Development of heart-cutting multidimensional gas chromatography coupled to time of flight mass spectrometry for silicon speciation at trace levels in gasoline samples

Journal of Chromatography A

Volumn 1264, Issue , 2012, Pages 80-86

  Chainet, Fabien ^a   Lienemann, Charles Philippe ^a   Ponthus, Jérémie ^a   Courtiade, Marion ^a   Donard, Olivier François Xavier ^b  

^a IFP ENERGIES NOUVELLES   (France)

^b CNRS   (France)

Author keywords

Characterization; Deans switch; Gas chromatography; Gasoline; Heart cutting; Silicon; Trace level

Indexed keywords

ANALYTICAL SYSTEMS; CALIBRATION CURVES; CYCLIC SILOXANE; GASOLINE SAMPLES; HEART-CUTTING; HEXAMETHYL DISILOXANE; HYDROTREATMENT; LIMITS OF DETECTION; MULTIDIMENSIONAL GAS CHROMATOGRAPHY; RETENTION TIME; SECOND-DIMENSION COLUMN; SELECTIVITY AND SENSITIVITY; TIME OF FLIGHT MASS SPECTROMETRY; TRACE LEVEL;

CATALYST POISONING; CHARACTERIZATION; GAS CHROMATOGRAPHY; GASOLINE; MASS SPECTROMETRY; PETROLEUM PRODUCTS; SILICON;

SILICON COMPOUNDS;

GASOLINE; HEXAMETHYLDISILOXANE; NAPHTHA; PETROLEUM; SILICON; SILOXANE;

ANALYTIC METHOD; ARTICLE; CALIBRATION; CATALYST; CHEMICAL STRUCTURE; CONCENTRATION (PARAMETERS); GAS ANALYSIS; GAS CHROMATOGRAPHY; LIMIT OF DETECTION; PHASE SEPARATION; PRIORITY JOURNAL; PROCESS DEVELOPMENT; REACTION TIME; THERMAL ANALYSIS; TIME OF FLIGHT MASS SPECTROMETRY; VALIDATION PROCESS;

GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GASOLINE; LIMIT OF DETECTION; SILICON;

EID: 84867897289     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.09.020     Document Type: Article

References (25)

1. Chainet F., Lienemann C.P., Courtiade M., Ponthus J., Donard O.F.X. J. Anal. Atom. Spectrom. 2011, 26:30.
2. Dufresne P. Appl. Catal., A 2007, 322:67.
3. Rome C., Hueston T.G. Silicone in the Oil and Gas Industry 2002, Dow Corning Corporation, Ref. n°26-1139-01.
4. Kremer L.N., Hueston T.G. Petrol. Tech. Q. Summer 2002, 65.
5. ASTM Method Ref. D6733, Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 50-Metre Capillary High Resolution Gas Chromatography, 2011.
6. Chainet F., Courtiade M., Lienemann C.P., Ponthus J., Donard O.F.X. J. Chromatogr. A 2011, 1218:9269.
7. Chainet F., Ponthus J., Lienemann C.P., Courtiade M., Donard O.F.X. Anal. Chem. 2012, 84:3998.
8. Tranchida P.Q., Sciarrone D., Dugo P., Mondello L. Anal. Chim. Acta 2012, 716:66.
9. Omais B., Courtiade M., Charon N., Roullet C., Ponthus J., Thiebaut D. J. Chromatogr. A 2012, 1226:61.
10. Striebich R.C., Contreras J., Balster L.M., West Z., Shafer L.M., Zabarnick S. Energy Fuels 2009, 23:5474.
11. Sciarrone D., Tranchida P.Q., Ragonese C., Schipilliti L., Mondello L. J. Sep. Sci. 2010, 33:594.
12. Zeigler C., Wilthon N., Albert Robbat Anal. Chem. 2012, 84:2245.
13. Mitrevski B., Webster R.L., Rawson P., Evans D.J., Choi H.K., Marriott P.J. J. Chromatogr. A 2012, 1224:89.
14. Seeley J. J. Chromatogr. A 2012, 10.1016/j.chroma.2012.01.027.
15. F. Chainet, M. Courtiade, C.P. Lienemann, J. Ponthus, O.F.X. Donard, Unpublished work (2012) 1.
16. Omais B., Courtiade M., Charon N., Ponthus J., Thiebaut D. Anal. Chem. 2011, 83:7550.
17. Marriott P.J., Chin S.T., Maikhunthod B., Schmarr H.G., Bieri S. Trac-Trend Anal. Chem. 2012, 34:1.
18. Seeley J.V., Micyus N.J., Bandurski S.V., Seeley S.K., McCurry J.D. Anal. Chem. 2007, 79:1840.
19. Dvornic P.R. High temperature stability of polysiloxanes. Silicon Compounds: Silanes and Silicones 2004, Gelest Inc.
20. Camino G., Lomakin S.M., Lazzari M. Polymer 2001, 42:2395.
21. Camino G., Lomakin S.M., Lageard M. Polymer 2002, 43:2011.
22. Hamdani S., Longuet C., Perrin D., Lopez-Cuesta J.M., Ganachaud F. Polym. Degrad. Stab. 2009, 94:465.
23. Arnby K., Rahmani M., Sanati M., Cruise N., Carlsson A.A., Skoglundh M. Appl. Catal. B-Environ. 2004, 54:1.
24. Larsson A.C., Rahmani M., Arnby K., Sohrabi M., Skoglundh M., Cruise N., Sanati M. Top. Catal. 2007, 45:121.
25. Spivack J.L., Pohl P., Kochs P. The Handbook of Environmental Chemistry 1997, 105. Springer, New York. G. Chandra (Ed.).