Comparison of dialysis and solid-phase extraction for isolation and concentration of dissolved organic matter prior to Fourier transform ion cyclotron resonance mass spectrometry

Analytical and Bioanalytical Chemistry

Volumn 404, Issue 2, 2012, Pages 447-457

  M Tfaily, Malak ^a   Hodgkins, Suzanne ^a   Podgorski, David C ^a,b   Chanton, Jeffrey P ^a   Cooper, William T ^a  

^a FLORIDA STATE UNIVERSITY   (United States)

^b FLORIDA STATE UNIVERSITY   (United States)

Author keywords

Dialysis; Dissolved organic matter; Peatlands; Solid phase extraction; Ultrahigh resolution mass spectrometry of DOM

Indexed keywords

DISSOLVED ORGANIC MATTERS; DIVINYL BENZENES; FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETRY; IN-SITU; MICROBIAL PRODUCTION; MINNESOTA; MOLECULAR CHARACTERIZATION; MOLECULAR REPRESENTATIONS; ORGANOSULFUR COMPOUNDS; PEAT LAND; SOLID-PHASE EXTRACTION; ULTRAHIGH-RESOLUTION MASS SPECTROMETRY OF DOM;

BENZENE; BIOLOGICAL MATERIALS; BUTADIENE; CARBOHYDRATES; CARBOXYLIC ACIDS; ELECTROSPRAY IONIZATION; MASS SPECTROMETRY; PHASE SEPARATION; STYRENE; SULFUR COMPOUNDS; WETLANDS;

DIALYSIS;

CLUSTER ANALYSIS; COMPARATIVE STUDY; CONFERENCE PAPER; CYCLOTRON; DIALYSIS; FOURIER ANALYSIS; MASS SPECTROMETRY; METHODOLOGY;

CLUSTER ANALYSIS; CYCLOTRONS; DIALYSIS; FOURIER ANALYSIS; MASS SPECTROMETRY;

EID: 84865508405     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-012-6120-6     Document Type: Conference Paper

References (25)

1. Swietlik J, Sikorska E (2006) Characterization of natural organic matter fractions by high pressure size-exclusion chromatography, specific UVabsorbance and total luminescence spectroscopy. Pol J Environ Stud 15:145-153
2. Hudson N, Baker A, Reynolds D (2007) Fluorescence analysis of dissolved organic matter in natural, waste and polluted waters-a review. River Res Appl 23:631-649
3. Gorham E (1991) Northern peatlands-role in the carbon-cycle and probable responses to climatic warming. Ecol Appl 1:182-195
4. Backstrand K, Crill PM, Jackowicz-Korczynski M, Mastepanov M, Christensen TR, Bastviken D (2010) Annual carbon gas budget for a subarctic peatland, Northern Sweden. Biogeosciences 7:95-108
5. Moore TR, Knowles R (1987) Methane and carbon-dioxide evolution from sub-arctic fens. Can J Soil Sci 67:77-81
6. Moore TR, Knowles R (1989) The influence of water-table levels on methane and carbon-dioxide emissions from peatland soils. Can J Soil Sci 69:33-38
7. Thurman EM (1985) Organic geochemistry of natural waters, M. Nijhoff; Distributors for the U.S. and Canada, Kluwer Academic, Dordrecht; Boston Hingham, MA, USA
8. Kujawinski EB, Del Vecchio R, Blough NV, Klein GC, Marshall AG (2004) Probing molecular-level transformations of dissolved organic matter: insights on photochemical degradation and protozoan modification of DOM from electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. Mar Chem 92:23-37
9. Cole RB (2000) Some tenets pertaining to electrospray ionization mass spectrometry. J Mass Spectrom 35:763-772
10. Kujawinski EB (2002) Electrospray ionization fourier transform ion cyclotron resonance mass spectrometry (ESI FT-ICR MS): characterization of complex environmental mixtures. Environ Forensic 3:207-216
11. Aiken GR, Thurman EM, Malcolm RL, Walton HF (1979) Comparison of xad macroporous resins for the concentration of fulvicacid from aqueous-solution. Anal Chem 51:1799-1803
12. Lara RJ, Thomas DN (1994) XAD-fractionation of "new" dissolved organic matter: is the hydrophobic fraction seriously underestimated? Mar Chem 47:93-96
13. Kim S, Simpson AJ, Kujawinski EB, Freitas MA, Hatcher PG (2003) High resolution electrospray ionization mass spectrometry and 2D solution NMR for the analysis of DOM extracted by C18 solid phase disk. Org Geochem 34:1325-1335
14. Dittmar T, Koch B, Hertkorn N, Kattner G (2008) A simple and efficient method for the solid-phase extraction of dissolved organic matter (SPE-DOM) from seawater. Limnol Oceanogr-Methods 6:230-235
15. Benner R, Biddanda B, Black B, McCarthy M (1997) Abundance, size distribution, and stable carbon and nitrogen isotopic compositions of marine organic matter isolated by tangential-flow ultrafiltration. Mar Chem 57:243-263
16. Simjouw J-P, Minor EC, Mopper K (2005) Isolation and characterization of estuarine dissolved organic matter: comparison of ultrafiltration and C18 solid-phase extraction techniques. Mar Chem 96:219-235
17. Sleighter RL, Hatcher PG (2008) Molecular characterization of dissolved organic matter (DOM) along a river to ocean transect of the lower Chesapeake Bay by ultrahigh resolution electrospray ionization fourier transform ion cyclotron resonance mass spectrometry. Mar Chem 110:140-152
18. Koprivnjak JF, Pfromm PH, Ingall E, Vetter TA, Schmitt-Kopplin P, Hertkorn N, Frommberger M, Knicker H, Perdue EM (2009) Chemical and spectroscopic characterization of marine dissolved organic matter isolated using coupled reverse osmosis-electrodialysis. Geochim Et Cosmochim Acta 73:4215-4231
19. Kim S, Kramer RW, Hatcher PG (2003) Graphical method for analysis of ultrahigh-resolution broadband mass spectra of natural organic matter, the van Krevelen diagram. Anal Chem 75:5336-5344
20. McLafferty FW, Turececk F (1993) Interpretation of mass spectra. University Science, Mill Valley
21. Koch BP, Witt MR, Engbrod R, Dittmar T, Kattner G (2005) Molecular formulae of marine and terrigenous dissolved organic matter detected by electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. Geochim Et Cosmochim Acta 69:3299-3308
22. Minor EC, Steinbring CJ, Longnecker K, Kujawinski EB (2012) Characterization of dissolved organic matter in Lake Superior and its watershed using ultrahigh resolution mass spectrometry. Org Geochem 43:1-11
23. D'Andrilli J, Chanton JP, Glaser PH, Cooper WT (2010) Characterization of dissolved organic matter in northern peatland soil porewaters by ultra high resolution mass spectrometry. Org Geochem 41:791-799
24. De Leeuw JW, Largeau C (1993) A review of macromolecular organic compounds that comprise living organisms and their role in kerogen, coal, and petroleum formation. In: Engel MH, Macko SA (eds) Organic geochemistry: principles and applications. Plenum Press, New York, pp 23-72
25. Tfaily MM, Podgorski DC, Corbett JE, Chanton JP, Cooper WT (2011) Influence of acidification on the optical properties and molecular composition of dissolved organic matter. Analytica Chimica Acta 706:261-267