Isotope pattern deconvolution-tandem mass spectrometry for the determination and confirmation of diclofenac in wastewaters

Analytica Chimica Acta

Volumn 765, Issue , 2013, Pages 77-85

  Castillo, Ángel ^a   Gracia Lor, Emma ^a   Roig Navarro, Antoni Francesc ^a   Sancho, Juan Vicente ^a   Rodríguez González, Pablo ^b   Alonso, J Ignacio García ^b  

^a UNIVERSITAT JAUME I   (Spain)

^b UNIVERSITY OF OVIEDO   (Spain)

Author keywords

Diclofenac; Isotope dilution mass; Isotope pattern deconvolution; Spectrometry; Tandem mass spectrometry

Indexed keywords

ALTERNATIVE APPROACH; CALIBRATION GRAPHS; CALIBRATION PROCEDURE; CLUSTER IONS; COEFFICIENTS OF VARIATIONS; COMPLEX MATRICES; DICLOFENAC; FALSE NEGATIVES; IMPURITIES IN; ISOTOPE COMPOSITIONS; ISOTOPE DILUTION MASS SPECTROMETRY; ISOTOPE DILUTIONS; ISOTOPE PATTERN; MOLAR FRACTIONS; MULTI-RESIDUE ANALYSIS; MULTIPLE LINEAR REGRESSIONS; NATURAL ABUNDANCE; SPIKED SAMPLES; TANDEM MASS SPECTROMETRY; URBAN WASTEWATER; WATER SAMPLES;

CALIBRATION; EFFLUENTS; LINEAR REGRESSION; MASS SPECTROMETRY; SPECTROMETRY;

ISOTOPES;

DICLOFENAC; ORGANIC COMPOUND; SURFACE WATER;

ANALYTIC METHOD; ARTICLE; CALCULATION; CALIBRATION; CHEMICAL COMPOSITION; CONCENTRATION (PARAMETERS); DRUG DETERMINATION; DRUG IMPURITY; FALSE NEGATIVE RESULT; FRAGMENTATION REACTION; ISOTOPE DILUTION MASS SPECTROMETRY; ISOTOPE PATTERN DECONVOLUTION TANDEM MASS SPECTROMETRY; MASS SPECTROMETER; PRIORITY JOURNAL; PROCESS DEVELOPMENT; QUANTITATIVE ANALYSIS; SEWAGE EFFLUENT; SPIKE; TANDEM MASS SPECTROMETRY; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; VALIDATION PROCESS; WASTE WATER; WATER ANALYSIS; WATER SAMPLING;

CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DICLOFENAC; ISOTOPE LABELING; LINEAR MODELS; TANDEM MASS SPECTROMETRY; WASTE DISPOSAL, FLUID; WASTE WATER; WATER;

EID: 84873702190     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2012.11.033     Document Type: Article

References (37)

1. Richardson S.D. Anal. Chem. 2010, 82:4742.
2. González-Antuña A., Rodríguez-González P., Centineo G., García Alonso J.I. Analyst 2010, 135:953.
3. Lambert J.B., Shurvell H.F., Lightner D., Cooks R.G. Introduction to Organic Spectroscopy 1987, Macmillan Publishing Company, New York, p. 353.
4. Meija J., Caruso J.A. J. Am. Soc. Mass Spectrom. 2004, 15:654.
5. Meija J., Centineo G., García Alonso J.I., Sanz-Medel A., Caruso J.A. J. Mass Spectrom. 2005, 40:807.
6. Rodríguez-Castrillón J.A., Moldovan M., Encinar J.R., García Alonso J.I. J. Anal. At. Spectrom. 2008, 23:318.
7. Rodríguez-Castrillón J.A., Moldovan M., García Alonso J.I. Anal. Bioanal. Chem. 2009, 394:351.
8. Meija J., Yang L., Caruso J.A., Mester Z. J. Anal. At. Spectrom. 2006, 21:1294.
9. Rodríguez-González P., Monperrus M., García Alonso J.I., Amouroux D., Donard O.F.X. J. Anal. At. Spectrom. 2007, 22:1373.
10. Meija J., Ouerdane L., Mester Z. Analyst 2009, 134:466.
11. Rodríguez-González P., Rodríguez-Cea A., García Alonso J.I., Sanz-Medel A. Anal. Chem. 2005, 77:7724.
12. Rodríguez-Castrillón J.A., Moldovan M., García Alonso J.I., Lucena J.J., García-Tomé M.L., Hernández-Apalaza L. Anal. Bioanal. Chem. 2008, 390:579.
13. Iglesias H.G., Fernández M.L., García Alonso J.I., Sanz-Medel A. Anal. Bioanal. Chem. 2007, 389:707.
14. Rojas C.L., Romera F.J., Alcántara E., Pérez-Vicente R., Sariego C., García Alonso J.I., Boned J., Marti G. J. Agric. Food Chem. 2008, 56(56):10774.
15. Rodríguez-Castrillón J.A., Hinojosa Reyes L., Marchante-Gayón J.M., Moldovan M., García Alonso J.I. J. Anal. At. Spectrom. 2008, 23:579.
16. Rodríguez-González P., García Alonso J.I. J. Anal. At. Spectrom. 2010, 25:239.
17. Castillo A., Rodríguez-González P., Centineo G., Roig-Navarro A.F., García Alonso J.I. Anal. Chem. 2010, 82:2773.
18. González-Gago A., Marchante-Gayón J.M., Ferrero M., García Alonso J.I. Anal. Chem. 2010, 82:2879.
19. Gracia-Lor E., Sancho J.V., Hernández F. J. Chromatogr. A 2010, 1217:622.
20. Kasprzyk-Hordern B., Dinsdale R.M., Guwy A.J. Talanta 2008, 74:1299.
21. Batt A.L., Kostich M.S., Lazorchak J.M. Anal. Chem. 2008, 80:5021.
22. Marín J.M., Gracia-Lor E., Sancho J.V., López F.J., Hernández F. J. Chromatogr. A 2009, 1216:1410.
23. Bijlsma L., Sancho J.V., Pitarch E., Ibáñez M., Hernández F. J. Chromatogr. A 2009, 1216:3078.
24. García Alonso J.I. Anal. Chim. Acta 1995, 312:57.
25. Haug L.S., Thomsen C., Becher G. J. Chromatogr. A 2009, 1216:385.
26. Klaassen T., Szwandt S., Kapron J.T., Roemer A. Rapid Commun. Spectrom. 2009, 23:2301.
27. Ramaley L., Cubero Herrera L. Rapid Commun. Mass Spectrom. 2008, 22:2714.
28. Stokvis E., Rosing H., Beijnen J.H. Rapid Commun. Mass Spectrom. 2005, 19:401.
29. Kato K., Jingu S., Ogawa N., Higuchi S. J. Pharm. Biomed. Anal. 2000, 24:237.
30. Wieling J. Chromatographia Suppl. 2002, 55:S107.
31. Valleix A., Carrat S., Caussignac C., Leonce E., Tchapla A. J. Chromatogr. A 2006, 1116:109.
32. Guo K., Ji C., Li L. Anal. Chem. 2007, 79:8631.
33. Kim Y., Ahn S., Chang T. Anal. Chem. 2010, 82:1509.
34. Itoh N., Numata M., Aoyagi Y., Yarita T. J. Chromatogr. A 2007, 1138:26.
35. European Union Decision 2002/657/EC, Off. J. Eur. Commun., L221, 2002, pp. 8-36 (12 August 2002).
36. European Commission DG-SANCO, Method validation and quality control procedures for pesticide residue analysis in food and feed No. SANCO/2007/3131, 31 October 2007, Brussels. http://ec.europa.eu/food/plant/protection/resources/qualcontrol_en.pdf.
37. Kragten J. Analyst 1994, 119:2161.