Partial conversion of methanol to formaldehyde in the gas chromatography injection port and reactivity with amines

Journal of Chromatography A

Volumn 1257, Issue , 2012, Pages 158-170

  Kee, Chee Leong ^a   Lai, Chian Sing ^a   Ge, Xiaowei ^a   Low, Min Yong ^a   Ciolino, Laura A ^b  

^a HEALTH SCIENCES AUTHORITY   (Singapore)

^b CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

Author keywords

Amines; GC MS; Injection port; Methanol; Oxazolidine; Variable inlet temperature

Indexed keywords

ALCOHOL MOIETIES; ANALYTES; CONDENSATION PRODUCT; GAS CHROMATOGRAPHS; GC-MS; INJECTION PORTS; INLET TEMPERATURE; ISOTOPIC LABELING; MASS SPECTRA; METHYLENE GROUPS; OXAZOLIDINES; PRIMARY AND SECONDARY AMINE; SOLVENT MIXTURES; SYSTEMATIC STUDY;

AMINES; EXPERIMENTS; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; METHANOL; PLASTICS;

FORMALDEHYDE;

ACETONITRILE; ALCOHOL; ALCOHOL DERIVATIVE; AMINE; CARBENOID; DESMETHYLSIBUTRAMINE; DIDESMETHYLSIBUTRAMINE; EPHEDRINE; FORMALDEHYDE; IMINE; METHANOL; NOREPHEDRINE; OXAZOLIDINE DERIVATIVE; SIBUTRAMINE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; CHEMICAL MODIFICATION; CHEMICAL REACTION; CONTROLLED STUDY; GAS CHROMATOGRAPHY; ISOTOPE LABELING; MASS SPECTROMETRY; POLYMERIZATION; PRIORITY JOURNAL; SOLVENT EFFECT; TEMPERATURE;

AMINES; CYCLOBUTANES; EPHEDRINE; FORMALDEHYDE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; IMINES; METHANOL; OXAZOLES; PHENYLPROPANOLAMINE; SOLVENTS; TEMPERATURE;

EID: 84865616409     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.08.021     Document Type: Article

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