Evaluation of injection conditions for preparative supercritical fluid chromatography

Journal of Chromatography A

Volumn 1250, Issue , 2012, Pages 256-263

  Miller, Larry ^a   Sebastian, Ian ^b  

^a AMGEN INC   (United States)

^b MERCK RESEARCH LABORATORIES   (United States)

Author keywords

Chiral chromatography; Enantioseparations; Preparative chromatography; Supercritical fluid chromatography

Indexed keywords

CHIRAL CHROMATOGRAPHY; CHROMATOGRAPHIC PERFORMANCE; DRUG CANDIDATES; ENANTIOSEPARATIONS; INJECTION CONDITIONS; INJECTION TECHNIQUES; INJECTION VOLUME; PHARMACEUTICAL DISCOVERY; PREPARATIVE CHROMATOGRAPHY; RAPID PURIFICATION; RESOLUTION OF ENANTIOMERS; SUPER CRITICAL FLUID CHROMATOGRAPHY; TRANS-STILBENE OXIDES;

DISSOLUTION; LIQUID CHROMATOGRAPHY;

GAS CHROMATOGRAPHY;

4 HYDROXYBENZOIC ACID; CHLORAMPHENICOL; CINCHOCAINE; DEXPANTHENOL; DIETHYLAMINE; DISOPYRAMIDE; DOXEPIN; FENOTEROL; GEMFIBROZIL; LABETALOL; METHANOL; METOPROLOL TARTRATE; METRONIDAZOLE; MIANSERIN; NABUMETONE; NAPROXEN; PHENAZONE; PROCAINAMIDE; PROPRANOLOL; PROPYL PARABEN; SOLVENT; SULCONAZOLE; SULFINPYRAZONE; TETRACAINE; TETRAMISOLE; THEOPHYLLINE; TOLBUTAMIDE; TRANS STILBENE OXIDE; UNINDEXED DRUG; WARFARIN;

ARTICLE; DISSOLUTION; DRUG RESEARCH; ELUTION; ENANTIOMER; FLOW RATE; PRIORITY JOURNAL; PURIFICATION; SUPERCRITICAL FLUID CHROMATOGRAPHY;

CHROMATOGRAPHY, SUPERCRITICAL FLUID; MODELS, CHEMICAL; PHARMACEUTICAL PREPARATIONS; STEREOISOMERISM; STILBENES;

EID: 84863873069     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.05.101     Document Type: Article

References (14)

1. Brocks D.R., Pasutto F.M., Jamali F. J. Chromatogr. 1992, 581:83.
2. Francotte E.R. Switz. Chimia 1997, 51(10):717.
3. Francotte E. Preparative Enantioselective Chromatography 2005, Blackwell Publishing.
4. Miller L., Honda D., Fronek R., Howe K. J. Chromatogr. A 1994, 658:429.
5. Francotte E.R. Switz. Chiral sep. 1997, 271. American Chemical Society. S. Ahuga (Ed.).
6. Cretier G., Majdalani R., Neffati J., Rocca J.L. Chromatographia 1994, 38(March (5/6)):330.
7. Hirata Y., Kawaguchi Y., Kitano K. Chromatographia 1995, 40(January (1/2)):42.
8. Gao J.Y., Kibbey C.E. Chromatographia 2000, 51(June (11/12)):747.
9. Yamauchi Y., Kuwajima M., Saito M. J. Chromatogr. 1990, 515:285.
10. T.A. Berger, K.D. Fogelman, US2003/0034307 A1.
11. Fogelman K. HPLC 2004 Poster 2004.
12. Neue U.D., Mazza C.B., Cavanaugh J.Y., Lu Z., Wheat T.E. Chromatographia Supplement 2003, 57:S-121.
13. Blom K.F. J. Combust. Chem. 2002, 4:295.
14. Shalliker R.A., Catchpoole H.J., Dennis G.R., Guiochon G. J. Chromatogr. A 2007, 1142:48.