, sensitive thermometer for variable-temperature MAS J. Magn. Reson. A 116 1995 215 220
    • (1995) J. Magn. Reson. A , vol.116 , pp. 215-220
    • Bielecki, A.1    Burum, D.P.2
  • 41
    • 0001802901 scopus 로고
    • High-speed MAS of quadrupolar nuclei in solids
    • D.M. Grant, R.K. Harris, Wiley New York
    • H.J. Jakobsen High-speed MAS of quadrupolar nuclei in solids D.M. Grant, R.K. Harris, Encyclopedia of Nuclear Magnetic Resonance vol. 4 1995 Wiley New York 2370 2379
    • (1995) Encyclopedia of Nuclear Magnetic Resonance , vol.4 , pp. 2370-2379
    • Jakobsen, H.J.1
  • 43
    • 0343359244 scopus 로고
    • Investigation of exchange processes by two-dimensional NMR spectroscopy
    • J. Jeener, B.H. Meier, P. Bachmann, and R.R. Ernst Investigation of exchange processes by two-dimensional NMR spectroscopy J. Chem. Phys. 71 1979 4546 4553
    • (1979) J. Chem. Phys. , vol.71 , pp. 4546-4553
    • Jeener, J.1    Meier, B.H.2    Bachmann, P.3    Ernst, R.R.4
  • 45
    • 0001542631 scopus 로고
    • Magic-angle spinning NMR spectra of satellite transitions for quadrupolar nuclei in solids
    • H.J. Jakobsen, J. Skibsted, H. Bildsøe, and N.C. Nielsen Magic-angle spinning NMR spectra of satellite transitions for quadrupolar nuclei in solids J. Magn. Reson. 85 1989 173 180
    • (1989) J. Magn. Reson. , vol.85 , pp. 173-180
    • Jakobsen, H.J.1    Skibsted, J.2    Bildsøe, H.3    Nielsen, N.C.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.