Rapid determination of alkylphenols in aqueous samples by in situ acetylation and microwave-assisted headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry

Journal of Separation Science

Volumn 35, Issue 16, 2012, Pages 2122-2130

  Wu, Yu Pei ^a   Wang, Yu Chen ^a   Ding, Wang Hsien ^a  

^a NATIONAL CENTRAL UNIVERSITY   (Taiwan)

Author keywords

Alkylphenols; GC MS; in situ Derivatization; Microwave assisted headspace solid phase microextraction; Water analysis

Indexed keywords

4-NONYLPHENOL ISOMER; 4-TERT-OCTYLPHENOL; ACETIC ANHYDRIDES; ALKYLPHENOLS; ANALYTES; AQUEOUS SAMPLES; DERIVATIZATIONS; ENVIRONMENTAL WATER SAMPLES; EXPERIMENTAL PROTOCOLS; EXTRACTION RECOVERY; GAS CHROMATOGRAPHY-ION TRAP MASS SPECTROMETRIES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GC-MS; HEAD-SPACE SOLID-PHASE MICROEXTRACTION; HEADSPACES; IN-SITU; IN-SITU DERIVATIZATION; ION STORAGE; LIMITS OF QUANTITATIONS; MICROWAVE-ASSISTED; OPTIMIZED CONDITIONS; RAPID DETERMINATION; RELATIVE STANDARD DEVIATIONS; SOLVENT-FREE PROCEDURES; STANDARD ADDITION METHOD;

ACETYLATION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; OPTIMIZATION; PHENOLS; SILICONES; SODIUM CHLORIDE; WATER ANALYSIS;

ISOMERS;

4 NONYLPHENOL; 4 TERT OCTYLPHENOL; ACETIC ANHYDRIDE; ALKYLPHENOL; DIMETICONE; DIVINYLBENZENE; POTASSIUM BICARBONATE; SODIUM CHLORIDE;

ACETYLATION; ARTICLE; CONTROLLED STUDY; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; MICROWAVE RADIATION; PRIORITY JOURNAL; PROCESS OPTIMIZATION; SOLID PHASE MICROEXTRACTION; WASTE WATER; WATER SAMPLING;

EID: 84865313122     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201200146     Document Type: Article

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