A new, robust method for measuring average fibre wall pore sizes in cellulose I rich plant fibre walls

Cellulose

Volumn 20, Issue 2, 2013, Pages 623-631

  Larsson, Per Tomas ^a,b   Svensson, Anna ^b   Wågberg, Lars ^b  

^a INNVENTIA AB   (Sweden)

^b ROYAL INSTITUTE OF TECHNOLOGY   (Sweden)

Author keywords

BET; Cellulose I; CP MAS 13C NMR; Fibre saturation point (FSP); Pore size; Water retention value (WRV)

Indexed keywords

CELLULOSE; GAS ADSORPTION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PORE SIZE;

CELLULOSE I; CP/MAS 13C NMR; FIBRE SATURATION POINT; SIZE MEASUREMENTS; SOLID STATE NMR; STRUCTURAL CHARACTERIZATION; STRUCTURE OF FIBRES; WATER RETENTION VALUE;

FIBERS;

EID: 84874521408     PISSN: 09690239     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10570-012-9850-x     Document Type: Article

References (31)

1. Andreasson B, Forsstrom J, Wågberg L (2003) The porous structure of pulp fibres with different yields and its influence on paper strength. Cellulose 10(2): 111-123.
2. Annergren G, Wågberg L (1997) Physiochemical characterization of papermaking fibres. The fundamentals of papermaking materials: Transaction of the 11th Fundamental Research Symposium held at Cambridge.
3. Brunauer S, Emmett PH, Teller E (1938) Adsorption of gases in multimolecular layers. J Am Chem Soc 60: 309-319.
4. Chunilall V, Bush T, Larsson PT, Iversen T, Kindness A (2010) A CP/MAS C-13-NMR study of cellulose fibril aggregation in eucalyptus dissolving pulps during drying and the correlation between aggregate dimensions and chemical reactivity. Holzforschung 64(6): 693-698.
5. Earl WL, Vanderhart DL (1980) High-resolution, magic angle sample spinning C-13 Nmr of solid cellulose-I. J Am Chem Soc 102(9): 3251-3252.
6. Fink HP, Hofmann D, Philipp B (1995) Some aspects of lateral chain order in cellulosics from X-ray-scattering. Cellulose 2(1): 51-70.
7. Forsstrom J, Andreasson B, Wågberg L (2005) Influence of pore structure and water retaining ability of fibres on the strength of papers from unbleached kraft fibres. Nord Pulp Paper Res J 20(2): 176-184.
8. Herrington TM, Midmore BR (1984) Adsorption of Ions at the Cellulose Aqueous-Electrolyte Interface. Part 2. Determination of the Surface-Area of Cellulose Fibers. J Chem Soc Faraday Trans I 80: 1539-1552.
9. Hult EL, Larsson PT, Iversen T (2001) Cellulose fibril aggregation-an inherent property of kraft pulps. Polymer 42(8): 3309-3314.
10. Jakob HF, Fengel D, Tschegg SE, Fratzl P (1995) The elementary cellulose fibril in Picea abies: comparison of transmission electron microscopy, small-angle X-ray scattering, and wide-angle X-ray scattering results. Macromolecules 28(26): 8782-8787.
11. Jarvis MC (1994) Relationship of chemical-shift to glycosidic conformation in the solid-state C-13 Nmr-Spectra of (1-4)-linked glucose polymers and oligomers-anomeric and related effects. Carbohydr Res 259(2): 311-318.
12. Kohnke T, Lund K, Brelid H, Westman G (2010) Kraft pulp hornification: a closer look at the preventive effect gained by glucuronoxylan adsorption. Carbohydr Polym 81(2): 226-233.
13. Krässig HA (1996) Cellulose structure, accessibility and reactivity, polymer monographs, vol 11. Gordon and Breach Science Publishers.
14. Larsson PT, Westlund PO (2005) Line shapes in CP/MAS C-13 NMR spectra of cellulose I. Spectroc Acta Pt A-Molec Biomolec Spectr 62(1-3): 539-546.
15. Larsson PT, Wickholm K, Iversen T (1997) A CP/MAS C-13 NMR investigation of molecular ordering in celluloses. Carbohydr Res 302(1-2): 19-25.
16. Li T-Q, Henriksson U, Ödberg L (1993) Determination of pore sizes in wood cellulose fibres by 2H and 1H NMR. Nord Pulp Paper Res J 3: 326-330.
17. Maloney TC, Paulapuro H, Stenius P (1998) Hydration and swelling of pulp fibers measured with differential scanning calorimetry. Nord Pulp Paper Res J 13(1): 31-36.
18. Moura MJ, Ferreira PJ, Figueiredo MM (2005) Mercury intrusion porosimetry in pulp and paper technology. Powder Technol 160(2): 61-66.
19. Newman RH (1992) Solid-State C-13 Nmr-Spectroscopy of Multiphase Biomaterials. ACS Symp Ser 489: 311-319.
20. Nocanda X, Larsson PT, Spark A, Bush T, Olsson A, Madikane M, Bissessur A, Iversen T (2007) Cross polarisation/magic angle spinning C-13-NMR spectroscopic studies of cellulose structural changes in hardwood dissolving pulp process. Holzforschung 61(6): 675-679.
21. Östlund Å, Köhnke T, Nordstierna L, Nyden M (2010) NMR cryoporometry to study the fiber wall structure and the effect of drying. Cellulose 17(2): 321-328.
22. Park S, Venditti RA, Jameel H, Pawlak JJ (2006) Changes in pore size distribution during the drying of cellulose fibers as measured by differential scanning calorimetry. Carbohydr Polym 66(1): 97-103.
23. Stone JE, Scallan AM (1966) Influence of drying on the pore structures of the cell wall. In: Consolidation of the paper web: Transactions of the symposium, Cambridge, vol 1, pp 145-174.
24. Stone JE, Scallan AM (1967) The effect of component removal upon the porous structure of the cell wall of wood II. Swelling in water and the fibre saturation point. Tappi 50(10): 496-501.
25. Svensson A, Larsson PT, Salazar-Alvarez G, Wågberg L (2013) Preparation of dry ultra-porous cellulosic fibres: characterization and possible initial uses. Carbohydr Polym 92(1): 775-783.
26. Teeäär R, Serimaa R, Paakkari T (1987) Crystallinity of Cellulose, as Determined by Cp/Mas Nmr and Xrd Methods. Polym Bull 17(3): 231-237.
27. Valckenborg RME, Pel L, Kopinga K (2002) Combined NMR cryoporometry and relaxometry. J Phys D-Appl Phys 35(3): 249-256.
28. Vanderhart DL, Atalla RH (1984) Studies of microstructure in native celluloses using solid-state C-13 Nmr. Macromolecules 17(8): 1465-1472.
29. Wang XS, Maloney TC, Paulapuro H (2003) Internal fibrillation in never-dried and once-dried chemical pulps. Appita J 56(6): 455-459.
30. Wickholm K, Larsson PT, Iversen T (1998) Assignment of non-crystalline forms in cellulose I by CP/MAS C-13 NMR spectroscopy. Carbohydr Res 312(3): 123-129.
31. Yamamoto H, Horii F (1993) Cp Mas C-13 Nmr analysis of the crystal transformation induced for Valonia cellulose by annealing at high-temperatures. Macromolecules 26(6): 1313-1317.