메뉴 건너뛰기




Volumn 211-212, Issue , 2012, Pages 432-441

Design, fabrication and characterization of microreactors for high temperature syntheses

Author keywords

High temperature synthetic processes; Microreactor; On line syntheses; Process intensification; Quantum dots; Thermal microfluidic characterization

Indexed keywords

CONVENTIONAL METHODS; HIGH TEMPERATURE; HIGH THROUGHPUT; HIGH-TEMPERATURE REACTION; HIGH-TEMPERATURE SYNTHESIS; INDUSTRIAL FIELDS; KINETICS AND THERMODYNAMICS; LIQUID-PHASE REACTION; MICRO-FLUIDIC REACTORS; MICRO-REACTOR; ON-LINE SYNTHESIS; OPERATIONAL ENVIRONMENTS; ORGANIC REAGENTS; PROCESS INTENSIFICATION; REACTION CONTROL; SYNTHETIC PROCESS;

EID: 84867741236     PISSN: 13858947     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cej.2012.09.101     Document Type: Article
Times cited : (26)

References (51)
  • 2
    • 0034624399 scopus 로고    scopus 로고
    • Five-coordinate intermediates in carbon-carbon reductive elimination reactions from Pt(IV)
    • Crumpton D.M., Goldberg K.I. Five-coordinate intermediates in carbon-carbon reductive elimination reactions from Pt(IV). J. Am. Chem. Soc. 2000, 122(5):962-963.
    • (2000) J. Am. Chem. Soc. , vol.122 , Issue.5 , pp. 962-963
    • Crumpton, D.M.1    Goldberg, K.I.2
  • 3
    • 28944445286 scopus 로고    scopus 로고
    • Kinetic studies on the nucleophilic aromatic substitution of fluoronitrobenzene derivatives with polyvinylamine in water mediated by 2,6-O-dimethyl-β-cyclodextrin
    • Roth I., Spange S. Kinetic studies on the nucleophilic aromatic substitution of fluoronitrobenzene derivatives with polyvinylamine in water mediated by 2,6-O-dimethyl-β-cyclodextrin. Macromolecules 2005, 38:10034-10041.
    • (2005) Macromolecules , vol.38 , pp. 10034-10041
    • Roth, I.1    Spange, S.2
  • 6
    • 84870058755 scopus 로고    scopus 로고
    • Book review of catalysis of organic reactions
    • Laird T. Book review of catalysis of organic reactions. Org. Process Res. Dev. 2009, 13(6):1432.
    • (2009) Org. Process Res. Dev. , vol.13 , Issue.6 , pp. 1432
    • Laird, T.1
  • 7
    • 77149177349 scopus 로고    scopus 로고
    • Translating high-temperature microwave chemistry to scalable continuous flow processes
    • Damm M., Glasnov T.N., Kappe C.O. Translating high-temperature microwave chemistry to scalable continuous flow processes. Org. Process Res. Dev. 2010, 14(1):215-224.
    • (2010) Org. Process Res. Dev. , vol.14 , Issue.1 , pp. 215-224
    • Damm, M.1    Glasnov, T.N.2    Kappe, C.O.3
  • 9
    • 58349108450 scopus 로고    scopus 로고
    • Synthesis and characterization of ZnO nanocrystals from thermolysis of new precursor
    • Salavati-Niasari M., Davar F., Fereshteh Z. Synthesis and characterization of ZnO nanocrystals from thermolysis of new precursor. Chem. Eng. J. 2009, 146(3):498-502.
    • (2009) Chem. Eng. J. , vol.146 , Issue.3 , pp. 498-502
    • Salavati-Niasari, M.1    Davar, F.2    Fereshteh, Z.3
  • 10
    • 44149124249 scopus 로고    scopus 로고
    • Development of an original model for the synthesis of silicon nanodots by low pressure chemical vapor deposition
    • Cocheteau V., Mur P., Billon T., Scheid E., Caussat B. Development of an original model for the synthesis of silicon nanodots by low pressure chemical vapor deposition. Chem. Eng. J. 2008, 140(1-3):600-608.
    • (2008) Chem. Eng. J. , vol.140 , Issue.1-3 , pp. 600-608
    • Cocheteau, V.1    Mur, P.2    Billon, T.3    Scheid, E.4    Caussat, B.5
  • 12
    • 79551614063 scopus 로고    scopus 로고
    • Continuous flow multi-step organic synthesis
    • Webb D., Jamison F. Continuous flow multi-step organic synthesis. Chem. Sci. 2010, 1:675-680.
    • (2010) Chem. Sci. , vol.1 , pp. 675-680
    • Webb, D.1    Jamison, F.2
  • 13
    • 53749090735 scopus 로고    scopus 로고
    • Continuous flow reactors a tool for the modern synthetic chemist
    • Wiles C., Watts P. Continuous flow reactors a tool for the modern synthetic chemist. Eur. J. Org. Chem. 2008, 1655-1671.
    • (2008) Eur. J. Org. Chem. , pp. 1655-1671
    • Wiles, C.1    Watts, P.2
  • 14
    • 84857174482 scopus 로고    scopus 로고
    • Continuous flow reactors: a perspective
    • Wiles C., Watts P. Continuous flow reactors: a perspective. Green Chem. 2012, 14:38-54.
    • (2012) Green Chem. , vol.14 , pp. 38-54
    • Wiles, C.1    Watts, P.2
  • 15
    • 70349471035 scopus 로고    scopus 로고
    • Microchemical systems for continuous-flow synthesis
    • Hartman R.L., Jensen K.F. Microchemical systems for continuous-flow synthesis. Lab Chip 2009, 9:2495-2507.
    • (2009) Lab Chip , vol.9 , pp. 2495-2507
    • Hartman, R.L.1    Jensen, K.F.2
  • 16
    • 79957603428 scopus 로고    scopus 로고
    • Synthesis of gold nanoparticles in an interdigital micromixer using ascorbic acid and sodium borohydride as reducers
    • Luty-Błocho M., Fitzner K., Hessel V., Löb P., Maskos M., Metzke D.D., Pacławski K., Wojnicki M. Synthesis of gold nanoparticles in an interdigital micromixer using ascorbic acid and sodium borohydride as reducers. Chem. Eng. J. 2011, 171(1):279-290.
    • (2011) Chem. Eng. J. , vol.171 , Issue.1 , pp. 279-290
    • Luty-Błocho, M.1    Fitzner, K.2    Hessel, V.3    Löb, P.4    Maskos, M.5    Metzke, D.D.6    Pacławski, K.7    Wojnicki, M.8
  • 17
    • 79953298152 scopus 로고    scopus 로고
    • Bridging the gap: anested-pipereactor for slow reactions in continuous flow chemical synthesis
    • Minnich Clemens.B., Greiner Lasse., Reimers Christian., Uerdingen Marc., Liauw Marcel.A. Bridging the gap: anested-pipereactor for slow reactions in continuous flow chemical synthesis. Chem. Eng. J. 2011, 168(2):759-764.
    • (2011) Chem. Eng. J. , vol.168 , Issue.2 , pp. 759-764
    • Minnich, C.1    Greiner, L.2    Reimers, C.3    Uerdingen, M.4    Liauw, M.5
  • 18
    • 79952450514 scopus 로고    scopus 로고
    • Novel Process Window for the safe and continuous synthesis of tert.-butyl peroxy pivalate in a micro-reactor
    • Illg Tobias, Hessel Volker, Löb Patrick, Schouten Jaap C. Novel Process Window for the safe and continuous synthesis of tert.-butyl peroxy pivalate in a micro-reactor. Chem. Eng. J. 2011, 167(2):SI504-SI509.
    • (2011) Chem. Eng. J. , vol.167 , Issue.2
    • Illg, T.1    Hessel, V.2    Löb, P.3    Schouten, J.C.4
  • 19
    • 79952449846 scopus 로고    scopus 로고
    • Synthesis of polypyridine derivatives using alumina supported gold nanoparticles under micro continuous flow conditions
    • Abahmane Lahbib, Knauer Andrea, Michael Köhler J., Alexander Groß G. Synthesis of polypyridine derivatives using alumina supported gold nanoparticles under micro continuous flow conditions. Chem. Eng. J. 2011, 167(2-3):519-526.
    • (2011) Chem. Eng. J. , vol.167 , Issue.2-3 , pp. 519-526
    • Abahmane, L.1    Knauer, A.2    Michael Köhler, J.3    Alexander Groß, G.4
  • 20
    • 77956650822 scopus 로고    scopus 로고
    • Development of microchemical, biological and thermal systems in China: a review
    • Tu S.-T., Yu X., Luan W., Löwe H. Development of microchemical, biological and thermal systems in China: a review. Chem. Eng. J. 2010, 163(3):165-179.
    • (2010) Chem. Eng. J. , vol.163 , Issue.3 , pp. 165-179
    • Tu, S.-T.1    Yu, X.2    Luan, W.3    Löwe, H.4
  • 22
    • 26444454884 scopus 로고    scopus 로고
    • High-temperature microfluidic synthesis of CdSe nanocrystals in nanoliter droplets
    • Chan E.M., Alivisatos A.P., Mathies R.A. High-temperature microfluidic synthesis of CdSe nanocrystals in nanoliter droplets. J. Am. Chem. Soc. 2005, 127:13854.
    • (2005) J. Am. Chem. Soc. , vol.127 , pp. 13854
    • Chan, E.M.1    Alivisatos, A.P.2    Mathies, R.A.3
  • 23
    • 2542543730 scopus 로고    scopus 로고
    • A microfluidic device for conducting gas-liquid-solid hydrogenation reactions
    • Kobayashi J., Mori Y., Okamoto K., Akiyama R., Ueno M., Kitamori T., et al. A microfluidic device for conducting gas-liquid-solid hydrogenation reactions. Science 2004, 304:1305.
    • (2004) Science , vol.304 , pp. 1305
    • Kobayashi, J.1    Mori, Y.2    Okamoto, K.3    Akiyama, R.4    Ueno, M.5    Kitamori, T.6
  • 24
    • 79955047660 scopus 로고    scopus 로고
    • Kinetics research on fast exothermic reaction between cyclohexanecarboxylic acid and oleum in microreactor
    • Wang K., Lu Y.C., Xia Y., Shao H.W., Luo G.S. Kinetics research on fast exothermic reaction between cyclohexanecarboxylic acid and oleum in microreactor. Chem. Eng. J. 2011, 169(1-3):290-298.
    • (2011) Chem. Eng. J. , vol.169 , Issue.1-3 , pp. 290-298
    • Wang, K.1    Lu, Y.C.2    Xia, Y.3    Shao, H.W.4    Luo, G.S.5
  • 26
    • 53849096396 scopus 로고    scopus 로고
    • Flash chemistry: fast chemical synthesis by using microreactors
    • Yoshida J.-I., Nagaki A., Yamada T. Flash chemistry: fast chemical synthesis by using microreactors. Chem. Eur. J. 2008, 14:7450-7459.
    • (2008) Chem. Eur. J. , vol.14 , pp. 7450-7459
    • Yoshida, J.-I.1    Nagaki, A.2    Yamada, T.3
  • 27
  • 28
    • 1842471350 scopus 로고    scopus 로고
    • An investigation of Knoevenagel condensation reaction in microreactors using a new zeolite catalyst
    • Zhang X., Lai E.S.M., Martin-Aranda R., Yeung K.L. An investigation of Knoevenagel condensation reaction in microreactors using a new zeolite catalyst. Appl. Catal. A 2004, 261(1):109-118.
    • (2004) Appl. Catal. A , vol.261 , Issue.1 , pp. 109-118
    • Zhang, X.1    Lai, E.S.M.2    Martin-Aranda, R.3    Yeung, K.L.4
  • 29
    • 71649094664 scopus 로고    scopus 로고
    • Intensifying esterification reaction between lactic acid and ethanol by pervaporation dehydration using chitosan-TEOS hybrid membranes
    • Ma J., Zhang M., Lu L., Yin X., Chen J., Jiang Z. Intensifying esterification reaction between lactic acid and ethanol by pervaporation dehydration using chitosan-TEOS hybrid membranes. Chem. Eng. J. 2009, 155(3):800-809.
    • (2009) Chem. Eng. J. , vol.155 , Issue.3 , pp. 800-809
    • Ma, J.1    Zhang, M.2    Lu, L.3    Yin, X.4    Chen, J.5    Jiang, Z.6
  • 30
    • 36049023075 scopus 로고    scopus 로고
    • Process optimization of a catalyzed bleach oxidation for the production of functionalized aldehydes using microreaction technology
    • Ferstl W., Schwarzer M., Loebbecke S., Fritz-Langhals E., Stohrer J. Process optimization of a catalyzed bleach oxidation for the production of functionalized aldehydes using microreaction technology. Chem. Eng. J. 2008, 135(S1):S292-S297.
    • (2008) Chem. Eng. J. , vol.135 , Issue.S1
    • Ferstl, W.1    Schwarzer, M.2    Loebbecke, S.3    Fritz-Langhals, E.4    Stohrer, J.5
  • 31
    • 13944256949 scopus 로고    scopus 로고
    • TS-1oxidation of aniline to azoxybenzene in amicrostructuredreactor
    • Wan Y.S.S., Yeung K.L., Gavriilidis A. TS-1oxidation of aniline to azoxybenzene in amicrostructuredreactor. Appl. Catal. A 2005, 281(1-2):285-293.
    • (2005) Appl. Catal. A , vol.281 , Issue.1-2 , pp. 285-293
    • Wan, Y.S.S.1    Yeung, K.L.2    Gavriilidis, A.3
  • 32
    • 47649087927 scopus 로고    scopus 로고
    • Microfluidic synthesis of nanomaterials
    • Song Y., Hormes J., Kumar C.S.S.R. Microfluidic synthesis of nanomaterials. Small 2008, 4:698-711.
    • (2008) Small , vol.4 , pp. 698-711
    • Song, Y.1    Hormes, J.2    Kumar, C.S.S.R.3
  • 33
    • 79956369769 scopus 로고    scopus 로고
    • Direct synthesis and integration of functional nanostructures in microfluidic devices
    • Kim J., Li Z., Park I. Direct synthesis and integration of functional nanostructures in microfluidic devices. Lab on a Chip 2011, 11:1946-1951.
    • (2011) Lab on a Chip , vol.11 , pp. 1946-1951
    • Kim, J.1    Li, Z.2    Park, I.3
  • 34
    • 84862198028 scopus 로고    scopus 로고
    • Microreactor with integrated temperature control for the synthesis of CdSe nanocrystals
    • Gómez-de Pedro S., Martínez-Cisneros C.S., Puyol M., Alonso-Chamarro J. Microreactor with integrated temperature control for the synthesis of CdSe nanocrystals. Lab Chip 2012, 12:1979-1986.
    • (2012) Lab Chip , vol.12 , pp. 1979-1986
    • Gómez-de Pedro, S.1    Martínez-Cisneros, C.S.2    Puyol, M.3    Alonso-Chamarro, J.4
  • 36
    • 65249183800 scopus 로고    scopus 로고
    • High temperature synthesis of CdSe nanocrystals in a serpentine microchannel: wide size tenability achieved under a short residence time
    • Yang H., Luan W., Tu S., Wang Z.M. High temperature synthesis of CdSe nanocrystals in a serpentine microchannel: wide size tenability achieved under a short residence time. Cryst. Growth Des. 2009, 9:1569-1574.
    • (2009) Cryst. Growth Des. , vol.9 , pp. 1569-1574
    • Yang, H.1    Luan, W.2    Tu, S.3    Wang, Z.M.4
  • 38
    • 33745716795 scopus 로고    scopus 로고
    • A microfabricated gas-liquid segmented flow reactor for high-temperature synthesis: the case of CdSe quantum dots
    • Yen B.K.H., Gunther A., Schmidt M.A., Jensen K.F., Bawendi M.G. A microfabricated gas-liquid segmented flow reactor for high-temperature synthesis: the case of CdSe quantum dots. Angew. Chem Int. Ed. 2005, 117:5583-5587.
    • (2005) Angew. Chem Int. Ed. , vol.117 , pp. 5583-5587
    • Yen, B.K.H.1    Gunther, A.2    Schmidt, M.A.3    Jensen, K.F.4    Bawendi, M.G.5
  • 39
    • 26444454884 scopus 로고    scopus 로고
    • High-temperature microfluidic synthesis of CdSe nanocrystals in nanoliter droplets
    • Chan E.M., Alivisatos A.P., Mathies R.A. High-temperature microfluidic synthesis of CdSe nanocrystals in nanoliter droplets. J. Am. Chem. Soc. 2005, 127:13854-13861.
    • (2005) J. Am. Chem. Soc. , vol.127 , pp. 13854-13861
    • Chan, E.M.1    Alivisatos, A.P.2    Mathies, R.A.3
  • 40
    • 77956650822 scopus 로고    scopus 로고
    • Development of micro chemical, biological and thermal systems in China: a review
    • Tu S.-T., Yu X., Luan W., Löwe H. Development of micro chemical, biological and thermal systems in China: a review. Chem. Eng. J. 2010, 163(3):165-179.
    • (2010) Chem. Eng. J. , vol.163 , Issue.3 , pp. 165-179
    • Tu, S.-T.1    Yu, X.2    Luan, W.3    Löwe, H.4
  • 43
    • 84857225893 scopus 로고    scopus 로고
    • A ceramic microreactor for the synthesis of water soluble CdS and CdS/ZnS nanocrystals with on-line optical characterization
    • Gomez-dePedro S., Puyol M., Izquierdo D., Salinas I., delaFuente J.M., Alonso-Chamrro J. A ceramic microreactor for the synthesis of water soluble CdS and CdS/ZnS nanocrystals with on-line optical characterization. Nanoscale 2012, 4:1328-1335.
    • (2012) Nanoscale , vol.4 , pp. 1328-1335
    • Gomez-dePedro, S.1    Puyol, M.2    Izquierdo, D.3    Salinas, I.4    delaFuente, J.M.5    Alonso-Chamrro, J.6
  • 45
    • 77958607449 scopus 로고    scopus 로고
    • Continuous flow synthesis of nanoparticles using ceramic microfluidic devices
    • Gómez-de Pedro S., Puyol M., Alonso-Chamarro J. Continuous flow synthesis of nanoparticles using ceramic microfluidic devices. Nanotechnology 2010, 21:415603.
    • (2010) Nanotechnology , vol.21 , pp. 415603
    • Gómez-de Pedro, S.1    Puyol, M.2    Alonso-Chamarro, J.3
  • 47
    • 76149110104 scopus 로고    scopus 로고
    • Ceramic microsystem incorporating a microreactor with immobilized biocatalyst for enzymatic spectrophotometric assays
    • Baeza M., Lopez C., Alonso J., Lopez-Santin J., Alvaro G. Ceramic microsystem incorporating a microreactor with immobilized biocatalyst for enzymatic spectrophotometric assays. Anal. Chem. 2010, 82:1006-1011.
    • (2010) Anal. Chem. , vol.82 , pp. 1006-1011
    • Baeza, M.1    Lopez, C.2    Alonso, J.3    Lopez-Santin, J.4    Alvaro, G.5
  • 48
    • 39149145836 scopus 로고    scopus 로고
    • Green-tape ceramics. New technological approach for integrating electronics and fluidics in microsystems,
    • Ibanez-Garcia N., Martinez-Cisneros C.S., Valdes F., Alonso J. Green-tape ceramics. New technological approach for integrating electronics and fluidics in microsystems,. TRAC-TRENDS in Anal. Chem. 2008, 27:24-33.
    • (2008) TRAC-TRENDS in Anal. Chem. , vol.27 , pp. 24-33
    • Ibanez-Garcia, N.1    Martinez-Cisneros, C.S.2    Valdes, F.3    Alonso, J.4
  • 49
    • 0037028945 scopus 로고    scopus 로고
    • Control of photoluminescence properties of CdSe nanocrystals in growth
    • Qu L., Peng X. Control of photoluminescence properties of CdSe nanocrystals in growth. J. Am. Chem. Soc. 2002, 124:2049-2055.
    • (2002) J. Am. Chem. Soc. , vol.124 , pp. 2049-2055
    • Qu, L.1    Peng, X.2
  • 50
    • 65249183800 scopus 로고    scopus 로고
    • High-temperature synthesis of cdse nanocrystals in a serpentine microchannel: wide size tunability achieved under a short residence time
    • Yang H., Luan W., Tu S., Wang Z.M. High-temperature synthesis of cdse nanocrystals in a serpentine microchannel: wide size tunability achieved under a short residence time. Cryst. Growth Des. 2009, 9:1569-1574.
    • (2009) Cryst. Growth Des. , vol.9 , pp. 1569-1574
    • Yang, H.1    Luan, W.2    Tu, S.3    Wang, Z.M.4
  • 51
    • 34047251680 scopus 로고    scopus 로고
    • Open-to-air synthesis of monodisperse CdSe nanocrystals via microfluidic reaction and its kinetics
    • Luan W., Yang H., Tu S., Wang Z. Open-to-air synthesis of monodisperse CdSe nanocrystals via microfluidic reaction and its kinetics. Nanotechnology 2007, 18:175603.
    • (2007) Nanotechnology , vol.18 , pp. 175603
    • Luan, W.1    Yang, H.2    Tu, S.3    Wang, Z.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.