An insight into the polymerization of anthracene oil to produce pitch using nuclear magnetic resonance

Fuel

Volumn 105, Issue , 2013, Pages 471-476

  Alvarez P ^a   Diez N ^a   Blanco, C ^a   Santamaria R ^a   Menendez R ^a   Granda, M ^a  

^a INSTITUTO NACIONAL DEL CARBÓN   (Spain)

Author keywords

Anthracene oil; Chemical structure; NMR; Pitch

Indexed keywords

ANTHRACENE OIL; C-H BOND; INERT ATMOSPHERES; INTERMEDIATE PRODUCT; NMR ANALYSIS; OXIDATIVE TREATMENT; PITCH; SHORT TIME SCALE; STRUCTURAL CHANGE;

ANTHRACENE; STRUCTURE (COMPOSITION);

NUCLEAR MAGNETIC RESONANCE;

EID: 84870463952     PISSN: 00162361     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.fuel.2012.09.047     Document Type: Article

References (26)

1. 3 by chromatography and related techniques J Chrom A 919 2001 255 266
2. A.L. Fernandez, M. Granda, J. Bermejo, and R. Menendez Catalytic polymerization of anthracene oil with aluminium trichloride Carbon 37 1999 1247 1255
3. J.J. Fernandez, and F. Alonso Anthracene oil synthetic pitch: a novel approach to hybrid pitches Light Metals 2004 499 502
4. P. Alvarez, M. Granda, J. Sutil, R. Menendez, J.J. Fernandez, and J.A. Viña Characterization and pyrolysis behaviour of novel anthracene oil derivatives Energy Fuels 22 2008 4077 4086
5. A. George, T.J. Morgan, P. Alvarez, M. Millan, A.A. Herod, and R. Kandiyoti Fractionation of a coal tar pitch by ultrafiltration and characterization by size exclusion chromatography, UV-fluorescence and laser desorption-mass spectroscopy Fuel 89 2010 2953 2970
6. P. Alvarez, G. Granda, J. Sutil, R. Santamaria, C. Blanco, and R. Menendez Preparation of low toxicity pitches by thermal oxidative condensation of anthracene oil Environ Sci Technol 43 2009 8126 8132
7. A.A. Herod, R. Kandiyoti, and K.D. Bartle Characterization of heavy hydrocarbon by chromatographic and mass spectrometric methods: an overview Energy Fuels 21 2007 2176 2203
8. A.A. Herod, K.D. Bartle, T.J. Morgan, and R. Kandiyoti Analytical methods for characterizing high-mass complex polydisperse hydrocarbon mixtures: an overview Chem Reviews 2012 3892 3923
9. M. Perez, M. Granda, R. Santamaria, T. Morgan, and R. Menéndez A thermoanalytical study of the co-pyrolysis of coal-tar pitch and petroleum pitch Fuel 83 2004 1257 1265
10. J. Bermejo, Fernandez.A.L. Granda, M. Rubiera, F. Suelves I, and R. Menendez Effects of thermal treatment on the composition and properties of air-blown anthracene oils Fuel 80 2001 1229 1231
11. A.L. Fernandez, M. Granda, J. Bermejo, and R. Menendez Air-blowing of anthracene oil for carbon precursors Carbon 38 2000 1315 1322
12. A. Dominguez, C. Blanco, R. Santamaria, M. Granda, C.G. Blanco, and R. Menendez Monitoring coal-tar pitch composition changes during air-blowing by gas chromatography J Chrom A 1026 2004 231 238
13. J. Bermejo, R. Menendez, A.L. Fernandez, M. Granda, I. Suelves, and A.A. Herod A comparative study of the composition of anthracene oil polymerized by different treatments Fuel 80 2001 2155 2162
14. A. Cristadoro, S.U. Kulkarni, W.A. Burgess, E.G. Cervo, H.J. Räder, and K. Müllen Structural characterization of the oligomeric constituents of petroleum pitches Carbon 47 2009 2358 2370
15. T.J. Morgan, A. George, P. Alvarez, M. Millan, A.A. Herod, and R. Kandiyoti Characterization of molecular mass ranges of two coal tar distillate fractions (creosote and anthracene oils) and aromatic Standards by LD-MS, GC-MS, probe-MS and size-exclusion chromatography Energy Fuels 22 2008 3275 3292
16. 13C-NMR methods for structural characterization of acetone & pyridine soluble/insoluble fractions of a coal tar pitch Energy Fuels 22 2008 1824 1835
17. 13C NMR. spectroscopy Fuel 64 1985 704 706
18. lH chemical shift correlation J. Mag. Reson. 57 1984 355 362
19. C. Díaz, and C.G. Blanco NMR: a powerful tool in the characterization of coal tar pitch Energy Fuels 17 2003 907 913
20. P. Alvarez, M. Granda, J. Sutil, R. Santamaria, C. Blanco, and R. Menendez A unified precess for preparing mesophase and isotropic material from anthracene oil-based pitch Fuel Process. Technol 92 2011 421 427
21. L. Rongbao, S. Zengmin, and L. Bailing Structural analysis of polycyclic aromatic hydrocarbons derived from petroleum and coal by carbon-13 and proton NMR spectroscopy Fuel 67 1988 565 569
22. E.M. Dickinson Structural comparison of petroleum fractions using proton and 13C NMR. spectroscopy Fuel 59 1980 290 294
23. M. Zander Physical and chemical properties of polycyclicaromatic hydrocarbons A. Bjorseth, Handbook of polycyclic and aromatic compounds 1983 Marcel and Dekker New York 1 26
24. H. Song, L. Liu, S.A. Qian, and B. Zhang Structural features and formation mechanism of soluble fractions of mesophase pitch derived from 1,2,4,5-tetramethylbenzene methylene-bridged oligomer Fuel 75 1996 1331 1338
25. M.D. Guillen, C. Diaz, and C.G. Blanco Characterization of coal tar pitches with different softening points by H-1 NMR - Role of the different kinds of protons in the thermal process Fuel Process. Technol 58 1998 1 15
26. I.C. Lewis, and L.S. Singer Polynuclear aromatic compounds B. Lawrence, Advances in chemistry series 217 1988: American Chemical Society Washington (DC) 269 285