Preparation and characterization of high water perm-selectivity ZSM-5 membrane without organic template

Journal of Membrane Science

Volumn 415-416, Issue , 2012, Pages 57-65

  Zhu, Mei Hua ^a,b   Lu, Zhang Hui ^b   Kumakiri, Izumi ^a   Tanaka, Kazuhiro ^a   Chen, Xiang Shu ^a,b   Kita, Hidetoshi ^a  

^a YAMAGUCHI UNIVERSITY   (Japan)

^b JIANGXI NORMAL UNIVERSITY   (China)

Author keywords

Crystallization time; Organic template free; Pervaporation; Water perm selectivity; ZSM 5 membrane

Indexed keywords

COLLOIDAL SILICA; CRYSTALLIZATION TIME; HIGH WATER; HYDROPHILIC PROPERTIES; OPTIMUM SYNTHESIS; ORGANIC TEMPLATES; ORGANIC-TEMPLATE FREE; PERMSELECTIVITIES; SEPARATION FACTORS; SILICA SOURCES; SILICALITE-1 CRYSTALS; SUPPORT TYPES; SYNTHESIS PARAMETERS; TEM CHARACTERIZATION; TEMPLATE-FREE; TOTAL FLUX; WELL WATER; XRD; ZSM-5 MEMBRANE;

ALUMINUM; EVAPORATION; HYDROTHERMAL SYNTHESIS; PERVAPORATION; SILICA; SILICATE MINERALS; SODIUM;

DEHYDRATION;

ACETONE; ALCOHOL; ALUMINUM; FLUORIDE SODIUM; METHANOL; SILICON DIOXIDE; WELL WATER;

ARTICLE; ARTIFICIAL MEMBRANE; COLLOID; CONTROLLED STUDY; CRYSTALLIZATION; PERFORMANCE; PERVAPORATION; PRECURSOR; PRIORITY JOURNAL; SCANNING ELECTRON MICROSCOPY; SYNTHESIS; TRANSMISSION ELECTRON MICROSCOPY; WATER PERMEABILITY; X RAY DIFFRACTION;

EID: 84864739455     PISSN: 03767388     EISSN: 18733123     Source Type: Journal    
DOI: 10.1016/j.memsci.2012.04.037     Document Type: Article

References (34)

1. Ulla M.A., Miro E., Mallada R., Coronas J., Santamaria J. Preparation of highly accessible mordenite coatings on ceramic monoliths at loadings exceeding 50% by weight. Chem. Commun. 2004, 528-529.
2. 2O over H-ZSM-5: acid catalyzed mechanism. J. Phys. Chem. B 2006, 110:16793-16800.
3. Holderich W.F., Bekkum H.V. Chapter 16 zeolites in organic syntheses. Stud. Surf. Sci. Catal. 1991, 58:631-726.
4. Ghobarkar H., Schaf O., Guth U. Zeolites-from kitchen to space. Prog. Solid State. Chem. 1999, 27:29-73.
5. Gues E.R., van Bekkum H. Calcination of large MFI-type single crystals, part 2: crack formation and thermomechanical properties in view of the preparation of zeolite membranes. Zeolites 1995, 15:333-341.
6. Noack M., Kolsch P., Seefeld V., Toussaint P., Georgi G., Caro J. Influence of the Si/Al-ratio on the permeation properties of MFI-membranes. Micropor. Mesopor. Mater. 2005, 79:329-337.
7. Mintova S., Hedlund J., Valtchev V., Schoeman B.J., Sterte J. ZSM-5 films prepared from template free precursors. J. Mater. Chem. 1998, 8:2217-2221.
8. Machado F.J., LoÂpez C.M., Centeno M.A., Urbina C. Template-free synthesis and catalytic behavior of aluminum-rich MFI-type zeolites. Appl. Catal. A: Gen. 1999, 181:29-38.
9. Lai R., Gavalas G.R. ZSM-5 membrane synthesis with organic-free mixtures. Micropor. Mesopor. Mater. 2000, 38:239-245.
10. Noack M., Kölsch P., Caro J., Schneider M., Toussaint P., Sieber I. MFI membranes of different Si/Al ratios for pervaporation and steam permeation. Micropor. Mesopor. Mater. 2000, 35-36:253-265.
11. Lassinantti M., Jareman F., Hedlund J., Creaser D., Sterte J. Preparation and evaluation of thin ZSM-5 membranes synthesized in the absence of organic template molecules. Catal. Today 2001, 67:109-119.
12. Pan M., Lin Y.S. Template-free secondary growth synthesis of MFI type zeolite membranes. Micropor. Mesopor. Mater. 2001, 43:319-327.
13. Li G., Kikuchi E., Matsukata M. A study on the pervaporation of water-acetic acid mixtures through ZSM-5 zeolite membranes. J. Membr. Sci. 2003, 218:185-194.
14. Li X.S., Kita H., Zhu H., Zhang Z.J., Tanaka K. Synthesis of long-term acid-stable zeolite membranes and their potential application to esterification reactions. J. Membr. Sci. 2009, 339:224-232.
15. Wang H.B., Lin Y.S. Synthesis and modification of ZSM-5/silicalite bilayer membrane with improved hydrogen separation performance. J. Membr. Sci. 2012, 396:128-137.
16. Arichi J., Louis B. Toward microscopic design of zeolite crystals: advantages of the fluoride-mediated synthesis. Cryst. Growth Des. 2008, 8:3999-4005.
17. Adachi-Pagano M., Forano C., Besse J.P. Synthesis of Al-rich hydrotalcite-like compounds by using the urea hydrolysis reaction-control of size and morphology. J. Mater. Chem. 2003, 13:1988-1993.
18. Zhang X.F., Liu H.O., Yeung K.L. Influence of seed size on the formation and microstructure of zeolite silicalite-1 membranes by seeded growth. Mater. Chem. Phys. 2006, 96:42-50.
19. Mintova S., Valtchev V. Effect of the silica source on the formation of nanosized silicalite-1: an in situ dynamic light scattering study. Micropor. Mesopor. Mater. 2002, 55:171-179.
20. Kalipcilar H., Culfaz A. Influence of nature of silica source on template-free synthesis of ZSM-5. Cryst. Res. Technol. 2001, 36:1197-1207.
21. Chao K.J., Tasi T.C., Chen M.S., Wang I. Kinetic studies on the formation of zeolite ZSM-5. J. Chem. Soc. Faraday Trans. 1981, 77:547-555.
22. Uguina M.A., de Lucas A., Ruiz F., Serano D.P. Synthesis of ZSM-5 from ethanol-containing systems. Influence of the gel composition. Ind. Eng. Chem. Res. 1995, 34:451-456.
23. 29Si triple resonance CP, REDOR, and TEDOR NMR experiments. J. Am. Chem. Soc. 2001, 123:6882-6891.
24. Louis B., Kiwi-Minsker L. Synthesis of ZSM-5 zeolite in fluoride media: an innovative approach to tailor both crystal size and acidity. Micropor. Mesopor. Mater. 2004, 74:171-178.
25. Zhang X.L., Zhu M.H., Zhou R.F., Chen X.S., Kita H. Synthesis of silicalite-1 membranes with high ethanol permeation in ultradilute solution containing fluoride. Sep. Purif. Technol. 2011, 81:480-484.
26. Helmkamp M.M., Davis M.E. Synthesis of porous silicalites. Annu. Rev. Mater. Sci. 1995, 25:161-192.
27. Singh R., Dutta P.K. MFI: a case study of zeolite synthesis, handbook of zeolite science and technology. Inorg. Chem. 2003, 21-63.
28. Aiello R., Crea F., Nigro E., Testa F., Mostowicz R., Fonseca A., Nagy J.B. The influence of alkali cations on the synthesis of ZSM-5 in fluoride medium. Micropor. Mesopor. Mater. 1999, 28:241-259.
29. Hasegawa Y., Abe C., Nishioka M., Sato K., Nagase T., Hanaoka T. Formation of high flux CHA-type zeolite membranes and their application to the dehydration of alcohol solutions. J. Membr. Sci. 2010, 364:318-324.
30. Feng X.S., Huang R.Y.M. Liquid separation by membrane pervaporation: a review. Ind. Eng. Chem. Res. 1997, 36:1048-1066.
31. Shah D., Kissick K., Ghorpade A., Hannah R., Bhattacharyya D. Pervaporation of alcohol-water and dimethylformamide-water mixtures using hydrophilic zeolite NaA membranes: mechanisms and experimental results. J. Membr. Sci. 2000, 179:185-205.
32. Li J., Nguyen Q.T., Zhou L.Z., Wang T., Long Y.C., Ping Z.H. Preparation and properties of ZSM-5 zeolite membrane obtained by low-temperature chemical vapor deposition. Desalination 2002, 147:321-326.
33. Lai R., Gavalas G.R. ZSM-5 membrane synthesis with organic-free mixtures. Micropor. Mesopor. Mater. 2000, 38:239-245.
34. Li S.G., Tuan V.A., Noble R.D., Falconer J.L. Pervaporation of water/THF mixtures using zeolite membranes. Ind. Eng. Chem. Res. 2001, 40:4577-4585.