Chemical preparation of samples of dead automobile catalyzers for subsequent determination of platinum, palladium, and rhodium using atomic emission spectrometry with inductively coupled plasma

Inorganic Materials

Volumn 48, Issue 14, 2012, Pages 1272-1278

  Dyachkova, A V ^a   Malutina, T M ^a   Alekseeva, T Yu ^b   Karpov, Yu A ^a  

^a INSTITUTE OF RARE METALS   (Russian Federation)

^b OOO Anserteko Analytical Ecological and Certification Center   (Russian Federation)

Author keywords

Acid decomposition; Alloying; Atomic emission spectrome try with inductively coupled plasma; Automobile catalyzers (catalytic converters); Chemical preparation of samples; Platinum group metals

Indexed keywords

ALLOYING; ATOMS; AUTOMOBILES; CATALYTIC CONVERTERS; DECOMPOSITION; PALLADIUM; PLATINUM; SPECTROMETRY;

ACID DECOMPOSITION; ATOMIC EMISSION; ATOMIC EMISSION SPECTROME-TRY WITH INDUCTIVELY COUPLED PLASMA; ATOMIC EMISSION SPECTROMETRY; AUTOMOBILE CATALYZER (CATALYTIC CONVERTER); CHEMICAL PREPARATION; CHEMICAL PREPARATION OF SAMPLE; INDUCTIVELY-COUPLED PLASMA; PLATINUM GROUP METALS; PLATINUM RHODIUM;

INDUCTIVELY COUPLED PLASMA;

EID: 84870285753     PISSN: 00201685     EISSN: 16083172     Source Type: Journal    
DOI: 10.1134/s0020168512140075     Document Type: Article

References (13)

1. Dubakin, V.A., Zotov, V.S., and Kuznetsov, S.D., Nei-tralizatsiya otrabotavshikh gazov avtomobil'nykh dvi-gatelei (Neutralization of exhaust gases of automobile engines), Moscow: Ekomash-KN, 2008
2. Heck, R.M. and Farrauto, R.J., Atomobile Exhaust Catalysts, Appl. Catal., A, 2001, no. 221, pp. 443-457
3. Simpson, L.A., Hearn, R., and Catterick, T., The Development of a High Accuracy Method for the Analysis of Pd, Pt and Rh in Auto Catalysts Using a Multi-Collector ICP-MS, J. Anal. At. Spectrom., 2004, vol. 19, pp. 1244-1251
4. Ginzburg, S.I., Ezerskaya, N.A., Prokof'eva, I.V., and Fedorenko, N.V., Analiticheskaya khimiya platinovykh metallov (Analytical Chemistry of Platinum Metals), Moscow: Nauka, 1972
5. Palacios, M.A., Gomez, M.M., Moldovan, M., and Morrison, G., Platinum-Group Elements Quantification in Collected Exhaust Fumes and Studies of Catalyst Surfaces, Sci. Total Environ., 2000, vol. 257, pp. 1-15
6. Rao, C.R.M. and Reddy, G.S., Platinum Group Metals (PGM); Occurrence, Use and Recent Trends in Their Determination, Trends Anal. Chem., 2000, vol. 19, no. 9, pp. 565-586
7. Puig, A.I. and Alvarado, J.I., Evaluation of Four Sample Treatments for Determination of Platinum in Automotive Catalytic Converters by Graphite Furnace Atomic Absorption Spectrometry, Spectrochim. Acta, Part B, 2006, vol. 61, pp. 1050-1053
8. Kylander, M.E., Rauch, S., Morrison, G.M., and Andam, K., Impact of Automobile Emissions on the Levels of Platinum and Lead in Accra, Ghana, J. Envi-ron. Monit., 2003, no. 5, pp. 91-95
9. Wayne, D.M., Direct Determination of Trace Noble Metals (Palladium, Platinum and Rhodium) in Automo-bile Catalysts by Glow Discharge Mass Spectrometry, J Anal. At. Spectrom., 1997, vol. 12, pp. 1195-1202
10. Dal'nova, O.A., Shiryaeva, O.A., Karpov, Yu.A., and Alekseeva, T.Yu., Direct Atomic-Absorption Determination of Platinum, Palladium, and Rhodium in Dead Auto Catalysis on a Ceramic Base, Zavod. Lab., Diagn Mater., 2009, vol. 75, no. 7, pp. 3-7
11. Malyutina, T.M., Alekseeva, T.Yu., D'yachkova, A.V., Kudryavtseva G.S., Berliner, L.D., and Karpov, Yu.A., Determination of Platinum and Palladium in Dead Cat-alysts Using the Method of Atomic-Emission Spectrom-etry with Inductively Coupled Plasma after Sample Decomposition Using High-Temperature Alloying, Zavod. Lab., Diagn. Mater., 2009, vol. 75, no. 1, pp. 4-7
12. Chudinov, E.G., Atomno-emissionnyi analiz s induktsion-noi plazmoi. Itogi nauki i tekhniki. Analiticheskaya khimiya (Atomic-Emission Analysis with Inductive Plasma), Moscow: VINITI, 1990, vol. 2
13. OST (Branch Standard) 153-39.2-032-2003: Dead Aluminum - Platinum Monometallic and Polymetallic Catalysts and Catalyst Production Residue, 2003