Analytical approach and occurrence for the determination of mass concentration of PCDD/PCDF and dl-PCB in flue gas emissions using long-term sampling devices

Science of the Total Environment

Volumn 435-436, Issue , 2012, Pages 7-13

  Rivera Austrui, J ^a   Martinez K ^a   Adrados, M A ^a   Abalos, M ^a   Abad, E ^a  

^a INSTITUTE OF ENVIRONMENTAL ASSESSMENT AND WATER RESEARCH   (Spain)

Author keywords

Dl PCB; Emissions; EN 1948; Long term sampling; Method validation; PCDD PCDF

Indexed keywords

DL-PCB; EN-1948; LONG-TERM SAMPLING; METHOD VALIDATIONS; PCDD/PCDFS;

FLUE GASES; GAS EMISSIONS; INCINERATION; PARTICULATE EMISSIONS; POLYCHLORINATED BIPHENYLS; WASTE INCINERATION;

ORGANIC POLLUTANTS;

DIOXIN; POLYCHLORINATED BIPHENYL; POLYCHLORINATED DIBENZODIOXIN; POLYCHLORINATED DIBENZOFURAN;

ANALYTICAL METHOD; COMBUSTION; INCINERATION; METHODOLOGY; MUNICIPAL SOLID WASTE; PCB; PCDD; PCDF; QUANTITATIVE ANALYSIS;

ACCURACY; AIR ANALYSIS; AIR MONITORING; ANALYTIC METHOD; ANALYTICAL BLANK; ANALYTICAL PARAMETERS; ARTICLE; CONCENTRATION (PARAMETERS); ENVIRONMENTAL MONITORING; EXTRACT ALIQUOT SIZE; EXTRACTION EFFICIENCY; FLUE GAS; HAZARD ASSESSMENT; HAZARDOUS WASTE; INCINERATION; LIMIT OF DETECTION; LIMIT OF QUANTITATION; PRIORITY JOURNAL; RELIABILITY; REPRODUCIBILITY; ROBUSTNESS; STANDARD;

AIR POLLUTANTS; DIOXINS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; INCINERATION; POLYCHLORINATED BIPHENYLS; REPRODUCIBILITY OF RESULTS; TETRACHLORODIBENZODIOXIN;

EID: 84870679148     PISSN: 00489697     EISSN: 18791026     Source Type: Journal    
DOI: 10.1016/j.scitotenv.2012.06.099     Document Type: Article

References (25)

1. CRM 490 The Certification of the Contents (Mass Fractions) of Five Polcyhlorodibenzo-p-Dioxins (D48, D54, D66, D67, D70) and Ten Polychlorodibenzofurans (F83, F94, F114, F114, F121, F124, F130) in Fly Ash. European Commission, BCR Information Series 1996, Reference Materials. Report EUR 16888 EN.
2. CRM 615 The Certification of the Contents (mass fractions) of Seven Polcyhlorodibenzo-p-Dioxins (D48, D54, D66, D67, D70, D73, D75) and Ten Polychlorodibenzofurans (F83, F94, F114, F114, F121, F124, F130, F131, F134, F135) in Low Level Fly Ash. European Commission, BCR Information Series 2002, Reference Materials. Report EUR 20283 EN.
3. Council Directive 2000/76/EC of 4 December 2000 on the waste incineration, Official Journal 28/12/2000, L 332/91-111.
4. EN-1948 Parts 1,2,3, 4 European Standard, Stationary Source Emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs 2006, European Committee for Standardization, Brussels.
5. Hattori S., Takaoka M., Matsumoto T., Oshita K., Takeda N., Tejima H., et al. Effect of de novo dioxin synthesis from boiler dust on dioxins emission from irregular operation of MSW Incinerator. Organohalogen Compd 2007, 69:182-185.
6. Horie Y., Yamamoto Y., Murotsu K., Reinmann J. Comparison of the performance of long-term automated sampling method of Amesa and those of JIS-TYPE I and TYPE III manual sampling methods for dioxins in flue gas. Organohalogen Compd 2007, 69:1305-1308.
7. Kawamoto K., Watanabe N., Asada S., Fujiyoshi H., Miyata H., Watanae G., et al. Dioxin surrogate under startup conditions of municipal waste incinerator. Organohalogen Compd 2007, 69:182-185.
8. Löthgren J.C., Van Bavel B. Dioxin emissions after installation of a polishing wet scrubber in a hazardous waste incineration facility. Chemosphere 2005, 61:405-412.
9. Martínez K., Rivera-Austrui J., Adrados M.A., Abalos M., Llerena J.J., van Bavel B., et al. Uncertainty assessment of polychlorinated dibenzo-p-dioxins and dibenzofuran and dioxin-like polychlorinated biphenyl analysis in stationary source sample emissions in accordance with the impending European standard EN-1948 using fly ashes. J Chromatogr A 2009, 1216:5888-5894.
10. Mayer J., Linnemann H., Becker E., Rentschler W., Jockel W., Wilbring P., et al. Certification of a long-term sampling system for PCDFs and PCDDs in the flue gas from industrial facilities. Chemosphere 2000, 40:1025-1027.
11. Ministère de l'écologie, de l'énergie, du développement durable et de la mer Arrêté du 3 aoÛt 2010 modifiant l'arrêté du 20 septembre 2002 relatif aux installations d'incinération et de co-incinération de déchets non dangereux et aux installations incinérant des déchets d'activités de soins à risques infectieux. J Off Répub Fr 2010, [Texte 10 sur 126, 21 aoÛt].
12. Mocak J., Bond A.M., Mitchell S., Scollary G. A statistical overview of procedures for determining the limits of detection and quantification: application to voltammetric and stripping techniques. Pure Appl Chem 1997, 69:297.
13. Neuer-Etscheidt K., Nordsieck H., Liu Y., Kettrup A., Zimmerman R. PCDD/F and other micropollutants in MSWI crude gas and ashes during plant start-up and shut-down processes. Environ Sci Technol 2006, 40:342-349.
14. Reinmann J., Roland W., Watson A. Continuous monitoring of unintentionally formed POPs listed under the Stockholm Convention (PCDDs/PCDFs, PCBs, HCB) using AMESA® long term sampling system. Organohalogen Compd 2006, 70:521-526.
15. Reinmann J., Weber R., Haag R. Long-term monitoring of PCDD/PCDF and other unintentionally produced POPs-concepts and case studies in Europe. Sci China Chem 2010, 53:1017-1024.
16. Reinmann J. More than 10 years continuous emission monitoring of dioxins by long-term sampling in Belgium and Europe-experiences, trends and new results. Organohalogen Compd 2011, 73:2209-2212.
17. Rivera-Austrui J., Borrajo J., Martínez K., Adrados M.A., Abalos M., Van Bavel B., et al. Assessment of polychlorinated dibenzo-p-dioxin and dibenzofuran emissions from a hazardous waste incineration plant using long-term sampling equipment. Chemosphere 2011, 82:1343-1349.
18. Rivera-Austrui J., Martínez K., Abad E., Rivera J., Guede E., Mostajo J. El control de emisiones de contaminantes persistentes en la utilización de combustibles alternativos en la industria del cemento. Rev Téc Cem Hormig 2010, 939:74-81.
19. Sakai S., Hiraoka M., Takeda N., Shiozaki K. Coplanar PCBs and PCDDs/PCDFs in municipal waste incineration. Chemosphere 1993, 27:233-240.
20. Sakurai T., Weber R., Ueno S., Nishino J., Tanaka M. Relevance of coplanar-PCBs for TEQ emission of fluidized bed incineration and impact of emission control devices. Chemosphere 2003, 53:619-625.
21. Steiner T. Long-term monitoring in the frame of the new European guideline EN1948-1. Organohalogen Compd 2003, 66:787-790.
22. Tejima H., Nishigaki M., Fujita Y., Matsumoto A., Takeda N., Takaoka M. Characteristics of dioxin emissions at startup and shutdown of MSW incinerators. Chemosphere 2007, 66:1123-1130.
23. UK Environment Agency Use of continuous isokinetic samplers for the measurement of dioxins and furans in emissions to atmosphere 2006, ISBN: 1844325504.
24. United Nations Environment Programme Stockholm Convention on persistent organic pollutants 2002, Geneva, Switzerland.
25. Wang L., Hsi H., Chang J., Yang X., Chang-Chien G., Lee W. Influence of start-up on PCDD/F emission of incinerators. Chemosphere 2007, 67:1346-1353.