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Crystal Structure Data for Compound 12: M w =482.27; colorless platelet; 0.27×0.22×0.06mm; orthorhombic; P 2 1 2 1 2 1 ; a =10.0062(7)Å, b =11.8687(4)Å, c =18.6029(12)Å; V =2209.3(2)Å 3 ; Z =4; D =1.451g·cm -3 ; μ =0.209mm -1 . 66682 reflections were measured with a Nonius KappaCCD diffractometer (Mo radiation, graphite monochromator, λ=0.71073Å) up to a resolution of sin θ / λ =0.65 Å -1 at 208K. 5067 reflections were unique (R int =0.0423) of which 4371 were observed with I o 2σ(I o ). The structure was solved by direct methods with the PATTY option of the DIRDIF program system 23b,c and refined against F 2 using SHELXL. 23d All non-hydrogen atoms were refined with anisotropic temperature factors. The hydrogen atoms were placed at calculated positions and refined isotropically in riding mode. The three fluorine atoms could not be refined adequately because of rotational disorder. The absolute structure was determined based on the anomalous dispersion of 2199 Friedel pairs, Flack parameter=0.00(12), the Hooft parameter y=0.014(16). R 1 =0.0685 [I 2σ(I)]; R 1 =0.0806 [all reflections]; S=1.537. Residual electron density between 1.334 and -0.562e·Å -3 . The data were deposited with the Cambridge Crystallographic Data Centre (CCDC 882528). More detailed information can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif
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