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Volumn 228, Issue , 2013, Pages 130-135

Accurate determinations of one-bond 13C-13C couplings in 13C-labeled carbohydrates

Author keywords

Carbohydrate structure; Carbon carbon coupling; Carbon carbon residual dipolar coupling; Constant time; Labeled carbohydrate

Indexed keywords

CARBON-CARBON COUPLING; CONSTANT TIME; DIAGONAL PEAKS; INTENSITY MODULATIONS; INTENSITY RATIO; MOLECULAR ARCHITECTURE; NULLING; OVERLAP PROBLEMS; PASSIVE COUPLING; PEAK SEPARATIONS; RELIABLE ASSESSMENT; RESIDUAL DIPOLAR COUPLINGS; SCALAR COUPLING; STRONG COUPLING; STRUCTURAL CALCULATIONS; STRUCTURAL STUDIES;

EID: 84873049841     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2013.01.001     Document Type: Article
Times cited : (7)

References (32)
  • 1
    • 0031080051 scopus 로고    scopus 로고
    • Glycosphingolipid antigens and cancer therapy
    • S.-I. Hakomori, and Y. Zhang Glycosphingolipid antigens and cancer therapy Chem. Biol. 4 1997 97 104
    • (1997) Chem. Biol. , vol.4 , pp. 97-104
    • Hakomori, S.-I.1    Zhang, Y.2
  • 2
    • 0034443638 scopus 로고    scopus 로고
    • The chemistry and immunochemistry of blood group A, B, H and Lewis antigens: Past, Present, and future
    • K.O. Lloyd The chemistry and immunochemistry of blood group A, B, H and Lewis antigens: past, Present, and future Glycoconjugate J. 17 2000 531 541
    • (2000) Glycoconjugate J. , vol.17 , pp. 531-541
    • Lloyd, K.O.1
  • 3
    • 0034440599 scopus 로고    scopus 로고
    • Unravelling the biochemical basis of blood group ABO and Lewis antigenic specificity
    • W.T.J. Morgan, and W.M. Watkins Unravelling the biochemical basis of blood group ABO and Lewis antigenic specificity Glycoconjugate J. 17 2000 501 530
    • (2000) Glycoconjugate J. , vol.17 , pp. 501-530
    • Morgan, W.T.J.1    Watkins, W.M.2
  • 4
    • 0026452953 scopus 로고
    • LeX and related structures as adhesion molecules
    • S.-I. Hakomori LeX and related structures as adhesion molecules Histochem. J. 24 1992 771 776
    • (1992) Histochem. J. , vol.24 , pp. 771-776
    • Hakomori, S.-I.1
  • 5
    • 0030722243 scopus 로고    scopus 로고
    • Direct measurement of distances and angles in biomolecules by NMR in a dilute liquid crystalline medium
    • N. Tjandra, and A. Bax Direct measurement of distances and angles in biomolecules by NMR in a dilute liquid crystalline medium Science 278 1997 1111 1114
    • (1997) Science , vol.278 , pp. 1111-1114
    • Tjandra, N.1    Bax, A.2
  • 6
    • 0036163082 scopus 로고    scopus 로고
    • Conformational studies of Lewis X and Lewis A trisaccharides using NMR residual dipolar couplings
    • H.F. Azurmendi, M. Martin-Pastor, and C.A. Bush Conformational studies of Lewis X and Lewis A trisaccharides using NMR residual dipolar couplings Biopolymers 63 2002 89 98
    • (2002) Biopolymers , vol.63 , pp. 89-98
    • Azurmendi, H.F.1    Martin-Pastor, M.2    Bush, C.A.3
  • 8
    • 0037070538 scopus 로고    scopus 로고
    • An alternative method for pucker determination in carbohydrates from residual dipolar couplings: A solution NMR study of the fructofuranosyl ring of sucrose
    • D.I. Freedberg An alternative method for pucker determination in carbohydrates from residual dipolar couplings: a solution NMR study of the fructofuranosyl ring of sucrose J. Am. Chem. Soc. 124 2002 2358 2362
    • (2002) J. Am. Chem. Soc. , vol.124 , pp. 2358-2362
    • Freedberg, D.I.1
  • 9
    • 15044360249 scopus 로고    scopus 로고
    • The utility of residual dipolar couplings in detecting motion in carbohydrates: Application to sucrose
    • R.M. Venable, F. Delaglio, S.E. Norris, and D.I. Freedberg The utility of residual dipolar couplings in detecting motion in carbohydrates: application to sucrose Carbohydr. Res. 340 2005 863 874
    • (2005) Carbohydr. Res. , vol.340 , pp. 863-874
    • Venable, R.M.1    Delaglio, F.2    Norris, S.E.3    Freedberg, D.I.4
  • 10
    • 0037710749 scopus 로고    scopus 로고
    • NMR experiments for the measurement of proton-proton and carbon-carbon residual dipolar couplings in uniformly labelled oligosaccharides
    • M. Martin-Pastor, A. Canales-Mayordomo, and J. Jimenez-Barbero NMR experiments for the measurement of proton-proton and carbon-carbon residual dipolar couplings in uniformly labelled oligosaccharides J. Biomol. NMR 26 2003 345 353
    • (2003) J. Biomol. NMR , vol.26 , pp. 345-353
    • Martin-Pastor, M.1    Canales-Mayordomo, A.2    Jimenez-Barbero, J.3
  • 11
    • 17444441807 scopus 로고    scopus 로고
    • J-modulated ADEQUATE (JM-ADEQUATE) experiment for accurate measurement of carbon-carbon coupling constants
    • K.E. Kövér, and P. Forgo J-modulated ADEQUATE (JM-ADEQUATE) experiment for accurate measurement of carbon-carbon coupling constants J. Magn. Reson. 166 2004 47 52
    • (2004) J. Magn. Reson. , vol.166 , pp. 47-52
    • Kövér, K.E.1    Forgo, P.2
  • 12
    • 34748829644 scopus 로고    scopus 로고
    • J-modulated ADEQUATE experiments using different kinds of refocusing pulses
    • C. Thiele, and W. Bermel J-modulated ADEQUATE experiments using different kinds of refocusing pulses Magn. Reson. Chem. 45 2007 889 894
    • (2007) Magn. Reson. Chem. , vol.45 , pp. 889-894
    • Thiele, C.1    Bermel, W.2
  • 15
    • 0033603869 scopus 로고    scopus 로고
    • Intensity-based measurement of homonuclear residual dipolar couplings from CT-COSY
    • F. Tian, P.J. Bolon, and J.H. Prestegard Intensity-based measurement of homonuclear residual dipolar couplings from CT-COSY J. Am. Chem. Soc. 121 1999 7712 7713
    • (1999) J. Am. Chem. Soc. , vol.121 , pp. 7712-7713
    • Tian, F.1    Bolon, P.J.2    Prestegard, J.H.3
  • 16
    • 0000408412 scopus 로고
    • Application of ω1-decoupled 2D correlation spectra to the study of proteins
    • M. Rance, G. Wagner, O.W. Sorensen, K. Wütrich, and R.R. Ernst Application of ω1-decoupled 2D correlation spectra to the study of proteins J. Magn. Reson. 59 1984 250 261
    • (1984) J. Magn. Reson. , vol.59 , pp. 250-261
    • Rance, M.1    Wagner, G.2    Sorensen, O.W.3    Wütrich, K.4    Ernst, R.R.5
  • 17
    • 0035742342 scopus 로고    scopus 로고
    • Measurement of homonuclear proton couplings based on cross-peak nulling in CT-COSY
    • Z. Wu, and A. Bax Measurement of homonuclear proton couplings based on cross-peak nulling in CT-COSY J. Magn. Reson. 151 2001 242 252
    • (2001) J. Magn. Reson. , vol.151 , pp. 242-252
    • Wu, Z.1    Bax, A.2
  • 19
    • 0030192091 scopus 로고    scopus 로고
    • High-resolution solid-state NMR spectra of integral membrane proteins reconstituted into magnetically oriented phospholipid bilayers
    • K.P. Howard, and S.J. Opella High-resolution solid-state NMR spectra of integral membrane proteins reconstituted into magnetically oriented phospholipid bilayers J. Magn. Reson. Ser. B 112 1996 91 94
    • (1996) J. Magn. Reson. Ser. B , vol.112 , pp. 91-94
    • Howard, K.P.1    Opella, S.J.2
  • 20
    • 0032174883 scopus 로고    scopus 로고
    • Characterization of magnetically oriented phospholipid micelles for measurement of dipolar couplings in macromolecules
    • M. Ottiger, and A. Bax Characterization of magnetically oriented phospholipid micelles for measurement of dipolar couplings in macromolecules J. Biomol. NMR V12 1998 361 372
    • (1998) J. Biomol. NMR , vol.12 V , pp. 361-372
    • Ottiger, M.1    Bax, A.2
  • 21
    • 0000741505 scopus 로고
    • Symmetric phase-alternating composite pulses
    • A.J. Shaka, and A. Pines Symmetric phase-alternating composite pulses J. Magn. Reson. 71 1987 495 503
    • (1987) J. Magn. Reson. , vol.71 , pp. 495-503
    • Shaka, A.J.1    Pines, A.2
  • 23
    • 84874192243 scopus 로고    scopus 로고
    • University of California, San Francisco
    • T.D. Goddard, D.G. Kneller, University of California, San Francisco, 2008. < http://www.cgl.ucsf.edu/home/sparky/ >.
    • (2008)
    • Goddard, T.D.1    Kneller, D.G.2
  • 24
    • 84874188886 scopus 로고    scopus 로고
    • O. Corporation, OriginLab Corporation, Northanpton, MA
    • O. Corporation, OriginLab Corporation, Northanpton, MA. < http://www.originlab.com >.
  • 26
    • 43949165635 scopus 로고
    • Assignment of carbon-13 chemical shift tensors in single crystal sucrose
    • M.H. Sherwood, D.W. Alderman, and D.M. Grant Assignment of carbon-13 chemical shift tensors in single crystal sucrose J. Magn. Reson. Ser. A 104 1993 132 145
    • (1993) J. Magn. Reson. Ser. A , vol.104 , pp. 132-145
    • Sherwood, M.H.1    Alderman, D.W.2    Grant, D.M.3
  • 27
    • 0000360528 scopus 로고    scopus 로고
    • Analyzing and assigning carbon-13 chemical shift tensors in fructose, sorbose and xylose single crystals
    • F. Lui, C.G. Phung, D.W. Alderman, and D.M. Grant Analyzing and assigning carbon-13 chemical shift tensors in fructose, sorbose and xylose single crystals J. Magn. Reson. Ser. B 120 1996 231 241
    • (1996) J. Magn. Reson. Ser. B , vol.120 , pp. 231-241
    • Lui, F.1    Phung, C.G.2    Alderman, D.W.3    Grant, D.M.4
  • 28
    • 0028794027 scopus 로고
    • 1H chemical shift anisotropy of sialic acid and its homopolymer (colominic acid) from cross-correlated relaxation
    • 1H chemical shift anisotropy of sialic acid and its homopolymer (colominic acid) from cross-correlated relaxation J. Am. Chem. Soc. 117 1995 368 374
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 368-374
    • Batta, G.1    Gervay, J.2
  • 29
    • 0000587142 scopus 로고
    • Interference between couplings and cross-relaxation in solution NMR spectroscopy: Consequences for macromolecular structure determination
    • G. Harbison Interference between couplings and cross-relaxation in solution NMR spectroscopy: consequences for macromolecular structure determination J. Am. Chem. Soc. 1993 3026 3027
    • (1993) J. Am. Chem. Soc. , pp. 3026-3027
    • Harbison, G.1
  • 30
    • 84857057964 scopus 로고    scopus 로고
    • More accurate 1JCH coupling measurement in the presence of 3JHH strong coupling in natural abundance
    • B. Yu, H. van-Ingen, C. Rademacher, S. Vivekanandan, S.E. Norris, and D.I. Freedberg More accurate 1JCH coupling measurement in the presence of 3JHH strong coupling in natural abundance J. Magn. Reson. 215 2012 10 22
    • (2012) J. Magn. Reson. , vol.215 , pp. 10-22
    • Yu, B.1    Van-Ingen, H.2    Rademacher, C.3    Vivekanandan, S.4    Norris, S.E.5    Freedberg, D.I.6
  • 31
    • 18444381437 scopus 로고    scopus 로고
    • NMR spectroscopy in the study of carbohydrates: Characterizing the structural complexity
    • W.A. Bubb NMR spectroscopy in the study of carbohydrates: characterizing the structural complexity Concept. Magn. Reson. 19 2003 1 19
    • (2003) Concept. Magn. Reson. , vol.19 , pp. 1-19
    • Bubb, W.A.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.