Polyacetylenes as a new alignment medium to measure residual dipolar couplings for chiral organic molecules

Tetrahedron Letters

Volumn 53, Issue 47, 2012, Pages 6439-6442

  Dama, Murali ^a   Berger, Stefan ^a  

^a UNIVERSITY OF LEIPZIG   (Germany)

Author keywords

Anisotropic Alignment; Liquid Crystals; NMR Spectroscopy; Residual Dipolar Couplings

Indexed keywords

DEUTERIUM; MENTHOL; POLYACETYLENE; STRYCHNINE;

ARTICLE; CHEMICAL STRUCTURE; ENANTIOMER; LIQUID CRYSTAL; MOLECULAR INTERACTION; MOLECULAR WEIGHT; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RESIDUAL DIPOLAR COUPLING; STRUCTURE ANALYSIS; SYNTHESIS;

STRYCHNOS TOXIFERA;

EID: 84867856971     PISSN: 00404039     EISSN: 18733581     Source Type: Journal    
DOI: 10.1016/j.tetlet.2012.09.060     Document Type: Article

References (29)

1. P. Trigo-Mourino, A. Navarro-Vázquez, J. Ying, R.R. Gil, and A. Bax Angew. Chem., Int. Ed. 50 2011 7576 7580
2. R.R. Gil Angew. Chem., Int. Ed. 50 2011 7222 7224
3. N. Tjandra, and A. Bax Science 278 1997 1111 1114
4. J.A. Losonczi, and J.H. Prestegard J. Biomol. NMR 12 1998 447 451
5. M. Ottiger, and A. Bax J. Biomol. NMR 12 1998 361 372
6. F. Rinaldi, M. Lin, M.J. Shapiro, and M. Petersheim Biophys. J. 73 1997 3337 3348
7. V.V. Klochkov, R.F. Baikeev, V.D. Skirda, A.V. Klochkov, F.R. Muhamadiev, I. Baskyr, and S. Berger Magn. Reson. Chem. 47 2009 57 62
8. M.R. Hansen, L. Mueller, and A. Pardi Nat. Struct. Biol. 5 1998 1065 1074
9. M. Zweckstetter, and A. Bax J. Biomol. NMR 20 2001 365 377
10. J.D. Swarbrick, P. Ung, X.-C. Su, A. Maleckis, S. Chhabra, T. Huber, G. Otting, and B. Graham Chem. Commun. 47 2011 7368 7370
11. G. Pintacuda, M. John, X.-C. Su, and G. Otting Acc. Chem. Res. 40 2007 206 212
12. B. Luy, K. Kobzar, and H. Kessler Angew. Chem., Int. Ed. 43 2004 1092 1094
13. C.M. Thiele, and S. Berger Org. Lett. 5 2003 705 708
14. V. Madiot, D. Gree, R. Gree, P. Lesot, and J. Courtieu Chem. Commun. 2000 169 170
15. V.V. Klochkov, B.I. Khairutdinov, A.V. Klochkov, M.S. Tagirov, C.M. Thiele, S. Berger, I.S. Vershinina, I.I. Stoikov, I.S. Antipin, and A.I. Konovalov Russ. Chem. Bull. Int. Ed. 53 2004 1 5
16. M.D. Poliks, Y.W. Park, and E.T. Samulski Mol. Cryst. Liq. Cryst. 153 1987 321 346
17. A. Marx, B. Böttcher, and C.M. Thiele Chem. Eur. J. 16 2010 1656 1663
18. U.R. Prabhu, and N. Suryaprakash J. Magn. Reson. 202 2010 217 222
19. Z. Serhan, A. Borgogno, I. Billault, A. Ferrarini, and P. Lesot Chem. Eur. J. 18 2012 117 126
20. M.M. Green, J.W. Park, T. Sato, A. Teramoto, S. Lifson, R.L.B. Selinger, and J.V. Selinger Angew. Chem., Int. Ed. 38 1999 3138 3154
21. K. Maeda, and E. Yashima Top. Curr. Chem. 265 2006 47 88
22. T. Kajitani, K. Okoshi, S.I. Sakurai, J. Kumaki, and E. Yashima J. Am. Chem. Soc. 128 2006 708 709
23. G. Tian, Y. Lu, and B.M. Novak J. Am. Chem. Soc. 126 2004 4082 4083
24. L. Arnold, A. Marx, C.M. Thiele, and M. Reggelin Chem. Eur. J. 16 2010 10342 10346
25. M. Dama, and S. Berger Org. Lett. 14 2012 241 243
26. K. Okoshi, K. Sakajiri, J. Kumaki, and E. Yashima Macromolecules 38 2005 4061 4064
27. M. Zweckstetter Nat. Protoc. 2008 679 690
28. R. Berger, J. Courtieu, R.R. Gil, C. Griesinger, M. Köck, P. Lesot, B. Luy, D. Merlet, A. Navarro-Vazquez, M. Reggelin, U.M. Reinscheid, C.M. Thiele, and M. Zweckstetter Angew. Chem., Int. Ed. 124 2012 2 6
29. N.-C. Meyer, A. Krupp, V. Schmidts, C.M. Thiele, and M. Reggelin Angew. Chem., Int. Ed. 51 2012 8334 8338