An experimental study of the competing processes of evaporation and polymerization of levoglucosan in cellulose pyrolysis

Journal of Analytical and Applied Pyrolysis

Volumn 99, Issue , 2013, Pages 130-136

  Bai, Xianglan ^a,b   Johnston, Patrick ^a   Brown, Robert C ^a,b  

^a IOWA STATE UNIVERSITY   (United States)

^b Iowa State University of Science and Technology   (United States)

Author keywords

Cellulose; Evaporation; Levoglucosan; Polymerization; Pyrolysis

Indexed keywords

CELLULOSE; EVAPORATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; POLYMERIZATION;

CELLULOSE DECOMPOSITION; CELLULOSE PYROLYSIS; ELEVATED TEMPERATURE; EXPERIMENTAL CONDITIONS; LEVOGLUCOSAN; LOW MOLECULAR WEIGHT; PYROLYSIS PRODUCTS; THERMOGRAVIMETRIC ANALYZERS;

PYROLYSIS;

EID: 84871715467     PISSN: 01652370     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jaap.2012.10.012     Document Type: Article

References (26)

1. A.V. Bridgwater, D. Meier, and D. Radlein An overview of fast pyrolysis of biomass Organic Geochemistry 30 1999 1479 1493
2. A.V. Bridgwater Review of fast pyrolysis of biomass and product upgrading Biomass and Bioenergy 38 2012 68 94
3. C.A. Mullen, and A.A. Boateng Chemical composition of bio-oils produced by fast pyrolysis of two energy crops Energy and Fuels 22 2008 2104 2109
4. S. Czernik, and A.V. Bridgwater Overview of applications of biomass fast pyrolysis oil Energy and Fuels 18 2004 590 598
5. N.M. Bennett, S.S. Helle, and S.J.B. Duff Extraction and hydrolysis of levoglucosan from pyrolysis oil Bioresource Technology 100 2009 6059 6063
6. D. Mohan, C.U. Pittman, and P.H. Steele Pyrolysis of wood/biomass for bio-oil: a critical review Energy and Fuels 20 2006 848 889
7. G. Dobele, T. Dizhbite, G. Rossinskaja, G. Telysheva, D. Meier, S. Radtke, and O. Faix Pre-treatment of biomass with phosphoric acid prior to fast pyrolysis: a promising method for obtaining 1,6-anhydrosaccharides in high yields Journal of Analytical and Applied Pyrolysis 68-69 2003 197 211
8. D.S. Scott, L. Paterson, J. Piskorz, and D. Radlein Pretreatment of poplar wood for fast pyrolysis: rate of cation removal Journal of Analytical and Applied Pyrolysis 57 2000 169 176
9. R.C. Brown, D. Radlein, and J. Piskorz Pretreatment processes to increase pyrolytic yield of levoglucosan from herbaceous feedstocks J. Bozell, Chemical and Materials from Renewable Resources 2001 ACS Symposium Series, Ameican Chemical Society Washington, DC 123 132
10. P. Patwardhan, J. Satrio, R. Brown, and B. Shanks Influence of inorganic salts on the primary pyrolysis products of cellulose Bioresource Technology 101 2010 4646 4655
11. G. Kwon, D. Kim, S. Kimura, and S. Kuga Rapid-cooling, continuous-feed pyrolyzer for biomass processing preparation of levoglucosan from cellulose and starch Journal of Analytical and Applied Pyrolysis 80 2007 1 5
12. G. Kwon, S. Kuga, K. Hori, M. Yatagai, K. Ando, and N. Hattori Saccharification of cellulose by dry pyrolysis Journal of Wood Science 52 2006 461 465
13. P.R. Patwardhan, J.A. Satrio, R.C. Brown, and B.H. Shanks Product distribution from fast pyrolysis of glucose-based carbohydrates Journal of Analytical and Applied Pyrolysis 86 2009 323 330
14. G. Dobele, G. Rossinskaja, T. Dizhbite, G. Telysheva, D. Meier, and O. Faix Application of catalysts for obtaining 1,6-anhydrosaccharides from cellulose and wood by fast pyrolysis Journal of Analytical and Applied Pyrolysis 74 2005 401 405
15. T. Funazukuri, R.R. Hudgins, and P.L. Silveston Product distribution in pyrolysis of cellulose in a microfluidized bed Journal of Analytical and Applied Pyrolysis 9 1986 139 158
16. M. Bajus Pyrolysis technologies for biomass and waste treatment to fuels and chemical production Petroleum and Coal 52 2010 1 10
17. V. Oja, and E.M. Suuberg Vapor pressures and enthalpies of sublimation of d-glucose, d-xylose, cellobiose and levoglucosan Journal of Chemical & Engineering Data 44 1999 26 29
18. E.M. Suuberg, I. Milosavljevic, and V. Oja Two-regime global kinetics of cellulose pyrolysis: the role of tar evaporation Twenty-Sixth Symposium (International) on Combustion 1996 1515 1521
19. F. Shafizadeh, C.W. Philpot, and N. Ostojic Thermal analysis of 1,6-anhydro-β-d-glucopyranose Carbohydrate Research 16 1970 279 287
20. M.L. Wolfrom, A. Thompson, and R.B. Ward The composition of pyrodextrins. II. Thermal Polymerization of levoglucosan Journal of the American Chemical Society 81 1959 4623 4625
21. G.R. Ponder, and G.N. Richards Polysaccharides from thermal polymerization of glucosides Carbohydrate Research 208 1990 93 104
22. Y. Houminer, and S. Patai Thermal polymerization of levoglucosan Journal of Polymer Science 7 1969 3005 3014
23. J. Carvaliio, W. Prins, and C. Schuerch Additional polymerization of anhydrosugar derivatives. I. A polyanhydroglucose Journal of the American Chemical Society 81 1959 4054 4058
24. H. Kawamoto, M. Murayama, and S. Saka Pyrolysis behavior of levoglucosan as an intermediate in cellulose pyrolysis: polymerization into polysaccharide as a key reaction to carbonized product formation Journal of Wood Science 49 2003 469 473
25. T. Hosoya, H. Kawamoto, and S. Saka Different pyrolytic pathways of levoglucosan in vapor- and liquid/solid-phases Journal of Analytical and Applied Pyrolysis 83 2008 64 70
26. F. Ronsse, X. Bai, W. Prins, and R.C. Brown Secondary reactions of levoglucosan and char in the fast pyrolysis of cellulose Environmental Progress & Sustainable Energy 31 2012 256 260