Rapid and efficient procedure for the synthesis of group 3 metal tris[bis(dimethylsilyl)amide] THF complexes

Organometallics

Volumn 32, Issue 5, 2013, Pages 1528-1530

  Smith, Adrian R ^a   Livinghouse, Tom ^a  

^a MONTANA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

SHORT REACTION TIME; TRIMETHYLSILYL;

ORGANOMETALLICS; SYNTHESIS (CHEMICAL);

AMIDES;

EID: 84874881252     PISSN: 02767333     EISSN: 15206041     Source Type: Journal    
DOI: 10.1021/om3006849     Document Type: Article

References (18)

1. Huang, C.-H., Ed. Rare Earth Coordination Chemistry: Fundamentals and Applications; John Wiley & Sons: Singapore, 2010.
2. Gade, L. H. Chem. Commun. 2000, 173-181
3. Anwander, R. Top. Organomet. Chem. 1999, 2, 1-61
4. Mishra, S. Coord. Chem. Rev. 2008, 252, 1996-2025
5. Herrmann, W. A.; Anwander, R.; Munck, F. C.; Scherer, W.; Dufaud, V.; Huber, N. W.; Artus, G. R. J. Z. Naturforsch. 1994, 49b, 1789-1797
6. Zi, G.; Li, H.; Xie, Z. Organometallics 2002, 21, 1136-1145
7. O'Shaughnessy, P. N.; Knight, P. D.; Morton, C.; Gillespie, K. M.; Scott, P. Chem. Commun. 2003, 1770-1771
8. Kerton, F. M.; Whitwood, A. C.; Willans., C. E. Dalton Trans. 2004, 2237-2244
9. Hultzsch, K. C.; Hampel, F.; Wagner, T. Organometallics 2004, 23, 2601-2612
10. Westmoreland, I.; Arnold, J. Dalton Trans. 2006, 4155-4163
11. Heck, R.; Schulz, E.; Collin, J.; Carpantier, J. J. Mol. Catal. A: Chem. 2007, 268, 163-168
12. Wu, B.; Gallucci, J. C.; Parquette, J. R.; RajanBabu, T. V. Angew. Chem., Int. Ed. 2008, 48, 1126-1129
13. Li, G.; Lamberti, M.; Mazzeo, M.; Pappalardo, D.; Roviello, G.; Pellecchia, C. Organometallics 2012, 31, 1180-1188
14. 2 (11 equiv) overnight followed by recrystallization from pentane at -30 C. Yuen, H. F.; Marks, T. J. Organometallics 2008, 27, 155-158
15. Bradley, D. C.; Ghotra, J. S.; Hart, F. A. J. Chem. Soc., Dalton Trans. 1973, 1021-1023
16. Alyea, E. C.; Bradley, D. C.; Copperthwaite, R. G. J. Chem. Soc., Dalton Trans. 1972, 1580-1584
17. Anwander, R.; Runte, O.; Eppinger, J.; Gerstberger, G.; Herdtweck, E.; Spiegler, M. J. Chem. Soc., Dalton Trans. 1998, 847-858
18. 3(THF) complexes, see: Aspinall, H. C.; Tillotson, M. R. Polyhedron 1994, 13, 3229-3234