Solid-state STRAFI NMR probe for material imaging of quadrupolar nuclei

Journal of Magnetic Resonance

Volumn 225, Issue , 2012, Pages 93-101

  Tang, Joel A ^a   Zhong, Guiming ^b   Dugar, Sneha ^a   Kitchen, Jason A ^a   Yang, Yong ^b   Fu, Riqiang ^a  

^a FLORIDA STATE UNIVERSITY   (United States)

^b XIAMEN UNIVERSITY   (China)

Author keywords

Fringe field; Magnetic resonance imaging; Materials; Quadrupolar nuclei; Stray field imaging (STRAFI)

Indexed keywords

FRINGE FIELDS; IMAGING MATERIALS; IMAGING METHOD; LI-ION BATTERIES; MICROMETER SCALE; NMR PROBE; QUADRUPOLAR NUCLEUS; SOLID MATERIAL; STRAY FIELD;

IMAGE RESOLUTION; MAGNETIC RESONANCE IMAGING; MATERIALS; PROBES;

LITHIUM;

EID: 84868537825     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2012.10.009     Document Type: Article

References (77)

1. P.J. McDonald Stray field magnetic resonance imaging Prog. Nucl. Magn. Reson. Spectrosc. 30 1997 69 99
2. J.H. Baltisberger, S. Hediger, and L. Emsley Multi-dimensional magnetic resonance imaging in a stray magnetic field J. Magn. Reson. 172 2005 79 84
3. 1H NMR imaging of polybutadiene polystyrene blends Macromolecules 22 1989 1618 1621
4. R.A. Wind, and C.S. Yannoni Selective spin imaging in solids J. Magn. Reson. 36 1979 269 272
5. A. Wong, and D. Sakellariou Contrast STRAFI-MAS imaging J. Magn. Reson. 206 2010 264 268
6. D.G. Cory, J.B. Miller, and A.N. Garroway Time-suspension multiple-pulse sequences - applications to solid-state imaging J. Magn. Reson. 90 1990 205 213
7. 1H NMR imaging of solids - 2nd averaging Mol. Phys. 70 1990 331 345
8. S. Hafner, D.E. Demco, and R. Kimmich Magic-echo solid-state NMR imaging Meas. Sci. Technol. 2 1991 882 885
9. S. Matsui Solid-state NMR imaging by magic sandwich echoes Chem. Phys. Lett. 179 1991 187 190
10. J.B. Miller, D.G. Cory, and A.N. Garroway Line-narrowing approaches to solid-state NMR imaging - pulse gradients and 2nd averaging Philos. Trans. Roy. Soc. Lond. Ser. A - Math. Phys. Eng. Sci. 333 1990 413 426
11. A.A. Samoilenko, D.Y. Artemov, and L.A. Sibeldina Formation of sensitive layer in experiments on NMR subsurface imaging of solids JETP Lett. 47 1988 417 419
12. G. Bennett, J.P. Gorce, J.L. Keddie, P.J. McDonald, and H. Berglind Magnetic resonance profiling studies of the drying of film-forming aqueous dispersions and glue layers Magn. Reson. Imaging 21 2003 235 241
13. P.M. Glover, P.J. McDonald, and B. Newling Stray-field imaging of planar films using a novel surface coil J. Magn. Reson. 126 1997 207 212
14. P.D.M. Hughes, P.J. McDonald, N.P. Rhodes, J.W. Rockliffe, E.G. Smith, and J. Wills A stray field magnetic resonance imaging study of the drying of sodium silicate films J. Colloid Interface Sci. 177 1996 208 213
15. E. Ciampi, and P.J. McDonald Skin formation and water distribution in semicrystalline polymer layers cast from solution: a magnetic resonance imaging study Macromolecules 36 2003 8398 8405
16. P. Ekanayake, P.J. McDonald, and J.L. Keddie An experimental test of the scaling prediction for the spatial distribution of water during the drying of colloidal films Eur. Phys. J. - Spec. Top 166 2009 21 27
17. A.C. Hellgren, M. Wallin, P.K. Weissenborn, P.J. McDonald, P.M. Glover, and J.L. Keddie New techniques for determining the extent of crosslinking in coatings Prog. Org. Coat. 43 2001 85 98
18. J. Mallegol, A.M. Barry, E. Ciampi, P.M. Glover, P.J. McDonald, J.L. Keddie, M. Wallin, A. Motiejauskaite, and P.K. Weissenborn Influence of drier combination on through-drying in waterborne alkyd emulsion coatings observed with magnetic resonance profiling J. Coating Technol. 74 2002 113 124
19. J. Mallegol, G. Bennett, P.J. McDonald, J.L. Keddie, and O. Dupont Skin development during the film formation of waterborne acrylic pressure-sensitive adhesives containing tackifying resin J. Adhesion 82 2006 217 238
20. J. Mallegol, J.P. Gorce, O. Dupont, C. Jeynes, P.J. McDonald, and J.L. Keddie Origins and effects of a surfactant excess near the surface of waterborne acrylic pressure-sensitive adhesives Langmuir 18 2002 4478 4487
21. R. Rodriguez, C.D. Alarcon, P. Ekanayake, P.J. McDonald, J.L. Keddie, M.J. Barandiaran, and J.M. Asua Correlation of silicone incorporation into hybrid acrylic coatings with the resulting hydrophobic and thermal properties Macromolecules 41 2008 8537 8546
22. M. Wallin, P.M. Glover, A.C. Hellgren, J.L. Keddie, and P.J. McDonald Depth profiles of polymer mobility during the film formation of a latex dispersion undergoing photoinitiated cross-linking Macromolecules 33 2000 8443 8452
23. 19F magnetic resonance imaging of solid paramagnetic compounds using large magnetic field gradients and Hahn echoes Solid State Nucl. Magn. Reson. 8 1997 173 178
24. 31P paramagnetic displacements Magn. Reson. Chem. 40 2002 93 95
25. E.W. Randall, A.A. Samoilenko, and T. Nunes NMR imaging of paramagnetic solids in the high-field gradient approximation with the STRAFI method J. Magn. Reson., Ser. A 116 1995 122 124
26. N.R.A. Bird, A.R. Preston, E.W. Randall, W.R. Whalley, and A.P. Whitmore Measurement of the size distribution of water-filled pores at different matric potentials by stray field nuclear magnetic resonance Eur. J. Soil Sci. 56 2005 135 143
27. U. Goerke, A.H.L. Chamberlain, E.A. Crilly, and P.J. McDonald Model for water transport into powdered xanthan combining gel swelling and vapor diffusion Phys. Rev. E 62 2000 5353 5359
28. P. Kinchesh, E.W. Randall, and K. Zick Magnetic susceptibility effects in imaging - distortion-free images of plant tissue in soil Magn. Reson. Imaging 12 1994 305 307
29. P. Kinchesh, A.A. Samoilenko, A.R. Preston, and E.W. Randall Stray field nuclear magnetic resonance of soil water: development of a new, large probe and preliminary results J. Environ. Qual. 31 2002 494 499
30. A.R. Preston, N.R.A. Bird, P. Kinchesh, E.W. Randall, and W.R. Whalley STRAFI-NMR studies of water transport in soil Magn. Reson. Imaging 19 2001 561 563
31. E.W. Randall, N. Mahieu, and G.I. Ivanova NMR studies of soil, soil organic matter and nutrients: spectroscopy and imaging Geoderma 80 1997 307 325
32. M.A. Baumann, G.M. Doll, and K. Zick Stray-field imaging (STRAFI) of teeth Oral Surg. Oral Med. Oral Pathol. 75 1993 517 522
33. 19F nuclear magnetic resonance spectroscopy of dental materials by stray-field imaging J. Mater. Sci. - Mater. Med. 10 1999 369 373
34. 1H stray-field magnetic resonance imaging Polymer 42 2001 8051 8054
35. 1H stray-field long spin-echo trains and MRI: novel studies on the photopolymerization of a commercial dental resin J. Phys. D - Appl. Phys. 35 2002 1251 1257
36. S.G. Pereira, T.G. Nunes, and S. Kalachandra Low viscosity dimethacrylate comonomer compositions [Bis-GMA and CH(3)Bis-GMA] for novel dental composites; analysis of the network by stray-field MRI, solid-state NMR and DSC & FTIR Biomaterials 23 2002 3799 3806
37. S.G. Pereira, N. Reis, and T.G. Nunes Spatially resolved studies on the photopolymerization of dimethacrylate monomers Polymer 46 2005 8034 8044
38. T.G. Nunes, F.C.P. Garcia, R. Osorio, R. Carvalho, and M. Toledano Polymerization efficacy of simplified adhesive systems studied by NMR and MRI techniques Dent. Mater. 22 2006 963 972
39. R.A. Pires, C. Fernandez, and T.G. Nunes Structural and spatially resolved studies on the hardening of a commercial resin-modified glass-ionomer cement J. Mater. Sci. - Mater. Med. 18 2007 787 796
40. T.G. Nunes, S.G. Pereira, and S. Kalachandra Effect of treated filler loading on the photopolymerization inhibition and shrinkage of a dimethacrylate matrix J. Mater. Sci. - Mater. Med. 19 2008 1881 1889
41. S.G. Pereira, R. Fulgencio, T.G. Nunes, M. Toledano, R. Osorio, and R.M. Carvalho Effect of curing protocol on the polymerization of dual-cured resin cements Dent. Mater. 26 2010 710 718
42. C.H. Lloyd, S.N. Scrimgeour, D.M. Lane, G. Hunter, and P.J. McDonald The application of magnetic resonance microimaging to the visible light curing of dental resins - 3. Stray-field nuclear magnetic resonance imaging (STRAFI) Dent. Mater. 17 2001 381 387
43. G. Hunter, D.M. Lane, S.N. Scrimgeour, P.J. McDonald, and C.H. Lloyd Measurement of the diffusion of liquids into dental restorative resins by stray-field nuclear magnetic resonance imaging (STRAFI) Dent. Mater. 19 2003 632 638
44. S. Black, D.M. Lane, P.J. McDonald, D.J. Hannant, M. Mulheron, G. Hunter, and M.R. Jones The visualization of the ingress of polymer treatment coatings into porous building-materials by stray-field magnetic resonance imaging J. Mater. Sci. Lett. 14 1995 1175 1177
45. M. Dias, J. Hadgraft, P.M. Glover, and P.J. McDonald Stray field magnetic resonance imaging: a preliminary study of skin hydration J. Phys. D - Appl. Phys. 36 2003 364 368
46. I. Hopkinson, R.A.L. Jones, S. Black, D.M. Lane, and P.J. McDonald Fickian and Case II diffusion of water into amylose: a stray field NMR study Carbohydr. Polym. 34 1997 39 47
47. I. Hopkinson, R.A.L. Jones, P.J. McDonald, B. Newling, A. Lecat, and S. Livings Water ingress into starch and sucrose: starch systems Polymer 42 2001 4947 4956
48. K.L. Perry, P.J. McDonald, E.W. Randall, and K. Zick Stray field magnetic-resonance-imaging of the diffusion of acetone into poly(vinyl chloride) Polymer 35 1994 2744 2748
49. P. Bodart, T. Nunes, and E.W. Randall Stray-field imaging of quadrupolar nuclei of half integer spin in solids Solid State Nucl. Magn. Reson. 8 1997 257 263
50. A. Wong, and D. Sakellariou Two- and three-dimensional multinuclear stray-field imaging of rotating samples with magic-angle spinning (STRAFI-MAS): from bio to inorganic materials J. Magn. Reson. Imaging 32 2010 418 423
51. 14N in solids by the stray-field method: prospects for imaging using Long Echo-Train Summation Solid State Nucl. Magn. Reson. 14 1999 173 179
52. C.A. Michal, and R. Tycko Stray-field NMR imaging and wavelength dependence of optically pumped nuclear spin polarization in InP Phys. Rev. B 60 1999 8672 8679
53. 19F stray-field imaging in solids and liquids J. Magn. Reson., Ser. A 117 1995 317 319
54. 1-weighting of Hahn echo-trains in the stray-field for deuterium, prospects for imaging using long echo-train summation Solid State Nucl. Magn. Reson. 14 1999 165 172
55. R. Freeman Shaped radiofrequency pulses in high resolution NMR Prog. Nucl. Magn. Reson. Spectrosc. 32 1998 59 106
56. D.J. Lurie A systematic design procedure for selective pulses in NMR imaging Magn. Reson. Imaging 3 1985 235 243
57. M.A. McCoy, and W.S. Warren Implementation of simple crafted 90 or 180-degrees pulse shapes in fourier-transform NMR spectroscopy J. Magn. Reson. 65 1985 178 182
58. C. Bauer, R. Freeman, T. Frenkiel, J. Keeler, and A.J. Shaka GAUSSIAN pulses J. Magn. Reson. 58 1984 442 457
59. C. Coarna, and B. Newling Short, shaped pulses in a large magnetic field gradient J. Magn. Reson. 196 2009 127 132
60. MATLAB, The MathWorks Inc., Natick, Massachusetts, 2009.
61. E.W. Randall A convenient method for calibration of the pulse-length in high field-gradients using Hahn echo-trains Solid State Nucl. Magn. Reson. 8 1997 179 183
62. A.D. Bain, and E.W. Randall Hahn spin echoes in large static gradients following a series of 90 degrees pulses J. Magn. Reson., Ser. A 123 1996 49 55
63. C.E. Hayes, W.A. Edelstein, J.F. Schenck, O.M. Mueller, and M. Eash An efficient, highly homogeneous radiofrequency coil for whole body NMR imaging at 1.5 T J. Magn. Reson. 63 1985 622 628
64. J.M. Jin, G. Shen, and T. Perkins On the field inhomogeneity of a birdcage coil Magn. Reson. Med. 32 1994 418 422
65. D.W. Alderman, and D.M. Grant Efficient decoupler coil design which reduces heating in conductive samples in superconducting spectrometers J. Magn. Reson. 36 1979 447 451
66. D.M. Ginsberg, and M.J. Melchner Optimum geometry of saddle shaped coils for generating a uniform magnetic field Rev. Sci. Instrum. 41 1970 122 123
67. C.E.G. Salmon, E.L.G. Vidoto, M.J. Martins, and A. Tannus Optimization of saddle coils for magnetic resonance imaging Braz. J. Phys. 36 2006 4 8
68. D.I. Hoult, and R.E. Richards Signal-to-noise ratio of nuclear magnetic-resonance experiment J. Magn. Reson. 24 1976 71 85
69. CST Microwave Studio, Computer Simulation Technology of America, Framingham, Massachusetts, 2009.
70. M. Van Landeghem, B. Bresson, B. Blumich, and J.B.D. de Lacaillerie Micrometer scale resolution of materials by stray-field magnetic resonance imaging J. Magn. Reson. 211 2011 60 66
71. S.-B. Liao, P. Dourmashkin, J. Belcher, Introduction to Electricity and Magnetism, Pearson Custom Publishing, 2004.
72. W. Benenson, J.W. Harris, H. Stocker, H. Lutz (Eds.), Magnetic Fields of Various Current Distributions, Handbook of Physics, Springer, New York, 2002, pp. 477-478.
73. N. Bloembergen On the magnetic resonance absorption in conductors J. Appl. Phys. 23 1952 1383 1389
74. 7Li MRI of Li batteries reveals location of microstructural lithium Nat. Mater. 11 2012 311 315
75. C. Lim, B. Yan, L.L. Yin, and L.K. Zhu Simulation of diffusion-induced stress using reconstructed electrodes particle structures generated by micro/nano-CT Electrochim. Acta 75 2012 279 287
76. P.R. Shearing, L.E. Howard, P.S. Jorgensen, N.P. Brandon, and S.J. Harris Characterization of the 3-dimensional microstructure of a graphite negative electrode from a Li-ion battery Electrochem. Commun. 12 2010 374 377
77. 2 positive electrode J. Power Sources 196 2011 3443 3447