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Volumn 15, Issue 2, 2013, Pages 320-324

Direct aerobic oxidation of 2-benzylpyridines in a gas-liquid continuous-flow regime using propylene carbonate as a solvent

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EID: 84873321858     PISSN: 14639262     EISSN: 14639270     Source Type: Journal    
DOI: 10.1039/c2gc36896j     Document Type: Article
Times cited : (90)

References (47)
  • 39
    • 50049109778 scopus 로고    scopus 로고
    • For a general discussion on novel process windows and process intensification technologies based on high-T/p conditions, see
    • S. Enthaler K. Junge M. Beller Angew. Chem., Int. Ed. 2008 47 3317 3321
    • (2008) Angew. Chem., Int. Ed. , vol.47 , pp. 3317-3321
    • Enthaler, S.1    Junge, K.2    Beller, M.3
  • 43
    • 77952935876 scopus 로고    scopus 로고
    • The yield of 2-benzylpyridine 2a was also calculated by GC-FID analysis using methyl phenylacetate as an internal standard and is consistent with the isolated yield It is worth mentioning that the high-T/p gas-liquid continuous flow approach described herein cannot be carried out using the "tube-in-tube" concept developed by the Ley group (e.g., ref. 19). Commercially available instruments using this technology are either used to saturate the liquid phase with the gaseous reactant before entering a heated residence time unit, or are limited to temperatures below 150 °C. For representative examples, see
    • T. Razzaq C. O. Kappe Chem.-Asian J. 2010 5 1274 1289
    • (2010) Chem.-Asian J. , vol.5 , pp. 1274-1289
    • Razzaq, T.1    Kappe, C.O.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.