Monitoring of photopolymerization kinetics and network formation by combined real-time near-infrared spectroscopy and ultrasonic reflectometry

Reactive and Functional Polymers

Volumn 73, Issue 2, 2013, Pages 316-322

  Alig, Ingo ^a   Lellinger, Dirk ^a   Agarwal, Suman ^a   Oehler, Harald ^a  

^a FRAUNHOFER INSTITUTE FOR STRUCTURAL DURABILITY AND SYSTEM RELIABILITY LBF   (Germany)

Author keywords

Acrylates; Monitoring of UV curing; Near infrared spectroscopy; Ultrasonic reflection

Indexed keywords

ACRYLATES; CATIONIC EPOXY; CHEMICAL COMPOSITIONS; CHEMICAL CONVERSIONS; CURING CONDITION; CURING TIME; DIFFUSION-CONTROLLED POLYMERIZATION; EPOXY ACRYLATE; IN-SITU MONITORING; LIGHT CURING; NETWORK FORMATION; PHOTOPOLYMERIZATION KINETICS; POLYMER NETWORKS; REFLECTOMETRY; RESCALING; UV-CURING; UV-RADIATION CURING; VISCOELASTIC RELAXATION;

EPOXY RESINS; INFRARED DEVICES; NEAR INFRARED SPECTROSCOPY; PHOTOPOLYMERIZATION; POLYMERIZATION; REACTION KINETICS; RESINS; SALTS; ULTRASONIC REFLECTION;

CURING;

EID: 84872612813     PISSN: 13815148     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.reactfunctpolym.2012.08.006     Document Type: Conference Paper

References (30)

1. A. Goldschmidt, and H.J. Streitberger BASF Handbook on Basics of Coating Technology 2003 Vincentz Network Hannover, Germany
2. R. Schwalm UV Coatings-Basics, Recent Developments and New Applications first ed. 2007 Elsevier
3. P. Gloeckner, T. Jung, S. Struck, and K. Studer Radiation Curing-Coatings and Printings Inks 2008 Vincentz Network Hannover
4. J.A. Johnson, and C.O. Bliss Radtech Rep. 13 2006 21
5. A. Endruweit, M.S. Johnson, and A.C. Long Polym. Compos. 27 2006 119 128
6. M.G. Parthun, and G.P. Johari J. Polym. Sci. Part B: Polym. Phys. 30 1992 655 667
7. I. Alig, D. Lellinger, and G.P. Johari Relaxations in thermosets. XVIII. Ultrasonic studies of curing kinetics of ethylene-diamine-cured epoxide J. Polym. Sci. Part B: Polym. Phys. 30 1992 791 799
8. J.E. Moore S.P. Pappas, UV Curing: Science and Technology 1978 Technology Market Publishers Stanford 33
9. C. Decker, and K. Moussa Makromol. Chem. 189 1988 2381 2394
10. T. Scherzer, and U. Decker Vib. Spectrosc. 19 1999 387 400
11. T. Scherzer, G. Mirschel, K. Heymann, and M.R. Buchmeiser Continuous Monitoring of Process Parameters in UV Curing Processes RadTech Rep. 24 2 2010 40 48
12. P.A.M. Steeman, A.A. Dias, D. Wenke, and T. Zwartkruis Macromolecules 37 2004 7001 7007
13. I. Alig, P.A.M. Steeman, D. Lellinger, A.A. Dias, and D. Wienke Progr. Org. Coat. 55 2006 88 96
14. I. Alig, H. Oehler, and D. Lellinger Adhäsion 5 2005 36 39
15. I. Alig, H. Oehler, D. Lellinger, and S. Tadjbach Progr. Org. Coat. 58 2007 200 208
16. S.A. Khan, I.M. Plitz, and R.A. Frantz Rheol. Acta 31 1992 151
17. L.E. Schmidt, Y. Leterrier, J.M. Vesin, M. Wilhelm, and J.A.E. Månson Macromol. Mater. Eng. 290 2005 1115
18. K. Osaka, A. Kasai, T. Kosaka, Y. Sawada, Cure monitoring of UV Polymers by Raman spectroscopy, in: Proceedings of the 16th International Conference on Composite Materials, Kyoto, 2007.
19. I. Alig, S. Agarwal, D. Lellinger, H. Oehler, Thermosets 2011-from monomers to composites, in: Proceedings of the 2nd International Conference on Thermosets, 21-23 September 2011, pp. 89-92. ISBN: 978-3-8396-0312-3.
20. A. Botella, J. Dupuy, A.-A. Roche, H. Sautereau, and V. Verney Macromol. Rapid Commun. 25 2004 1155 1158
21. T. Scherzer, M.W. Schröder, Simultaneous analysis of the UV curing of acrylate-nanoparticle formulations by combined photorheometry and FT-NIR spectroscopy, in: Proceedings RadTech Europe 2009 Conference, Nizza, 2009. p. 14.-15.10
22. W.P. Mason, W.O. Baker, H.J. Mc Skimin, and J.H. Heiss Phys. Rev. 75 1949 936 946
23. I. Alig, D. Lellinger, J. Sulimma, and S. Tadjbakhsch Rev. Sci. Instrum. 68 1997 1536 1542
24. D. Lellinger, S. Tadjbakhsch, and I. Alig Macromol. Symp. 184 2002 203 213
25. I. Alig, S. Tadjbach, D. Lellinger, H. Oehler, M. Wenzel, Ultraschallverfahren zur Verfolgung von Trocknung und Verfestigung von Lacken und Klebstoffen Farbe & Lack 109 (Supplement: Prüf- und Messtechnik aktuell) 8 (2003) 4-7.
26. H. Vogel Phys. Z. 22 645 1921 645 646
27. G.S. Fulcher J. Am. Ceram. Soc. 8 1925 339 355
28. A.T. DiBenedetto J. Polym. Sci. Polym. Phys. 26 1987 1949 1969
29. S. Havriliak, and S. Negami Polymer 8 1967 161 210
30. S. Agarwal, PhD thesis, In Situ Monitoring of UV-Curing Kinetics of Acrylate Coatings by Combined Ultrasound Reflectometry and Near-Infrared Spectroscopy, TU-Darmstadt, 2011.